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11. 发明专利

JPH05501861A 失效
公开(公告)号：JPH05501861A
公开(公告)日：1993-04-08
申请号：JP51026990
申请日：1990-06-21
IPC分类号： A61K8/55 , A61K8/06 , A61K8/14 , A61K8/49 , A61K8/58 , A61K8/92 , A61K9/00 , A61K9/127 , A61K31/675 , A61K47/24 , A61K49/00 , C07F9/09 , C07F9/10 , C07F9/14 , C07F9/24 , C07F9/6533

12. 发明专利

JPH03128388A FLUOROPHOSPHORIC ACID DIESTER AND ITS PRODUCTION 失效
公开(公告)号：JPH03128388A
公开(公告)日：1991-05-31
申请号：JP23118388
申请日：1988-09-13
申请人： OZAKI SHOICHIRO
发明人： WATANABE YUTAKA , HYODO NOBUYUKI , OZAKI SHOICHIRO
IPC分类号： C07F9/14
摘要： NEW MATERIAL:A compound expressed by the formula (R is aralkyl, alkyl or aryl). EXAMPLE:Dibenzyl fluorophosphate. USE:A reagent for di-substituted phosphorylation of various hydroxyl groups. PREPARATION:A phosphoric acid diester is reacted with a 2-fluoropyridinium salt or pyrophosphoric acid tetraester is reacted with cesium fluoride.

13. 发明专利

JPH0331292A (DI)(THIO)PHOSPHDRIC ACID CSULPHONIC ACID)(AMIDE)ESTERS 失效
公开(公告)号：JPH0331292A
公开(公告)日：1991-02-12
申请号：JP15007990
申请日：1990-06-11
申请人： BAYER AG
发明人： HERUBERUTO ZOMAA , DEIITAA ARURUTO , YURUGEN HARUTOBITSUHI
IPC分类号： A01N57/12 , A01N57/04 , A01N57/20 , A01N57/28 , A01N57/32 , C07F9/09 , C07F9/113 , C07F9/14 , C07F9/165 , C07F9/17 , C07F9/20 , C07F9/24 , C07F9/40 , C07F9/42 , C07F9/44 , C07F9/553 , C07F9/572 , C07F9/576

14. 发明专利

JPH0145476B2 失效
公开(公告)号：JPH0145476B2
公开(公告)日：1989-10-03
申请号：JP14111681
申请日：1981-09-09
申请人： HOECHST AG
发明人： YURUGEN GUROOSE
IPC分类号： C01B25/10 , C07F9/12 , C07F9/14 , C07F9/143 , C07F9/20 , C07F9/206 , C07F9/34 , C07F9/42 , C07F9/53 , C07F9/6574

15. 发明专利

JPS62155287A PRODUCTION OF ALPHA-DIHYDROPOLYPRENYL DICHLOROPHOSPHATE 失效
公开(公告)号：JPS62155287A
公开(公告)日：1987-07-10
申请号：JP29794185
申请日：1985-12-27
申请人： KURARAY CO
发明人： NAKAGAWA SUNAO , TAKIGAWA TETSUO , KAGEYU AKIRA , SHIMAMURA MICHIYA , OKADA MASAFUMI , MIZUNO MASAO
IPC分类号： C07F9/14 , B01J31/02 , C07B61/00
摘要： PURPOSE:To obtain the titled compound useful as a rate determining factor for synthesis of glycoprotein, ameliorant of hepatic function, anti-inflammatory agent, immunological enhancer, etc., in high yield, by reacting alpha- dihydropolyprenol with phosphorus oxychloride in an ether based solvent in the presence of a basic compound. CONSTITUTION:alpha-Dihydropolyprenol expressed by formula I (m is 4-22) is reacted with preferably 2-10mol equivalents, based on the compound expressed by formula I, phosphorus oxychloride in the presence of preferably 1.5-5mol equivalents, based on the compound expressed by formula I, basic compound, preferably triethylamine or pyridine in an ether based solvent, preferably THF, 1,2-dimethoxyethane or diethyl ether to afford the aimed compound expressed by formula II.

16. 发明专利

JPS6270381A METHOD OF SYNTHESIZING PHOSPHORIC ACID MONOALKYL ESTER DIHALIDE 失效
公开(公告)号：JPS6270381A
公开(公告)日：1987-03-31
申请号：JP21083485
申请日：1985-09-24
申请人： MITSUBISHI KASEI VINYL
发明人： HASEGAWA RYUICHI , ASANO HIROKI
IPC分类号： C07F9/14
摘要： PURPOSE:In reacting a phosphorus oxyhalide with an alkyl alcohol, to obtain the titled compound in a short time without requiring cooling, by using a specific solvent slightly dissolving an evolved hydrogen halide. CONSTITUTION:A phosphorus oxyhalide is reacted with an alkyl alcohol prefer ably in equimolar amounts in the presence of a solvent slightly dissolving hydro gen halides preferably under reduced pressure without cooling, to give the aimed compound. The reaction temperature is preferably 20-50 deg.C. An aromatic com pound such as benzene, xylene, etc., aliphatic hydrocarbon such as octane, dodecane, etc.,, halogenated compound such as trichloroethane, etc., are effective as the solvent and an amount of it used is preferably 50-200wt% based on the phosphorus oxyhalide. The aimed compound is useful as a raw material for an alkylaryl phosphate useful as a plasticizer for vinyl chloride resin.

17. 发明专利

JPS6248657A ANTIINFLAMMATORY AND NALGESIC COMPOUND AND COMPOSITION 失效
公开(公告)号：JPS6248657A
公开(公告)日：1987-03-03
申请号：JP13292386
申请日：1986-06-10
申请人： PROCTER & GAMBLE
发明人： ERIZABESU EFU BAAMAN , BURAIAN RII BATSUKUUORUTAA , TOMASU RII KATSUPUSU , JIYOSEFU HAAMAN GAADONAA
IPC分类号： C07F9/14 , A61K31/165 , A61K31/215 , A61K31/66 , A61P25/04 , A61P29/00 , C07C67/00 , C07C231/00 , C07C235/34 , C07C301/00 , C07C305/24 , C07C325/00 , C07C327/40 , C07C327/44 , C07F9/12

18. 发明专利

JPS6185453A Production of flame-retardant 失效
标题翻译：阻燃剂的生产
公开(公告)号：JPS6185453A
公开(公告)日：1986-05-01
申请号：JP20653884
申请日：1984-10-02
申请人： Hitachi Chem Co Ltd
发明人： NANAUMI KEN , YOSHIMURA YUKIO , KUMAKURA YOSHITOSHI
IPC分类号： C09K21/12 , C07F9/14 , C08K5/00 , C08K5/52 , C08L7/00 , C08L21/00 , C08L23/00 , C08L51/00 , C08L51/02 , C08L67/00 , C08L101/00
摘要： PURPOSE: To prepare a novel flame-retardant having improved heat resistance, containing phosphorus and bromine in a molecule, by reacting a phosphoric ester with a halogen-containing aromatic alcohol.
CONSTITUTION: (A) A phosphoric ester shown by the formula I (R
1 WR
3 are alkyl, or aryl such as triphenyl phosphate containing preferably an aromatic group and (B) a halogen-containing aromatic alcohol, preferably 2,4,6- tribromophenyl-β-hydroxyethyl ether shown by the formula II or formula III (R and R' are H, or alkyl; X and X' are bromine or chlorine; m+n=5; Y is group shown by the formula IV or formula V; q and n are 1W10) in a ratio of the component A/B of 1/0.1W1/2 are subjected to ester exchange reaction in the presence of 0.1W5wt% basic catalyst (base on total amounts of the components A and B) in the absence of a solvent under heating at 130W170°C, to give the aimed flame-retardant.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过使磷酸酯与含卤素的芳族醇反应，制备分子中含有磷和溴的耐热性提高的新型阻燃剂。（A）由式I表示的磷酸酯（R1-R3是烷基或芳基，例如优选芳基的三苯基磷酸酯和（B）含卤素的芳族醇，优选2,4,6-三溴苯基（R和R'为H或烷基; X和X'为溴或氯; m + n = 5; Y为式IV或式V所示的基团） ; q和n为1-10），组分A / B为1 / 0.1-1 / 2的比例在0.1-5wt％碱性催化剂存在下进行酯交换反应（基于组分总量 A和B）在130-170℃加热下不溶于溶剂，得到目标阻燃剂。

19. 发明专利

JPS56501092A 失效
公开(公告)号：JPS56501092A
公开(公告)日：1981-08-06
申请号：JP50210580
申请日：1980-08-28
IPC分类号： C08G65/00 , C07F9/09 , C07F9/14 , C07F9/165 , C07F9/20 , C07K14/555 , C08G65/32 , C08G65/335 , C08G65/336 , C08G65/337

20. 发明专利

JPS55130988A MANUFACTURE OF PHOSPHORIC ACID ALKYLESTER DICHLORIDE 失效
公开(公告)号：JPS55130988A
公开(公告)日：1980-10-11
申请号：JP3487580
申请日：1980-03-21
申请人： BAYER AG
发明人： KARURUUYUURIUSU SHIYUMITSUTO , FURIIDORITSUHI SHIYUMITSUTO , PEETAA JIIGURE , GERUTOOHANZEN
IPC分类号： C07F9/12 , C07F9/14

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