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81. 发明专利

JPS61210076A NOVEL ADDUCT OF 2-SUBSTITUTED-4,6-DIAMINO-S-TRIAZINE AND ISOCYANURIC ACID, SYNTHESIS OF SAID ADDUCT, AND CURING OF POLYEPOXIDE RESIN USING SAID ADDUCT 失效
公开(公告)号：JPS61210076A
公开(公告)日：1986-09-18
申请号：JP5182885
申请日：1985-03-14
申请人： SHIKOKU CHEM
发明人： KAMAGATA KAZUO , YAMADA TOSHIAKI , SAWA NATSUO
IPC分类号： C07D251/18 , C07D251/32 , C07D401/12 , C07D403/12 , C08G59/00 , C08G59/40 , C08G59/50 , C08G59/56
摘要： NEW MATERIAL:The 2-substituted-4,6-diamino-s-triazine-isocyanuric acid adduct of formula I or formula II [R is ethyl, n-propyl, n-heptadecyl, methoxyethyl, aminoethyl, o-cyanophenyl, acetoxyethyl, etc.; R' is bis(diethylenetriamine-1,3)- ethyl or bis(m-xylylenediamino)-ethyl]. USE:Hardener for polyepoxide resin. A cured product having high heat-resistance, insulation property and adhesivity, and excellent migration resistance can be produced by the addition of the above adduct. PREPARATION:The titled adduct can be produced by heating the 2- substituted-4,6-diamino-s-triazine of formula III or formula IV with nearly equimolar amount of isocyanuric acid in the presence of water to obtain a homogeneous solution, cooling the solution and filtering and drying the precipitated crystal.

82. 发明专利

JPS61122280A Synthesis of 2-vinyl-4,6-diamino-s-triazine 失效
标题翻译： 2-乙烯基-4,6-二氨基-3-三唑的合成
公开(公告)号：JPS61122280A
公开(公告)日：1986-06-10
申请号：JP24265284
申请日：1984-11-17
申请人： Shikoku Chem Corp
发明人： SAWA NATSUO , MASUDA TAKESHI
IPC分类号： C07D251/18
摘要： PURPOSE: To obtain the titled compound on an industrial scale, at a low cost, by heating 2-{β-imidazolyl-(1')}-ethyl-4,6-diamino-s-triazine together with powdery or granular heat transfer medium in the presence of a polymerization inhibitor under reduced pressure.
CONSTITUTION: The objective compound of formula II useful as a comonomer can be produced from an inexpensive raw material with simple operation, in high yield, and accordingly by a method suitable for the practice on an industrial scale, by heating the compound of formula I together with a powdery or granular heat transfer medium such as quartz sand, sea sand, river sand, glass powder, silica powder, alumina powder, iron powder, copper powder, etc., in the presence of a polymerization inhibitor such as sodium sulfide, potassium sulfide, hydroquinone, copper sulfate, β-naphthylamine, etc., under a vacuum of 5W20mmHg at 80W320°C. The compound of formula I used as the starting compound can be pro- duced easily from acrylonitrile, imidazole and dicyandiamide by conventional method.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过将2- {β-咪唑基 - （1'） - 乙基-4,6-二氨基-s-三嗪与粉末或颗粒状热转移加热，以低成本获得工业规模的标题化合物在减压下在聚合抑制剂存在下进行。构成：用作共聚单体的式II的目的化合物可以通过简单的操作，高产率的廉价原料生产，因此通过适用于工业规模的方法，通过将式I化合物加热在石英砂，海砂，河砂，玻璃粉末，二氧化硅粉末，氧化铝粉末，铁粉，铜粉等粉末状或粒状的传热介质中，在阻聚剂如硫化钠，钾硫化物，氢醌，硫酸铜，β-萘胺等，在5-20mmHg的真空度下在80-320℃。用作起始化合物的式I化合物可以通过常规方法容易地从丙烯腈，咪唑和双氰胺生产。

83. 发明专利

JPS6160665A 1-(2-trifluoromethoxy-phenylsulfonyl)-3- heteroarylureas or thioureas 失效
标题翻译： 1-（2-三氟甲基 - 苯基氟基）-3-杂环或硫代
公开(公告)号：JPS6160665A
公开(公告)日：1986-03-28
申请号：JP18870485
申请日：1985-08-29
申请人： Bayer Ag
发明人： HANSU YOAHIMU DEIIRU , KURISUTA FUESUTO , RORUFU KIRUSUTEN , YOAHIMU KURUTO , KURAUSU HERUMUUTO MIYURAA , TEODOORU PUFUISUTAA , UBE PURIISUNITSUTSU , HANSU YOTSUHEMU RIIBERU , BORUFUGANGU ROI , HANSU YOAHIMU ZANTERU , ROBERUTO AARU SHIYUMITSUTO , RUUTOUITSUHI OIE , ERUNSUTO KIZERA
IPC分类号： A01N47/36 , C07C311/65 , C07C331/32 , C07D239/42 , C07D239/46 , C07D251/16 , C07D251/18 , C07D251/22 , C07D251/46 , C07D253/06 , C07D257/08 , C07D521/00
CPC分类号： C07D521/00 , A01N47/36 , C07C311/65 , C07C331/32

84. 发明专利

JPS6110564A Herbicidal sulfonamides 失效
公开(公告)号：JPS6110564A
公开(公告)日：1986-01-18
申请号：JP12237885
申请日：1985-06-05
申请人： Du Pont
发明人： DONARUDO JIYOSEFU DEYUMASU
IPC分类号： C07D251/16 , A01N47/34 , A01N47/36 , C07D239/42 , C07D239/47 , C07D239/52 , C07D239/70 , C07D251/18 , C07D251/22 , C07D251/42 , C07D251/46 , C07D251/50 , C07D251/52 , C07D491/048 , C07D491/052

85. 发明专利

JPS60228443A BETA-NAPHTHYLALKYLAMINES 失效
公开(公告)号：JPS60228443A
公开(公告)日：1985-11-13
申请号：JP7365085
申请日：1985-04-09
申请人： BAYER AG
发明人： YOAHIMU BAISUMIYURAA , BIRUHERUMU BURANDESU , GERUTO HENSURAA , PAURU RAINETSUKE
IPC分类号： C07D295/08 , A01N33/02 , A01N33/04 , A01N33/10 , A01N43/40 , A01N43/84 , C07C33/18 , C07C67/00 , C07C209/00 , C07C209/08 , C07C209/26 , C07C211/30 , C07C213/00 , C07C217/62 , C07D211/14 , C07D251/18 , C07D265/30 , C07D295/02 , C07D295/03 , C07D295/04

86. 发明专利

JPS60184076A NOVEL IMIDAZOLIUM COMPOUND, ITS SYNTHESIS, AND SYNTHESIS OF 2-VINYL-4,6-DIAMINO-S-TRIAZINE THEREFROM 失效
公开(公告)号：JPS60184076A
公开(公告)日：1985-09-19
申请号：JP3945884
申请日：1984-02-29
申请人： SHIKOKU CHEM
发明人： SAWA NATSUO , MASUDA TAKESHI
IPC分类号： C07D251/18 , C07D233/00 , C07D251/00 , C07D403/14
摘要： NEW MATERIAL:1,3-Di{beta-[4',6'-diamino-S-triazinyl-(2')]-ethyl}-2-methyli midazolium chloride shown by the formula I . USE:Useful as a precursor for synthesizing 2-vinyl-4,6-diamino-S-triazine useful as a comonomer. When this 2-vinyl-4,6-diamino-S-triazine is introduced to a side chain of high polymer, the high polymer has extremely raised softening point, glass transition point, and high specific gravity, and solubility is also extremely changed. PREPARATION:2-{ beta-[ 2'-Methylimidazolyl-(1') ]-ethyl }-4,6-diamino-S-triazine is reacted with benzyl chloride or allyl chloride, to give a compound shown by the formula I .

87. 发明专利

JPS60181076A SYNTHESIS OF 2-VINYL-4,6-DIAMINO-S-TRIAZINE 失效
公开(公告)号：JPS60181076A
公开(公告)日：1985-09-14
申请号：JP3669184
申请日：1984-02-27
申请人： SHIKOKU CHEM
发明人： SAWA NATSUO , MASUDA TAKESHI
IPC分类号： C07D251/18 , C07D403/06
摘要： PURPOSE:To produce the titled compound useful as a comonomer, from an inexpensive raw material, easily, in high yield, by reacting 2-[2'-methylimidazolyl (1)']-ethyl-4,6-diamino-S-triazine with epichlorohydrin. CONSTITUTION:The compound of formula III is produced by reacting 2-[2'-methylimidazolyl(1)']-ethyl-4,6-diamino-S-triazine of formula I with epichlorohyrin of formula II in an aqueous solution under heating. Concretely, the raw materials composed of 1mol of the compound of formula I , 1mol of epichlorohydrin of formula II, a small amount of a polymerization inhibitor and a proper amount of water are heated and refluxed for 30min under agitation. The product is cooled, and the obtained product is subjected to conventional recrystallization procedure to obtain the objective substance.

88. 发明专利

JPS59152377A N-phenylsulfonyl-n'-pyrimidinylurea and -n'-triazinylurea, manufacture and plant growth regulator 失效
标题翻译： N-苯基磺酰基-N'-吡啶二酮和-N'-三氮杂环戊二烯，制造和植物生长调节剂
公开(公告)号：JPS59152377A
公开(公告)日：1984-08-31
申请号：JP1929584
申请日：1984-02-04
申请人： Ciba Geigy Ag
发明人： RORUFU SHIYURUTAA , RUDORUFU SHII TSUMUMERU , BUERUNAA TEPUFURU , UIRII MAIYAA , DEIITAA DEYURU
IPC分类号： C07D249/16 , A01N47/36 , C07C67/00 , C07C301/00 , C07C311/39 , C07D207/38 , C07D207/40 , C07D207/404 , C07D239/42 , C07D239/46 , C07D239/47 , C07D251/16 , C07D251/18 , C07D251/22 , C07D251/46 , C07D251/52 , C07D275/02 , C07D521/00
CPC分类号： C07D207/404 , A01N47/36 , C07D207/38 , C07D239/42 , C07D239/47 , C07D251/16 , C07D275/02 , C07D521/00

89. 发明专利

JPS5989669A HERBICIDAL UREA DERIVATIVE 失效
公开(公告)号：JPS5989669A
公开(公告)日：1984-05-23
申请号：JP18765483
申请日：1983-10-06
申请人： CIBA GEIGY AG
发明人： HENRII SUTSUEPANSUKII
IPC分类号： C07D249/16 , A01N47/36 , C07C45/00 , C07C45/45 , C07C49/15 , C07C67/00 , C07D239/42 , C07D239/46 , C07D239/47 , C07D251/16 , C07D251/18 , C07D251/20 , C07D251/22 , C07D251/24 , C07D251/42 , C07D521/00

90. 发明专利

JPS5948465A Alkylsulfonylsulfonamides 失效
标题翻译： ALKYLSULFONYLSULFONAMIDES
公开(公告)号：JPS5948465A
公开(公告)日：1984-03-19
申请号：JP14581983
申请日：1983-08-11
申请人： Du Pont
发明人： JIYOOJI REBITSUTO , ANSONII DEBITSUDO URUFU
IPC分类号： C07D251/18 , A01N47/36 , C07D239/42 , C07D239/47 , C07D239/48 , C07D251/52

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