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61. 发明专利

JP2000178233A LIQUID CRYSTALLINE (METH)ACRYLATE COMPOUND, LIQUID CRYSTAL COMPOSITION CONTAINING THE COMPOUND AND OPTICALLY ANISOTROPIC MATERIAL PRODUCED BY USING THE COMPOSITION 失效
公开(公告)号：JP2000178233A
公开(公告)日：2000-06-27
申请号：JP21294499
申请日：1999-07-27
申请人： JAPAN CHEMICAL INNOVATION INST , AGENCY IND SCIENCE TECHN
发明人： HASEBE HIROSHI , SHIMIZU HIROSHI
IPC分类号： C07D521/00 , C07C69/92 , C08F20/26 , C09K19/38 , C09K19/42 , G02F1/13
摘要： PROBLEM TO BE SOLVED: To provide the subject new compound giving an optically anisotropic material having excellent transparency, etc., after polymerization. SOLUTION: The objective liquid crystalline (meth)acrylate compound is expressed by formula I (L1 to L3 are each H or methyl; the 6-membered rings A and B are each 1,4-phenylene, 1,4-cyclohexylene or the like; the 6-membered ring C is 1,3,4-benzenetriyl or the like; Y1 and Y2 are each single bond, CH2CH2 or the like; X1 to X3 are each single bond, O, COO or the like; Sp1 to Sp3 are each a 1-20C spacer group), e.g. the compound of formula II. The compound of formula I can be produced e.g. by bonding a spacer group added with hydroxyl group to each of a compound of formula III (the 6-membered rings A' and B' are each unsubstituted 1,4-phenylene or the like) and a compound of formula IV (the 6-membered ring C' is unsubstituted 1,3,4-benzenetriyl or the like) using a base, esterifying each of the obtained compounds with (meth)acrylic acid using an acid catalyst and bonding the reaction products with each other through ester bond by using a condensation agent and a base catalyst.

62. 发明专利

JP2000140632A SEPARATION MATERIAL USING STIMULUS RESPONSIVE POLYMER AND SEPARATION METHOD USING SAME 失效
公开(公告)号：JP2000140632A
公开(公告)日：2000-05-23
申请号：JP32093198
申请日：1998-11-11
申请人： JAPAN CHEMICAL INNOVATION INST , AGENCY IND SCIENCE TECHN
发明人： OKANO MITSUO , AKIYAMA YOSHIKATSU , YOSHIZAKO KIMIHIRO , UENO KATSUHIKO
IPC分类号： B01J20/285 , B01J20/26 , B01J20/281 , C08L33/26 , G01N30/54 , G01N30/88 , G01N30/48
摘要： PROBLEM TO BE SOLVED: To increase the recovery rate of a useful biopolymer by causing a physical or chemical change of a stimulus responsive polymer, physically or chemically varying the environment of interaction between molecules which interact with the objective material and the objective material and separating the objective material. SOLUTION: A physical or chemical change of a stimulus responsive polymer is caused and a composite of the stimulus responsive polymer, the objective material and molecules which interact with the objective material is held on a solid phase of a chemically modified filler for chromatography. The environment of interaction between the molecules and the objective material is then physically or chemically varied by stepwise varying the external temperature and the composite is passed through the same mobile phase to separate the objective material. Since severe chemical conditions are not used, the recovery rate of a useful biopolymer can be increased.

63. 发明专利

JP2000119222A LIQUID CRYSTALLINE (METH)ACRYLATE COMPOUND, LIQUID CRYSTAL COMPOSITION CONTAINING THE SAME COMPOUND AND OPTICALLY ANISOTROPIC BODY OBTAINED BY USING THE COMPOSITION 失效
公开(公告)号：JP2000119222A
公开(公告)日：2000-04-25
申请号：JP28854498
申请日：1998-10-09
申请人： JAPAN CHEMICAL INNOVATION INST , AGENCY IND SCIENCE TECHN
发明人： HASEBE HIROSHI , SHIMIZU HIROSHI
IPC分类号： C07D239/26 , C07C69/92 , C07D213/65 , C07D309/08 , C07D319/06 , C08F20/26 , C09K19/12 , C09K19/14 , C09K19/16 , C09K19/18 , C09K19/20 , C09K19/30 , C09K19/34 , C09K19/38
摘要： PROBLEM TO BE SOLVED: To provide the novel subject compound useful as optical, indicating and recording materials, an optical compensator for liquid crystal displays and a polarization prism material. SOLUTION: This liquid crystalline (meth)acrylate compound is expressed by formula I (L1 and L2 are each H or methyl; the six-membered rings A and B are each 1,4-phenylene, 1,4-cyclohexylene or the like; the six-membered ring C is 1,3-phenylene or the like; Y1 and Y2 are each a single bond, CH2CH2 or the like; X1 and X2 are each a single bond, O or OCO; Sp1 and Sp2 are each a 1-20C spacer group), e.g. a compound expressed by formula II. The compound of formula I is obtained, e.g. when X1 and Y2=OCO; Y1 = a single bond; X2=COO; L1=L2=L; the 6 membered rings A, B=6 membered rings A', B'; Sp1, Sp2=Sp, by heating a compound of formula III and a compound of formula IV in the presence of an acid catalyst such as p-toluenesulfonic acid at >=230 deg.C to obtain a compound of formula V, which is condensed with an alcohol derivative using a condensing agent, a basic catalyst, etc. to form an ester derivative.

64. 发明专利

JP2000044675A POLYPHENOL 失效
公开(公告)号：JP2000044675A
公开(公告)日：2000-02-15
申请号：JP21311798
申请日：1998-07-28
申请人： AGENCY IND SCIENCE TECHN , JAPAN CHEMICAL INNOVATION INST
发明人： KOBAYASHI SHIRO , UYAMA HIROSHI , OGUCHI TAKAHISA
IPC分类号： C12P7/22 , C08G65/44
摘要： PROBLEM TO BE SOLVED: To obtain a polyphenol useful as an electroconductive material or antioxidant by specifying the ratio for the extinction peak areas corresponding to each specific wavelength. SOLUTION: This polyphenol is such one as to be >=10 in the ratio A/B (A is the extinction peak area at wavelengths 960-986 cm-1, and B is the extinction peak area at wavelengths 996-1,018 cm-1 in the infrared absorption spectrum). This polyphenol is obtained, preferably by the following procedure: horseradish peroxidase dissolved in e.g. a phosphate buffer solution at pH 7 is dissolved in phenol dissolved in methanol followed by dripping 30 wt.% hydrogen peroxide to the resultant solution at a rate of 0.25 mL/h for 5 h and then agitation to carry out a polymerization of the phenol.

65. 发明专利

JP2000034188A PRODUCTION OF MICRO-POROUS CRYSTAL 失效
公开(公告)号：JP2000034188A
公开(公告)日：2000-02-02
申请号：JP19713698
申请日：1998-07-13
申请人： JAPAN CHEMICAL INNOVATION INST , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , HAMADA HIDEAKI
IPC分类号： C01B39/02 , C30B7/10 , C30B29/14 , C30B29/34
摘要： PROBLEM TO BE SOLVED: To provide a hydrothermal crystallization method for micro-porous crystals (aluminosilicate, aluminophosphate or the like) that can give a large single crystal useful as a molecular sieve, electronic devices, sensor or the like. SOLUTION: As resources for the elements constituting the skeleton of the micro-porous crystal (Si, Al, P, O and the like) among raw materials to be subjected to the reaction, are employed the bulks of the compounds containing these elements (silica, alumina, phosphoric acid or the like). These bulks have particles sizes that they cannot pass through the sieve of 0.5 mm mesh. Their shape may be any of lumps, plates, tubes and others. The usual reaction conditions for hydrothermal crystallization are applied in this process other than that the raw materials are used in the bulk forms. In comparison with the conventional synthetic process where the raw materials are used in the form of finely pulverized powders, the elution rates of the skeleton-constituting elements are suppressed and their super-saturation is decreased whereby the formation of crystal nucleuses are inhibited and the growth of the crystal is promoted. Thus, crystals with large sizes exceeding several hundred μm can be readily obtained.

66. 发明专利

JP2002220412A METHOD FOR PRODUCING TERMINALLY MODIFIED POLYPROPYLENE AND PROPYLENE.alpha-OLEFIN BLOCK COPOLYMER 失效
公开(公告)号：JP2002220412A
公开(公告)日：2002-08-09
申请号：JP2001019877
申请日：2001-01-29
申请人： JAPAN CHEMICAL INNOVATION INST
发明人： SANO YOJI , UOZUMI TOSHIYA , JIN JIJU , MURATA MASAHIDE , HOAN BAN TE , KAWABE MASANAO , FUKUI YOSHIFUMI , OZAKI HIROYUKI , KASE TOSHIO
IPC分类号： C08F297/08 , C08F4/645 , C08F8/00 , C08F10/06
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a terminally modified polypropylene and a propylene.α-olefin block copolymer in which the polymerization can be performed using an organometallic comlex catalyst in a high temperature region over the room temperature and the stereoregularity of a polypropylene portion is improved. SOLUTION: The method uses a specific titanium diamide complex, a specific organoaluminum compound and a specific boron compound.

67. 发明专利

JP2002161107A POLYMERIZATION CATALYST AND METHOD FOR PRODUCING POLYMER USING THE SAME 失效
公开(公告)号：JP2002161107A
公开(公告)日：2002-06-04
申请号：JP2000359676
申请日：2000-11-27
申请人： NAT INST OF ADV IND & TECHNOL , JAPAN CHEMICAL INNOVATION INST
发明人： TSUCHIHARA KENJI , ASAI MICHIHIKO , SUZUKI YASUZO , HAGIWARA HIDEAKI , MURATA MASAHIDE , OZAKI HIROYUKI , KAWABE MASANAO , KASE TOSHIO , HOAN TE BAN , JIN JIJU , FUKUI YOSHIFUMI
IPC分类号： C08F4/26 , C08F10/00 , C08F20/14 , C08F20/44
摘要： PROBLEM TO BE SOLVED: To provide a polymerization catalyst to be used for polymerization of polar vinyl monomers and/or olefins, and a method for producing a polymer using the above polymerization catalyst. SOLUTION: The polymerization catalyst to be used for polymerization of polar vinyl monomers and/or olefins, comprises a copper complex containing a terdentate phosphine ligand, and the method for producing a polymer is characterized by polymerizing polar vinyl monomers and/or olefins in the presence of the above polymerization catalyst.

68. 发明专利

JP2002080569A NEW SUBSTITUTED RESORCIN OXIDATIVE CONDENSATE 失效
公开(公告)号：JP2002080569A
公开(公告)日：2002-03-19
申请号：JP2000272120
申请日：2000-09-07
申请人： NAT INST OF ADV IND & TECHNOL , JAPAN CHEMICAL INNOVATION INST
发明人： HIGASHIMURA HIDEYUKI , KOBAYASHI SHIRO
IPC分类号： C08G65/40 , C08G61/10
摘要： PROBLEM TO BE SOLVED: To obtain a crystalline resorcin oxidative condensate having a substituent with >=5 number of carbon atoms. SOLUTION: This substituted resorcin oxidative condensate is obtained by performing an oxidative polymerization of a substituted resorcin expressed by formula I (wherein, Q2 is a >=5C aliphatic hydrocarbon group or a >=5C substituted aliphatic hydrocarbon group; Q1 is the same as the Q2 or in the case that it is different from the Q2, it is H, a 1-9C hydrocarbon group or a 19 C substituted hydrocarbon group; R1 to R4 are each independently H, a 1-9C hydrocarbon group, a 1-9C substituted hydrocarbon group, a 1-9C hydrocarbon group, a 1-9C substituted hydrocarbonoxy group, amino, a 1-9C substituted amino group, mercapto, a 1-9C substituted mercapto group or a halogen atom; and R1 together with R2 and/or R3 together with R4 may form a ring, but any 2 groups in Q1 and R1 to R4 are H).

69. 发明专利

JP2002080568A NEW SUBSTITUTED HYDROQUINONE OXIDATIVE CONDENSATE 失效
公开(公告)号：JP2002080568A
公开(公告)日：2002-03-19
申请号：JP2000272153
申请日：2000-09-07
申请人： NAT INST OF ADV IND & TECHNOL , JAPAN CHEMICAL INNOVATION INST
发明人： HIGASHIMURA HIDEYUKI , KOBAYASHI SHIRO
IPC分类号： C08G65/44 , C08G61/02
摘要： PROBLEM TO BE SOLVED: To obtain a crystalline hydroquinone oxidative condensate having an aliphatic hydrocarbon group with >=17 number of carbon atoms. SOLUTION: This new substituted hydroquinone oxidative condensate is obtained by performing an oxidative polymerization of a substituted hydroquinone expressed by formula I [wherein, Q2 is a >=17C aliphatic hydrocarbon group or a >=17C substituted aliphatic hydrocarbon group; Q1 is the same as the Q2 or in the case that it is different from the Q2, it is H, a 1-9C hydrocarbon group or a 1-9C substituted hydrocarbon group; R1 to R4 are each independently H, a 1-9C hydrocarbon group, a 1-9C substituted hydrocarbon group, amino, a 1-9C substituted amino group, mercapto, a 1-9C substituted mercapto group or a halogen atom; and R1 together with R2 or R3 together with R4 may form a ring, but any 2 groups in Q1 and R1 to R4 are H].

70. 发明专利

JP2002053663A (2,5-DISUBSTITUTED-1,4-PHENYLENE OXIDE) BLOCK COPOLYMER AND GRAFT COPOLYMER 失效
公开(公告)号：JP2002053663A
公开(公告)日：2002-02-19
申请号：JP2001102614
申请日：2001-03-30
申请人： NAT INST OF ADV IND & TECHNOL , JAPAN CHEMICAL INNOVATION INST
发明人： HIGASHIMURA HIDEYUKI , NAMEKAWA TAKAHIRA , KOBAYASHI SHIRO
IPC分类号： C08L55/00 , C08F290/06 , C08G65/48 , C08L71/12
摘要： PROBLEM TO BE SOLVED: To obtain both a new (2,5-disubstituted-1,4-phenylene oxide) block copolymer and a new (2,5-disubstituted-1,4-phenylene oxide) graft copolymer converted into a high molecular weight. SOLUTION: This (2,5-disubstituted-1,4-phenylene oxide) block copolymer has one or more units of block structural units represented by general formula (I) (wherein, R1 denotes a substituted or an unsubstituted hydrocarbon group; R4 denotes a trifunctional unsubstituted hydrocarbon group or a trifunctional substituted hydrocarbon group; U denotes CO, OCO or NHCO; a denotes the number-average degree of polymerization and a number of >=5; and f is 1 or 0) and one or more units of specific bivalent structural units in one molecule. The (2,5-disubstituted-1,4-phenylene oxide) graft polymer has one or more units of structural units represented by general formula (IV) or three or more units of the structural units represented by the general formula (IV) and specific bifunctional structural units in one molecule.

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