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1. 发明公开

EP4277887A1 REMOVAL OF SULFATE FROM MEG STREAMS USING CALCIUM CHLORIDE 审中-实审
公开(公告)号：EP4277887A1
公开(公告)日：2023-11-22
申请号：EP22740219.5
申请日：2022-01-18
申请人： Cameron Technologies Limited
发明人： MESSENGER, Brian Edward
IPC分类号： C07C29/94 , C07C29/76 , C07C31/20

2. 发明授权

EP3988529B1 A METHOD FOR THE PREPARATION OF 1,2-PROPANEDIOL 有权
公开(公告)号：EP3988529B1
公开(公告)日：2022-09-28
申请号：EP20203021.9
申请日：2020-10-21
发明人： WIEDERHOLD, Holger , BOLZ, David , GLATZ, Patrik
IPC分类号： C07C29/48 , C07C31/20 , C07C29/86 , C07C29/94

3. 发明公开

EP3774706A1 IMPROVED PROCESS FOR THE TRANSFORMATION OF PRIMARY ALIPHATIC ALCOHOLS INTO HIGHER ALIPHATIC ALCOHOLS 有权转让
公开(公告)号：EP3774706A1
公开(公告)日：2021-02-17
申请号：EP19714217.7
申请日：2019-04-04
申请人： Alma Mater Studiorum Universita di Bologna
发明人： CAVANI, Fabrizio , ZANOTTI, Valerio , MAZZONI, Rita , LUCARELLI, Carlo , CESARI, Cristiana , TABANELLI, Tommaso , PUZZO, Francesco
IPC分类号： C07C29/34 , C07C29/94

4. 发明公开

EP3511313A1 METHOD FOR PREPARING 1,3-CYCLOHEXANEDIMETHANOL 审中-公开
公开(公告)号：EP3511313A1
公开(公告)日：2019-07-17
申请号：EP17849059.5
申请日：2017-09-05
申请人： Lotte Chemical Corporation
发明人： CHA, Mi Sun , CHOI, Seong Hwan , KIM, Sung Min , PARK, Sung Joon , YUN, Chan Yeong , CHOI, Young Heon
IPC分类号： C07C29/94 , C07C29/17 , C07C35/14 , B01J23/62 , B01J23/46
摘要： The present invention relates to a method for preparing high-purity 1,3-cyclohexanedimethanol capable of achieving a high conversion rate by allowing most of the reactant to participate in the reaction, and of increasing reaction efficiency and economic efficiency by further simplifying the reaction process, while minimizing by-products within a shorter period of time.
Specifically, the method for preparing 1,3-cyclohexanedimethanol includes reducing 1,3-cyclohexanedicarboxylic acid in the presence of a metal catalyst, which is fixed to a silica support and includes a ruthenium (Ru) compound, a tin (Sn) compound and a platinum (Pt) compound in a weight ratio of 1:0.8 to 1.2:1.2 to 2.4.

6. 发明公开

EP3187481A4 METHOD FOR PREPARING NEOPENTYL GLYCOL AT HIGH EFFICIENCY AND APPARATUS FOR PREPARING SAME 有权
公开(公告)号：EP3187481A4
公开(公告)日：2018-04-25
申请号：EP15820424
申请日：2015-09-15
申请人： LG CHEMICAL LTD
发明人： EOM SUNG SHIK , KO DONG HYUN , KIM MI YOUNG , JUNG DA WON , KIM TAE YUN , CHOI MIN JI
IPC分类号： C07C29/141 , B01J21/08 , B01J23/78 , C07C29/94 , C07C31/20
CPC分类号： C07C29/141 , B01J19/24 , B01J21/08 , B01J23/78 , B01J2219/00103 , C07C31/20
摘要： Disclosed are a highly efficient neopentyl glycol preparation method and a device therefor. More particularly, disclosed are a method of preparing neopentyl glycol, wherein the method includes adding a hydroxypivaldehyde solution and hydrogen to a hydrogenation reactor that including a hydrogenation catalyst, wherein the hydroxypivaldehyde solution includes 6 to 30 % by weight of hydroxypivaldehyde, 35 to 70 % by weight of neopentyl glycol, 10 to 30 % by weight of alcohol, and 10 to 30 % by weight of water, and a device therefor. According to the present disclosure, a neopentyl glycol preparation method wherein separate heating is not required in a section of a feed vessel to an inlet of a hydrogenation reactor unlike conventional technologies to save energy, and, at the same time, by-products with a high boiling point are not generated in the section to prevent poisoning of a hydrogenation catalyst in a reactor due to the by-products with a high boiling point and increase a hydrogenation yield, and a device therefor can be provided.

7. 发明公开

EP2736870A2 CATALYTIC PROCESS FOR CONTINUOUSLY GENERATING POLYOLS 审中-公开
标题翻译：催化方法用于多元醇的连续生产
公开(公告)号：EP2736870A2
公开(公告)日：2014-06-04
申请号：EP12817278.0
申请日：2012-07-11
申请人： UOP LLC
发明人： KALNES, Tom, N. , CHEN, John, Q. , KOCAL, Joseph, A.
IPC分类号： C07C29/94 , C07C31/26 , C07C31/18 , B01J23/42 , B01J23/46
CPC分类号： C07C29/132 , C10G3/44 , C10G3/46 , C10G3/48 , C10G3/52 , C10G3/56 , C10G2300/1014 , Y02P20/52 , Y02P30/20 , C07C31/202 , C07C31/205
摘要： A catalytic process for generating at least one polyol from a feedstock comprising cellulose is performed in a continuous manner. The process involves, contacting, continuously, hydrogen, water, and a feedstock comprising cellulose, with a catalyst to generate an effluent stream comprising at least one polyol, water, hydrogen, and at least one co-product. The water, hydrogen, and at least one co-product are separated from the effluent stream and recycled to the reaction zone. The polyol is recovered from the effluent stream.

8. 发明公开

EP2483225A1 PROCESS FOR THE PURIFICATION OF CRUDE ALKALINE GLYCEROL 审中-公开
标题翻译：一种用于净化Rohalkalinglycerol过程
公开(公告)号：EP2483225A1
公开(公告)日：2012-08-08
申请号：EP10768554.7
申请日：2010-09-29
申请人： Rhodia Poliamida E Especialidades Ltda
发明人： LOURENCO, Wagner, Célio, Ferraz , MACRET, Richard , CIELO, José, Eduardo
IPC分类号： C07C29/94
CPC分类号： C07C29/88 , C07C31/225
摘要： The present invention generally concerns a treatment process for crude alkaline glycerol obtained as a by-product of transesterification reaction of natural oils and fats with lower alcohols. The present invention particularly concerns the treatment of crude alkaline glycerol obtained as a by-product of the biodiesel production from vegetable oils and animal fats using organic alkyl carboxylic acids or their aqueous solution, comprising the steps of: (a) acidification of the crude alkaline glycerol stock to pH in the range of about 4 to about 6, particularly 4 to 5, with organic alkyl carboxylic acids, in the presence of water in the range from about 5% to about 50%, particularly 15 to 30%, in weight with respect to the weight of the crude alkaline glycerol stock; (b) separating the formed free fatty acids, for instance by flotation; (c) removing the alcohol present in the acidified crude glycerol stock, for instance by distillation; (d) separating the acidic glycerol.

9. 发明公开

EP2454222A2 RECOVERY OF BUTANOL FROM A MIXTURE OF BUTANOL, WATER AND AN ORGANIC EXTRACTANT 审中-公开
标题翻译：从丁醇，水和有机萃取剂的混合物中回收丁醇
公开(公告)号：EP2454222A2
公开(公告)日：2012-05-23
申请号：EP10734422.8
申请日：2010-07-15
申请人： Butamax(tm) Advanced Biofuels LLC
发明人： XU, Yihui, Tom , PARTEN, William, D.
IPC分类号： C07C29/80 , C07C29/86 , C07C29/94 , C07C31/12 , C12P7/16
CPC分类号： B01D3/002 , B01D3/143 , C07C29/84 , C07C31/12
摘要： A process for recovering butanol from a mixture comprising a water-immiscible organic extractant, water, butanol, and optionally a non-condensable gas, is provided. The butanol is selected from 1-butanol, isobutanol, and mixtures thereof. An overhead stream from a first distillation column is decanted into two liquid phases. The wet butanol phase is refined in a second distillation column; the aqueous phase is returned to the first distillation column. A portion of the wet butanol phase from the decanter is also returned to the first distillation column. The extractant comprises at least one solvent selected from the group consisting of C
7 to C
22 fatty alcohols, C
7 to C
22 fatty acids, esters of C
7 to C
22 fatty acids, C
7 to C
22 fatty aldehydes, and mixtures thereof.
摘要翻译：提供了从包含与水不混溶的有机萃取剂，水，丁醇和任选的不可冷凝气体的混合物中回收丁醇的方法。丁醇选自1-丁醇，异丁醇及其混合物。将来自第一蒸馏塔的顶部物流倾析成两个液相。湿丁醇相在第二蒸馏塔中精制; 水相返回第一蒸馏塔。来自滗析器的一部分湿丁醇相也返回第一蒸馏塔。萃取剂包含至少一种选自C 7至C 22脂肪醇，C 7至C 22脂肪酸，C 7至C 22脂肪酸酯，C 7至C 22脂肪醛及其混合物的溶剂。

10. 发明公开

EP2308818A1 Process for the purification of crude alkaline glycerol 审中-公开
标题翻译： Verfahren zur Reinigung von Rohalkalinglycerol
公开(公告)号：EP2308818A1
公开(公告)日：2011-04-13
申请号：EP09171811.4
申请日：2009-09-30
申请人： Rhodia Poliamida E Especialidades Ltda
发明人： Lourenco, Wagner, Celio, Ferraz , Macret, Richard , Cielo, Jose, Eduardo
IPC分类号： C07C29/94
CPC分类号： C07C29/88 , C07C31/225
摘要： The present invention generally concerns a treatment process for crude alkaline glycerol obtained as a by-product of transesterification reaction of natural oils and fats with lower alcohols. The present invention particularly concerns the treatment of crude alkaline glycerol obtained as a by-product of the biodiesel production from vegetable oils and animal fats using organic alkyl carboxylic acids or their aqueous solution, comprising the steps of:
(a) acidification of the crude alkaline glycerol stock to pH in the range of about 4 to about 6, particularly 4 to 5, with organic alkyl carboxylic acids, in the presence of water in the range from about 5% to about 50%, particularly 15 to 30%, in weight with respect to the weight of the crude alkaline glycerol stock;
(b) separating the formed free fatty acids, for instance by flotation;
(c) removing the alcohol present in the acidified crude glycerol stock, for instance by distillation;
(d) separating the acidic glycerol.
摘要翻译：本发明一般涉及作为天然油和脂肪与低级醇的酯交换反应的副产物获得的粗碱性甘油的处理方法。本发明特别涉及使用有机烷基羧酸或其水溶液处理作为来自植物油和动物脂肪的生物柴油生产的副产物的粗碱性甘油，其包括以下步骤：（a）粗碱化甘油储备液在有机烷基羧酸的约4至约6，特别是4至5的范围内，在约5％至约50％，特别是15至30％重量的水存在下相对于粗碱性甘油原料的重量; （b）分离形成的游离脂肪酸，例如通过浮选; （c）例如通过蒸馏除去存在于酸化粗甘油原料中的醇; （d）分离酸性甘油。

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