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12. 发明专利

JP2005089343A Method for producing alicyclic ketone compound 审中-公开
标题翻译：制备高分子酮酮化合物的方法
公开(公告)号：JP2005089343A
公开(公告)日：2005-04-07
申请号：JP2003322605
申请日：2003-09-16
申请人： Tokuyama Corp , 株式会社トクヤマ
发明人： HIROTA YOSHIHIRO , SHIIKI TAKAFUMI , YAMAGUCHI MASAO
IPC分类号： C07C49/453
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an alicyclic ketone compound in a high yield, by which an alicyclic hydrocarbon compound or an alicyclic alcohol compound is oxidized with sulfuric acid. SOLUTION: In the method for producing an alicyclic ketone compound such as 2-adamantanone, etc., by which an alicyclic hydrocarbon compound such as adamantane, cyclohexane, etc., or an alicyclic alcohol compound such as cyclohexanol, 1-adamantanol, etc., is oxidized in sulfuric acid, sulfuric acid oxidation is carried out in the presence of at least one kind of a reaction type desiccating agent such as phosphorus pentoxide, etc. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供以高产率制备脂环族酮化合物的方法，通过该方法脂肪族烃化合物或脂环族醇化合物被硫酸氧化。解决方案：在用于生产诸如金刚烷，环己烷等脂环族烃化合物或脂环族醇化合物如环己醇，1-金刚烷醇等脂环族酮化合物的2-金刚烷酮等的制造方法中，等等，在硫酸中氧化，硫酸氧化在至少一种反应型干燥剂如五氧化二磷等的存在下进行。版权所有（C）2005，JPO＆NCIPI

13. 发明专利

JP2005082582A Manufacturing method of 2-adamantanone 审中-公开
标题翻译： 2-ADAMANTANONE的制备方法
公开(公告)号：JP2005082582A
公开(公告)日：2005-03-31
申请号：JP2003319891
申请日：2003-09-11
申请人： Tokuyama Corp , 株式会社トクヤマ
发明人： SHIIKI TAKAFUMI , TANAKA NORIHIRO , HIROTA YOSHIHIRO , YAMAGUCHI MASAO
IPC分类号： C07C45/28 , C07B61/00 , C07C45/29 , C07C49/453
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing 2-adamantanone containing a little amount of resinous compounds with an increased isolation yield of 2-adamantanone.
SOLUTION: 2-Adamantanone is manufactured by oxidizing at least one raw material compound selected from the group consisting of adamantane, 1-adamantanol and 2-adamantanol in the presence of an inorganic salt such as sodium sulfate, potassium sulfate, magnesium sulfate or calcium sulfate in an amount of 0.01-10 times equivalent of the raw material compound in concentrated sulfuric acid or fuming sulfuric acid.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供一种含有少量树脂化合物的2-金刚烷酮的方法，其中2-金刚烷酮的分离收率提高了。解决方案：2-金刚烷酮通过在无机盐如硫酸钠，硫酸钾，硫酸镁存在下氧化至少一种选自金刚烷，1-金刚烷醇和2-金刚烷醇的原料化合物来制备或硫酸钙，其量为浓硫酸或发烟硫酸中原料化合物的0.01-10倍。版权所有（C）2005，JPO＆NCIPI

14. 发明专利

JPWO2002036533A1 電子吸引性基含有単量体及びその製造法有权
公开(公告)号：JPWO2002036533A1
公开(公告)日：2004-03-11
申请号：JP2002539295
申请日：2001-10-31
申请人：ダイセル化学工業株式会社
发明人：井上　慶三
IPC分类号： C08F24/00 , C07C29/40 , C07C33/44 , C07C35/52 , C07C41/01 , C07C41/06 , C07C41/58 , C07C43/172 , C07C43/178 , C07C43/192 , C07C43/196 , C07C43/313 , C07C45/64 , C07C45/66 , C07C45/68 , C07C49/453 , C07C49/513 , C07C49/653 , C07C49/755 , C07D307/00 , C07D307/30 , C07D307/93 , C07D313/10 , C07D317/42 , C07D339/06 , C08F16/00 , C08F34/00 , G03F7/004 , G03F7/039
CPC分类号： C07C41/58 , C07C33/44 , C07C35/52 , C07C41/06 , C07C41/54 , C07C41/56 , C07C43/313 , C07C43/317 , C07C49/755 , C07C2602/42 , C07C2603/74 , C07D307/30 , C07D307/93 , C07D313/10 , C07D317/42 , C07D339/06 , C08F24/00 , G03F7/0046 , G03F7/0397 , C07C43/1786 , C07C43/196
摘要：本発明の電子吸引性基含有単量体は、下記式(a)、(b)又は(c)(式中、A1、A2、A3は環を示し、Ra、Rb、Rc、Ruは、同一又は異なって、水素原子又は有機基を示す。Rs、Rw及びRvのうち少なくとも1つ、Rt及びRw1のうち少なくとも1つ、2つのRw2のうち少なくとも1つは、それぞれ電子吸引基を示し、残りは水素原子又は有機基を示す。W1は単結合又は連結基を示し、nは2〜25の整数を示す。Ra、Rb、Rc、Rs、Rt、Ru、Rv、Rw、Rw1、Rw2、W1、A1環を構成する炭素原子、A2環を構成する炭素原子、A3環を構成する炭素原子は、それぞれ2以上が結合して環を形成していてもよい)で表される。前記Rs、Rt、Rv、Rw、Rw1、Rw2における電子吸引性基は、例えばフッ素原子含有基である。この単量体はフォトレジスト用高分子化合物の原料として有用である。

15. 发明专利

JP2003267906A METHOD FOR PRODUCING 2-ADAMANTANONE 审中-公开
公开(公告)号：JP2003267906A
公开(公告)日：2003-09-25
申请号：JP2002070082
申请日：2002-03-14
申请人： TOKUYAMA CORP
发明人： TANAKA KENJI , YAMAGUCHI MASAO , SHIIKI TAKAFUMI
IPC分类号： C07C45/28 , C07C49/453
摘要： PROBLEM TO BE SOLVED: To develop a method for producing 2-adamantanone in high yield and high purity in oxidation of adamantane with sulfuric acid. SOLUTION: In the method for producing 2-adamantanone by oxidizing adamantine with sulfuric acid, the reaction is carried out by keeping sulfuric concentration to 98.5-100 wt.% and retaining the reaction system for ≥10 hr at 30-40°C and raising the temperature of the reaction system to 45-55°C and retaining the temperature for ≥3 hr and further heating the reaction system to 60-90°C to produce the 2-adamantanone while suppressing production of tar content as by-product. COPYRIGHT: (C)2003,JPO

16. 发明专利

JP2003183204A METHOD FOR PRODUCING ADAMANTANOLS 审中-公开
公开(公告)号：JP2003183204A
公开(公告)日：2003-07-03
申请号：JP2001390041
申请日：2001-12-21
申请人： TOKUYAMA CORP
发明人： TANAKA KENJI , YAMAGUCHI MASAO
IPC分类号： C07C29/48 , C07C35/37 , C07C45/29 , C07C49/453 , C07C67/08 , C07C67/14 , C07C69/54
摘要： PROBLEM TO BE SOLVED: To realize a method for producing an adamantanol from adamantanes in a high yield and high selectivity by an industrially advantageous method. SOLUTION: This method for producing adamantanols comprises reacting adamantanes such as adamantine in a reaction solution comprising a concentrated sulfuric acid, a carbocation-producing compound such as tertiary butyl alcohol and an organic nitrile compound such as acetonitrile and mixing the resultant reaction solution with water at 20-90°C, preferably in such water amount used that sulfuric acid concentration after mixing with the reaction solution becomes 30-60 wt.%. COPYRIGHT: (C)2003,JPO

18. 发明专利

JP2001131105A METHOD FOR PRODUCING AND SEPARATING ALICYCLIC ALCOHOLS 失效
公开(公告)号：JP2001131105A
公开(公告)日：2001-05-15
申请号：JP31445599
申请日：1999-11-04
申请人： DAICEL CHEM
发明人： CHIKAMORI MASAHIRO , NOGUCHI TAKUYA , KATAOKA TAKESHI
IPC分类号： C07C29/78 , C07B61/00 , C07C29/50 , C07C29/86 , C07C35/37 , C07C45/29 , C07C49/453
摘要： PROBLEM TO BE SOLVED: To efficiently separate an alicyclic monool and/or a alicyclic diol from a mixture containing at least the alicyclic monool and the alicyclic diol. SOLUTION: This method for separating the alicyclic alcohol is a method for separating the monodiol and the diol from the mixture containing at least the alicyclic monodol and the alicyclic diol. The method comprises (b) an alicyclic monool crystallization process for subjecting the mixture to a crystallization operation using an aqueous solvent containing at least water to crystallize the alicyclic monool, (c) an extraction process for extracting a residual liquid from which the alicyclic monool is recovered with a mixed solvent of a >=3C alcohol and an alicyclic hydrocarbon and partitioning the alicyclic diol into an organic solvent layer. Further the method may include (d) an alicyclic monool cleaning process for cleaning a crystal obtained by the alicyclic monool crystallization process with an aqueous solution of an alkali.

19. 发明专利

JPH10309469A CATALYST FOR OXO-SYNTHESIS AND PRODUCTION OF KETONE OR THE LIKE BY USING THE SAME 失效
公开(公告)号：JPH10309469A
公开(公告)日：1998-11-24
申请号：JP12252797
申请日：1997-05-13
申请人： DAICEL CHEM , ISHII YASUTAKA
发明人： ISHII YASUTAKA , NAKANO TATSUYA
IPC分类号： C07D207/46 , B01J31/02 , B01J31/22 , B01J31/34 , B01J31/36 , C07B61/00 , C07C29/50 , C07C45/28 , C07C45/33 , C07C45/34 , C07C45/36 , C07C49/04 , C07C49/417 , C07C49/453 , C07D209/48 , C07D209/76
摘要： PROBLEM TO BE SOLVED: To efficiently subject a substrate to oxo-synthesis. SOLUTION: A substrate is subjected to oxo-synthesis with high conversion and selectivity by bringing the substrate into contact with oxygen in the existence of imide compound (N-hydroxyphthalimide or the like) and strong acid or this imide compound, strong acid and a co-catalyst (transition-metal compound or the like). In the formula, R and R denote hydrogen atom, halogen atom, alkyl group, aryl group and cycloalkyl group. R and R are mutually combined and double bond, aromatic or nonaromatic ring may be formed. X denotes O or OH and (n) denotes 1-3. The substrate contains a compound of at least one kind which is selected from among (a) a compound having methyl group or methylene group in the site adjacent to an unsaturated bond, (b) an allotropic or hetrocyclic compound having methylene group, (c) a compound having methine carbon atom, (d) a compound having methyl group or methylene group in the site adjacent to an aromatic ring and (e) a compound having methyl group or methylene group in the site adjacent to carbonyl group.

20. 发明专利

JPH0774168B2 失效
公开(公告)号：JPH0774168B2
公开(公告)日：1995-08-09
申请号：JP8443186
申请日：1986-04-14
IPC分类号： C07D207/46 , B01J31/00 , B01J31/02 , C07B31/00 , C07B41/00 , C07B41/02 , C07B41/06 , C07B61/00 , C07C27/00 , C07C29/132 , C07C29/48 , C07C29/50 , C07C33/02 , C07C45/00 , C07C45/34 , C07C45/53 , C07C49/453 , C07C49/603 , C07C49/613 , C07C49/627 , C07C49/653 , C07C67/00 , C07C407/00 , C07C409/04 , C07C409/14 , C07D209/48 , C07D209/66 , C07J9/00

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