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11. 发明专利

JPH01128993A METHYL-4,6-0-(7-HYDROXY-3,7-DIMETHYL)OCTYLIDENE-D-GLYCOSIDE 失效
公开(公告)号：JPH01128993A
公开(公告)日：1989-05-22
申请号：JP28707387
申请日：1987-11-12
申请人： KANEBO LTD
发明人： IKEMOTO TAKESHI , KOMAKI RYOICHI , KUWAORI TOMIYA , FUJITA AKIRA
IPC分类号： C11B9/00 , A23L27/20 , A61K8/00 , A61Q13/00 , C07H9/04
摘要： NEW MATERIAL:A compound of formula I (the wave lines represent axial or equatorial bonds). EXAMPLE:Methyl-4,6-0-(7-hydroxy-3,7-dimethyl)octylidene-alpha,B-glucop yranoside. USE:Flavor-maintaining agent. PREPARATION:A methyl-D-glycoside of formula II is allowed to react with hydroxycitroneral dimethyl acetal of formula III in an organic solvent such as DMF or dichloroethane in the presence of an acid such as p-toluenesulfonic acid, or sulfuric acid, preferably at a molar ratio of 1:(0.5-2), for example, at 40-150 deg.C for 1-6 hours.

12. 发明专利

JPS6284194A PRODUCTION OF IRANIAN OIL EXCELLENT IN FLAVOR AND LOW IN SENSITIVITY 失效
公开(公告)号：JPS6284194A
公开(公告)日：1987-04-17
申请号：JP22534185
申请日：1985-10-08
申请人： KANEBO LTD
发明人： IKEMOTO TAKESHI , KAKISHIMA HIROSHI , KUWAORI TOMIYA , INUI MASAYOSHI
IPC分类号： C11B9/02 , A61K8/00 , A61Q13/00 , C11B9/00

13. 发明专利

JPS60260509A PERFUME CONDITIONER 失效
公开(公告)号：JPS60260509A
公开(公告)日：1985-12-23
申请号：JP11716284
申请日：1984-06-06
申请人： KANEBO LTD
发明人： KOMAKI RIYOUICHI , IKEMOTO TAKESHI , KUWAORI TOMIYA
IPC分类号： A61K8/00 , A61Q13/00 , C11B9/00
摘要： PURPOSE:A perfume conditioner that contains, as an effective component, a specific diethylene glycol diether, thus developing both actions of perfume retention and solubilization with chemical stability and safety to skins. CONSTITUTION:At least one selected from diethylene glycol diether of formula I, formula II (C5H9O4 is residue of pentose; C6H11O5 is hexose residue; R is 1-6C alkyl) is used as a perfume conditioner. It has been found that the compounds of formulas I and II are colorless, odorless and clear liquid with chemical stability. Further, they are safe to skins and improve aromatic and solubilizing properties of perfumes.

14. 发明专利

JPH03106997A PERFUME COMPOSITION FOR SPRAYING IN ROOM 失效
公开(公告)号：JPH03106997A
公开(公告)日：1991-05-07
申请号：JP24606089
申请日：1989-09-20
申请人： KANEBO LTD
发明人： YAMASHITA YOSHIKUNI , KUWAORI TOMIYA , IKEMOTO TAKESHI
IPC分类号： A61L9/01 , C11B9/00
摘要： PURPOSE:To obtain the title composition which leaves no odor even after repeated use by spraying and always gives a fresh inherent aroma by using a low-boiling component of a perfume, prepared by a specified process, and a volatile solvent as the constituents. CONSTITUTION:The title composition consists of a low-boiling component of a perfume (e.g. lavender oil), obtained by distillation under a vacuum of 0.2-0.5mmHg at 30-110 deg.C, and a volatile solvent (e.g. a mixture of ethanol and water).

15. 发明专利

JPH02160717A BATHING AGENT 失效
公开(公告)号：JPH02160717A
公开(公告)日：1990-06-20
申请号：JP31703688
申请日：1988-12-14
申请人： KANEBO LTD
发明人： IKEMOTO TAKESHI , KUWAORI TOMIYA , ISHIDA TAKAO
IPC分类号： A61K8/00 , A61K8/60 , A61Q19/10
摘要： PURPOSE:To provide a bathing agent containing lower alkyl glycosides and having excellent skin-beautifying effect to impart the skin with smoothness, moist-feeling, etc. CONSTITUTION:The objective agent contains at least one kind of a lower alkyl glycoside (e.g. ethyl glucose, propyl glucose, butyl glucose or pentaglucose). The amount of the lower alkyl glycoside in the bathing agent is about 0.5-50%, preferably 3-25% and the agent may be used singly or in combination with other components. The agent may be incorporated with conventional bathing agent components such as NaCl, potassium nitrate, benzoic acid, citric acid, crude drugs or oil and fat.

16. 发明专利

JPH01238595A METHYL-4,6-0-ALKYLIDENE OR CYCLOHEXENYLIDENE-D-GLYCOSIDE 失效
公开(公告)号：JPH01238595A
公开(公告)日：1989-09-22
申请号：JP6671488
申请日：1988-03-18
申请人： KANEBO LTD
发明人： IKEMOTO TAKESHI , KOMAKI RYOICHI , KUWAORI TOMIYA
IPC分类号： C07H15/04 , A61K8/00 , A61Q13/00 , C11B9/00
摘要： NEW MATERIAL:A compound expressed by formula I (R is formula II or formu la III; wave line is axial or equatorial bond). EXAMPLE:Methyl-4,6-0-[4-hydroxy-4-methylpentan-1-yl) 3-cyclohexenylidene]-alpha-, D-glucopyranoside. USE:A retaining agent for compound perfume composition. PREPARATION:Methyl-D-glycoside expressed by formula IV is brought into contact with aldehydedimethylacetal expressed by formula V in an organic solvent (e.g., DMF or dichloroethane) in the presence of an acid (preferably p-toluenesulfonic acid, sulfuric acid or phosphoric acid), preferably of 0.1-5wt.%, preferably at 40-150 deg.C for 1-6hr.

17. 发明专利

JPH01139520A COSMETIC HAVING SUPPRESSED SKIN-IRRITATION 失效
公开(公告)号：JPH01139520A
公开(公告)日：1989-06-01
申请号：JP29711287
申请日：1987-11-24
申请人： KANEBO LTD
发明人： IKEMOTO TAKESHI , KUWAORI TOMIYA , KAKISHIMA HIROSHI , TOKUNAGA KAZUNOBU
IPC分类号： A61K8/00 , A61K8/60 , A61Q1/00 , A61Q1/12 , A61Q19/00
摘要： PURPOSE:To obtain a cosmetic having sufficiently suppressed skin irritation caused by perfume, by compounding a specific glycoside derivative to a perfume- containing cosmetic. CONSTITUTION:A perfume-containing cosmetic is compounded with >=0.05wt.%, preferably 0.05-5.0wt.% of a compound of formula (the wavy line is axial or equatorial bond; R is 5-11C alkyl or 5-11C alkenyl). The compound of formula is e.g., methyl-4,6-0-hexylidene-alpha- or beta-glycopyranoside and methyl-4,6-0- heptylided-alpha- or beta-D-glycopyranoside. The characterization and feeling to the skin can be sufficiently satisfied without reducing the compounding amount of perfumery nor deteriorating the commercial value and effect of the cosmetic.

18. 发明专利

JPS62265296A METHYL-4,6-O-PHENYLALKYLIDENE-ALPHA-D-GLYCOSIDE 失效
公开(公告)号：JPS62265296A
公开(公告)日：1987-11-18
申请号：JP10928186
申请日：1986-05-12
申请人： KANEBO LTD
发明人： KOMAKI RYOICHI , IKEMOTO TAKESHI , KUWAORI TOMIYA , FUJITA AKIRA
IPC分类号： C07H9/04 , C07H15/04 , C11B9/00
摘要： NEW MATERIAL:A compound expressed by formula I (wavy line represents axial or equatorial bond; n is 1 or 2). EXAMPLE:Methyl-4,6-O-beta-phenylethylidene-alpha-D-glucopyranoside. USE:A fixative for perfumes. PREPARATION:A methyl-alpha-D-glycoside expressed by formula II (example; methyl-alpha-D-glucopyranoside, etc.) is reacted with a phenylaldehyde dialkyl acetal expressed by formula III (R' represents lower alkyl) (example; phenylacetaldehyde dimethyl acetal, etc.) in an organic solvent such as DMF, etc., in the presence of an acid (preferably p-toluenesulfonic acid) preferably at 40-150 deg.C for 1-6hr.

19. 发明专利

JPS6183114A Perfume fixative 失效
标题翻译： PERFUME固定
公开(公告)号：JPS6183114A
公开(公告)日：1986-04-26
申请号：JP20434784
申请日：1984-09-28
申请人： Kanebo Ltd
发明人： KOMAKI RYOICHI , IKEMOTO TAKESHI , KUWAORI TOMIYA
IPC分类号： A61K8/33 , A61K8/00 , A61Q13/00 , C11B9/00
摘要： PURPOSE: The titled odorless and chemically stable fixative having high safety to the skin, showing high fixative effect on perfume in blending with perfume, comprising an ether compound derived from 5C or 6C saccharide.
CONSTITUTION: The titled fixative comprising 5W70wt.% ether compound shown by the formula I or formula II [C
5 H
l O
m (l is 6W9; m is 1W4) is 5C saccharide residue; C
6 H
x O
y (x is 7W11; y is 1W5) is 6C saccharide residue; R is 4W20C hydrocarbon residue; n is 1W4; z is 1W5] as an active ingredient. The ether compound is obtained by condensing a reaction product of 5C saccharide (e.g., xylose or arabinose0 or 6C saccharide (e.g., glucose or galactose) and sodium hydride with a compound obtained by brominating a hydroxyl group of 4W20C saturated or unsaturated monohydric alcohol.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：标准无臭，化学稳定的固定剂对皮肤的安全性高，对与香水混合的香料具有较高的固定效果，包括衍生自5C或6C糖的醚化合物。构成：包含5-70wt％由式I或式II表示的醚化合物的标题固定剂[C5H10m（I为6-9; m为1-4））为5℃糖残基; C6HxOy（x为7-11; y为1-5）为6C糖残基; R是4-20C烃残基; n为1-4; z为1-5]作为活性成分。醚化合物通过将5℃糖（例如，木糖或阿拉伯糖0或6C糖（例如葡萄糖或半乳糖）和氢化钠）的反应产物与通过溴化4-20℃饱和或不饱和一元醇的羟基获得的化合物。

20. 发明专利

JPS6163612A Adjusting agent for perfume 失效
标题翻译：调味剂
公开(公告)号：JPS6163612A
公开(公告)日：1986-04-01
申请号：JP18519584
申请日：1984-09-03
申请人： Kanebo Ltd
发明人： KOMAKI RYOICHI , IKEMOTO TAKESHI , KUWAORI TOMIYA
IPC分类号： A61K8/33 , A61K8/00 , A61Q13/00 , C11B9/00
摘要： PURPOSE: An adjusting agent for perfume, showing simultaneously effects as a fixative and a solubilizer alone, containing a specific diethylene glycol ether compound as an active ingredient to be added to perfume.
CONSTITUTION: Perfume is blended with at least one of diethylene glycol diether compounds shown by the formula I [group shown by the formula II (l is 6W8; m is 1W3) is 5C saccharide residue; R is 1W6C alkyl; n is 2W4] or formula III [group shown by the formula IV (x is 7W10; Y is 1W4) is 6C saccharide residue; z is 2W5] as an active ingredient. An amount of the compound contained as an active ingredient in perfume is 5W70wt% based on the total amounts of the composition. The compound is obtained by reacting 5C saccharide such as xylose, etc., or 6C saccharide such as glucose, galactose, etc. with a diethylene glycol monoalkyl ether whose OH group is brominated.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：用于香水的调节剂，同时显示作为固定剂和单独的增溶剂的作用，其含有特定的二甘醇醚化合物作为待添加到香料中的活性成分。构成：将香料与式I所示的二甘醇二醚化合物中的至少一种共混[式II所示的基团（I为6-8; m为1-3）为5个糖残基; R为1-6C烷基; n为2-4]或式Ⅲ[式IV所示基团（x为7-10; Y为1-4）为6C糖残基; z为2-5]作为活性成分。在香料中作为活性成分含有的化合物的量相对于组合物的总量为5-70重量％。该化合物通过使诸如木糖等的5C糖，或诸如葡萄糖，半乳糖等的6C糖与OH基被溴化的二甘醇单烷基醚反应而获得。

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