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41. 发明专利

JPS62160661A PRODUCTION OF THIN CARBON PLATE FOR FUEL CELL SEPARATOR 失效
公开(公告)号：JPS62160661A
公开(公告)日：1987-07-16
申请号：JP129386
申请日：1986-01-09
申请人： KAWASAKI STEEL CO
发明人： TAKANO SHIGERU , KANESHIRO TSUNEO
IPC分类号： H01M8/02
摘要： PURPOSE:To obtain thin carbon plates for separator excellent in gas impermeability, electric conductivity and mechanical strength without generating cracking and the like by combining phenol fiber, obtained such that novolak type phenol resin is spun and subjected to hardening process, with thermohardening resin and graphite powder. CONSTITUTION:Phenol fiber, obtained such that novolak type phenol resin is spun and subjected to hardening process, is combined with thermohardening resin and graphite powder. It is used as said phenol resin that is obtained by fusing and spinning phenol resin composed of phenol and formaldehyde by using acid catalyst, and subjecting same to hardening process at a temperature of 100 deg.C-150 deg.C. In case of felt or cloth type of said phenol resin, it is laminated and formed into a plate shape to have a desired thickness after being dipped in a solution where graphite powder and phenol resin powder are mixed, and dried. While in case of fiber type, it is formed into a plate shape after being mixed with phenol resin powder evenly. Next, said plate shape molding is completely hardened and thereafter heated to 1,000 deg.C to be carbonized so that thin carbon plates 1, 1' for fuel cell separator may be obtained.

42. 发明专利

JPS61162585A PRODUCTION OF HYDROGENATION-TREATED PITCH 失效
公开(公告)号：JPS61162585A
公开(公告)日：1986-07-23
申请号：JP287985
申请日：1985-01-11
申请人： KAWASAKI STEEL CO
发明人： HIROSE SHIRO , TSUBOTA HIDEKAZU , KANESHIRO TSUNEO , NAKAI SUSUMU
IPC分类号： D01F9/15 , C10C3/04 , D01F9/14 , D01F9/145 , D01F9/155
摘要： PURPOSE:To obtain the titled pitch suitable for carbonaceous ceramics, etc. without supplying expensive hydrogen-donating solvent from the outside of the system, by gas-liquid separation of a mixture of solvent ad hydrogenated pitch after heat treatment followed by hydrogenation of the solvent to retain its hydrogen-donating ability. CONSTITUTION:Feedstock pitch 1 and hydrogen-donating solvent 2 are fed to mixing tank 3, the resultant pitch-solvent mixture being conveyed to heating furnace 7 in a pressurized state. Before the introduction into this furnace 7, hydrogen 5 for use in reaction is incorporated in said mixture. The resulting mixture is heated in the furnace 7 followed by feeding to pitch hydrogenation column 8 to perform hydrogenation. The resultant reaction mixture comprising hydrogenated pitch, the solvent and a gas such as hydrogen is then introduced into high-pressure gas-liquid separator 9 to carry out gas-liquid separation. A gas phase from the top of the separator 9 is fed to solvent hydrogenation column 11 along with incorporation of hydrogen 6 for use in reaction to convert the solvent into a modified one with enhanced hydrogenation-donating ability. Gaseous phase 16 separated in the separator 9 is fed to low-pressure gas-liquid separator 17 and the objective hydrogenation-treated pitch being taken out through the bottom whereas solvent 18 being separated through the top.

43. 发明专利

JPS58134182A GAS-LIQUID SEPARATION METHOD IN COAL LIQUEFACTION PROCESS 失效
公开(公告)号：JPS58134182A
公开(公告)日：1983-08-10
申请号：JP1685682
申请日：1982-02-04
申请人： KAWASAKI STEEL CO , KAWATETSU KAGAKU KK
发明人： NAKAI SUSUMU , HIROSE SHIROU , KANESHIRO TSUNEO , KATOU TATSUHIKO , TSUBOTA HIDEKAZU
IPC分类号： C10G1/00 , C10G1/06
摘要： PURPOSE:To suppress the generation of mist in flushing, by controlling the liquid level of the reaction liquid of coal slurry in the reactor between the gas extraction port and the liquid extraction port, thereby charging the reaction liquid into the high-pressure separator after being separated into the gaseous phase and the liquid phase. CONSTITUTION:A reactor 2 is furnished with a gas extraction port 12 at its upper part and a liquid extraction port 13 at its lower part, and coal slurry is made to react in the reactor 2. The liquid level 14 of the reaction liquid is controlled to be positioned constantly between the gas extraction port 12 and the liquid extraction port 13. The gaseous phase and the liquid phase are separated from each other by this arrangement, and are charged to a high-pressure separation tank 3 through the lines 15 and 16, respectively. EFFECT:The generation of mist in flushing operation is suppressed, the solid component accompanied by the mist can be reduced, and the troubles in the following apparatuses by the solid component can be eliminated.

44. 发明专利

JPS5681386A PRODUCTION OF BLAST FURNACE COKE 失效
公开(公告)号：JPS5681386A
公开(公告)日：1981-07-03
申请号：JP15673579
申请日：1979-12-05
申请人： KAWASAKI STEEL CO
发明人： KANESHIRO TSUNEO , MIYAGAWA TSUGIO , TANIHARA HIDETAROU
IPC分类号： C10B57/04 , C10B57/06 , C10B57/08
摘要： PURPOSE:To obtain blast furnace coke in which the reactivity of the coke produced is easily controlled, by a method wherein regenerated coal in which the H/C mole ratio is adjusted to a value corresponding to the volatile matter of low-grade coal, is blended with the low-grade coal. CONSTITUTION:In the production of blast furnace coke from low-grade coal by blending regenerated coal with the low-grade coal, regenerated coal in which the H/C mole ratio is adjusted to a value corresponding to the volatile matter of the low-grade coal, is used. The reactivity of the coke is greatly varied depending on the H/C mole ratio of each component of the regenerated coal. Even when low- grade coal having a high content of the volatile matter is used as the raw material, the coke having low reactivity can be obtd. by blending regenerated coal having a small H/C mole ratio, or the component of the regenerated coal or a mixt. thereof with the low-grade coal. In order to classify the regenerated coal into components having different H/C mole ratio, a method such as a solvent separation method, a centrifugation method, a filtration method or a gravity settling method can be used.

45. 发明专利

JPS5556185A PRODUCTION OF METALLURGICAL COKE FROM GENERALLGRADE COAL 失效
公开(公告)号：JPS5556185A
公开(公告)日：1980-04-24
申请号：JP13024078
申请日：1978-10-23
申请人： KAWASAKI STEEL CO
发明人： KANESHIRO TSUNEO , MUROKI YOSHIO
IPC分类号： C10B57/04
摘要： PURPOSE:A modified coal that has been made by heating general-grade coal and a binder over the softening point of the binder to fuse them, a binder are incorporated to a low-fluidity coal in a specific proportion, thus producing said metallurigical coke with high strength. CONSTITUTION:Previously, a general-grade coal and a binder are heated together over the softening point of the binder to fuse them and prepare a modified coal. Then, the resulting modified coal and a binder are incorporated to a low-fluidity coal, thus producing said metallurgical coal. At this time, the mixing ratio of the binder to the low-fluidity coal is given as alpha, when the strength of the coke becomes maximum; the mixing ratio of the binder to the general coal is given as beta, when the strength of the coke becomes maximum; the contents of the low-fluidity coal, the modified coal and the binder are given as X1, X2, and X3 respectively and the amount of the binder and modified coal to be added are determined according to formula I and II and the mixing ratio of the binder in the modified coal and the general-grade coal is regulated by formula III, thus producing said metallurgical coke with high strength.

46. 发明专利

JPS5448802A MANUFACTURE OF COKE FOR IRON MANUFACTURE 失效
公开(公告)号：JPS5448802A
公开(公告)日：1979-04-17
申请号：JP11460077
申请日：1977-09-26
申请人： KAWASAKI STEEL CO
发明人： SUGIBE HIDETAKA , KANESHIRO TSUNEO , TANIHARA HIDETAROU , HIRATANI TATSUO
IPC分类号： C10B57/04

47. 发明专利

JPH0648829A PRECURSOR FOR CARBON FIBER-REINFORCED CARBON COMPOSITE MATERIAL 失效
公开(公告)号：JPH0648829A
公开(公告)日：1994-02-22
申请号：JP20111792
申请日：1992-07-28
申请人： KAWASAKI STEEL CO
发明人： URUNO TOMOYUKI , KANESHIRO TSUNEO
IPC分类号： B32B27/04 , C01B31/02 , C04B35/52 , C04B35/83 , C08J5/24
摘要： PURPOSE:To provide a precursor for carbon fiber-reinforced carbon composite material so that the decomposed gas of the matrix resin can be released from the precursor without damaging the precursor in order to obtain high-strength carbon fiber-reinforced carbon composite material. CONSTITUTION:This precursor for carbon fiber-reinforced carbon composite material consists of plural fiber bundles which consist of continuous long fiber of carbon fiber and continuous long fiber of thermoplastic resin and are impregnated with a thermosetting resin. The fiber diameter of the thermoplastic resin fiber is

48. 发明专利

JPH0543719A PRODUCTION OF PRECURSOR MOLDED BODY FOR CARBON-FIBER REINFORCED CARBON COMPOSITE MATERIAL 失效
公开(公告)号：JPH0543719A
公开(公告)日：1993-02-23
申请号：JP20926191
申请日：1991-08-21
申请人： KAWASAKI STEEL CO
发明人： EBATO OSAMU , URUNO TOMOYUKI , KANESHIRO TSUNEO
IPC分类号： B32B27/04 , C01B31/02 , C04B35/52 , C04B35/83 , C08J5/04 , C08J5/24
摘要： PURPOSE:To obtain the subject molded body capable of providing a carbon-fiber reinforced carbon composite material of a good shape without causing laminar cracks in burning and carbonizing by impregnating 4 carbon fiber woven fabric with a carbonizable resin, laminating the resultant sheets, pressurizing, heating and molding the laminate and subsequently heating the molded laminate under reduced pressure. CONSTITUTION:Carbon fiber woven fabric is impregnated with a carbonizable resin (e.g. a liquid phenolic resin), heated at ambient temperature for 4hr and then precured at 100 deg.C in an oven for 45min to provide a carbon fiber prepreg having 50% resin basis weight. The resultant woven fabric prepreg is then cut to 30cm square and 20 sheets are laminated, hot molded in an atmosphere at 150 deg.C under 2kg/cm pressure in an autoclave for 120min and subsequently heat-treated at 150 deg.C under 5mmHg vacuum in a vacuum dryer for 40hr to afford the objective precursor molded body, useful as a carbon-fiber reinforced carbon composite and capable of providing the carbon-fiber reinforced carbon composite having a good shape without causing laminar cracks in burning and carbonizing.

49. 发明专利

JPH04331811A ROLL-PROCESSED SCREW MADE OF C/C AND MANUFACTURE THEREOF 失效
公开(公告)号：JPH04331811A
公开(公告)日：1992-11-19
申请号：JP9917991
申请日：1991-04-30
申请人： KAWASAKI STEEL CO
发明人： SATO MASARU , KANESHIRO TSUNEO
IPC分类号： C04B35/83 , C04B35/52 , F16B35/00
摘要： PURPOSE:To provide a C/C made roll-processed screw and its manufacture wherein strength of a screw thread part of the C/C made male screw is improved by continuously forming a carbon fiber reinforcing member on the screw thread part, and which brings about the effects that a cost and labor are reduced by dispensing with mechanical processing. CONSTITUTION:In a roll-processed screw 1 made of C/C, a carbon fiber reinforcing member 2 composing a screw thread part 4 is continuously formed on an outer periphery of a core part 10 composed of a round bar made of C/C. The carbon fiber reinforcing member 2 impregnated with resin by using a rolling dies is wound around and superposed on the outer periphery of the C/C made round bar, to form the screw thread having a specified shape. Then, thermosetting and/or temporary sintering is performed by a heater provided on the rolling dies, followed by permanent sintering.

50. 发明专利

JPH04317464A PRODUCTION OF CARBON FIBER REINFORCED CARBON COMPOSITE MAETRIAL 失效
公开(公告)号：JPH04317464A
公开(公告)日：1992-11-09
申请号：JP7078091
申请日：1991-04-03
申请人： KAWASAKI STEEL CO
发明人： URUNO TOMOYUKI , EBATO OSAMU , KANESHIRO TSUNEO
IPC分类号： C01B31/02 , C04B35/52 , C04B35/80 , C04B35/83
摘要： PURPOSE:To prevent the swelling and interlaminar exfoliation of a resin molded body due to gas generated when the molded body obtd. by working carbon fibers as a reinforcing material into sheets with thermosetting resin as a binder, laminating the sheets and molding them under heating is fired to carbonize the resin. CONSTITUTION:A resin molded body to be fired to carbonize the resin is repeatedly heated to 100-250 deg.C and cooled to

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