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1. 发明公开

EP2894145A1 METHOD FOR PRODUCING UNSATURATED ACID AND/OR UNSATURATED ACID ESTER 审中-公开
标题翻译：方法用于生产不饱和酸和/或不饱和酸酯
公开(公告)号：EP2894145A1
公开(公告)日：2015-07-15
申请号：EP13835065.7
申请日：2013-08-30
申请人： Asahi Glass Company, Limited
发明人： FUJITA, Tomoyuki , WADA, Shinji , OKAZOE, Takashi , MURATA, Koichi
IPC分类号： C07C51/093 , C07C51/377 , C07C53/19 , C07C57/04 , C07C67/00 , C07C67/317 , C07C69/63 , C07C69/653 , C07B61/00
CPC分类号： C07C67/317 , C07C51/093 , C07C51/377 , C07C67/00 , C07C67/40 , C07C53/19 , C07C69/63 , C07C69/653
摘要： The present invention relates to a method for producing an unsaturated acid and/or an unsaturated acid ester, containing a process A of reacting a compound (1) represented by the following formula (1) at a temperature of 0°C to 350°C in the presence of a Brønsted acid catalyst and/or a Lewis acid catalyst, to prepare a compound (2) represented by the following formula (2);

in which each of R 1 , R 2 and R 4 independently represents a hydrogen atom, a deuterium atom or an alkyl group; each of R 3 and R 5 independently represents a hydrogen atom or a deuterium atom; R 6 represents a hydrogen atom, a deuterium atom, or an alkyl group or an aryl group; and X represents a chlorine atom, a fluorine atom, a bromine atom, or an iodine atom.
摘要翻译：本发明涉及一种用于在不饱和酸和/或在不饱和羧酸酯的制造，含有使（1）由下式表示的化合物的方法A（1），在0℃至350℃的温度下在布朗斯台德酸催化剂和/或路易斯酸催化剂的存在下，以制备化合物（2）由下式表示（2）; 其在每一种，R 1，R 2和R 4独立地darstellt氢原子，氘原子或烷基; 每个R 3和R 5unabhängigdarstellt氢原子或氘原子的; R 6表示氢原子，氘原子，或烷基或芳基的; X表示氯原子，氟原子，溴原子，或碘原子上。

2. 发明公开

EP2576486A4 CARBOCATALYSTS FOR CHEMICAL TRANSFORMATIONS 审中-公开
标题翻译：卡博催化剂上的化学转化
公开(公告)号：EP2576486A4
公开(公告)日：2014-01-01
申请号：EP11787494
申请日：2011-05-27
申请人： GRAPHEA INC
发明人： BIELAWSKI CHRISTOPHER W , DREYER DANIEL R , JIA HONG-PENG
IPC分类号： C07B41/00 , B01J21/18 , C07C29/09 , C07C45/42 , C07C51/093
CPC分类号： B01J31/04 , B01J8/067 , B01J8/382 , B01J19/00 , B01J21/18 , B01J21/185 , B01J35/002 , B01J35/023 , B01J37/12 , B01J37/349 , B01J2208/00176 , B01J2208/00212 , B01J2219/00006 , B01J2219/00031 , B01J2219/00033 , B01J2219/00038 , B82Y30/00 , B82Y40/00 , C01B32/194 , C01B32/23 , C07C45/28 , C07C45/29 , C07C45/30 , C07C201/12 , C07C315/02 , C07C319/24 , C07D333/22

3. 发明公开

EP2576486A2 CARBOCATALYSTS FOR CHEMICAL TRANSFORMATIONS 审中-公开
标题翻译：卡博催化剂上的化学转化
公开(公告)号：EP2576486A2
公开(公告)日：2013-04-10
申请号：EP11787494.1
申请日：2011-05-27
申请人： Graphea, Inc.
发明人： BIELAWSKI, Christopher W. , DREYER, Daniel R. , JIA, Hong-Peng
IPC分类号： C07B41/00 , B01J21/18 , C07C45/42 , C07C51/093 , C07C29/09
CPC分类号： B01J31/04 , B01J8/067 , B01J8/382 , B01J19/00 , B01J21/18 , B01J21/185 , B01J35/002 , B01J35/023 , B01J37/12 , B01J37/349 , B01J2208/00176 , B01J2208/00212 , B01J2219/00006 , B01J2219/00031 , B01J2219/00033 , B01J2219/00038 , B82Y30/00 , B82Y40/00 , C01B32/194 , C01B32/23 , C07C45/28 , C07C45/29 , C07C45/30 , C07C201/12 , C07C315/02 , C07C319/24 , C07D333/22
摘要： The disclosure relates to catalytically active carbocatalysts, e.g., a graphene oxide or graphite oxide catalyst suitable for use in a variety of chemical transformations. In one embodiment, it relates to a method of catalyzing a chemical reaction of an organic molecule by reacting the organic molecule in the presence of a sufficient amount of graphene oxide or graphite oxide for a time and at a temperature sufficient to allow catalysis of a chemical reaction. According to other embodiments, the reaction may be an oxidation reaction, a hydration reaction, a dehydrogenation reaction, a condensation reaction, or a polymerization reaction. Some reactions may include auto-tandem reactions. The disclosure further provides reaction mixtures containing an organic molecule and graphene oxide or graphite oxide in an amount sufficient to catalyze a reaction of the organic molecule.

4. 发明公开

EP2736865A1 METHOD FOR HYDROLYZING ALPHA - CHLORINATED TOLUENE COMPOUNDS 审中-公开
标题翻译： METHOD FOR水解ALPHA-氯化甲苯化合物的
公开(公告)号：EP2736865A1
公开(公告)日：2014-06-04
申请号：EP11746509.6
申请日：2011-07-26
申请人： INEOS ChloroToluenes Limited.
发明人： VAN DEYNSE, Dirk , VAN AKEN, Koen , VAN HECKE, Wouter
IPC分类号： C07C29/124 , C07C33/22 , C07C45/43 , C07C47/54 , C07C51/093 , C07C63/06
CPC分类号： C07C37/02 , C07C29/124 , C07C33/22
摘要： The current invention provides and improved method for hydrolyzing alpha- chlorinated toluene compounds comprising the steps of: -providing an alpha-chlorinated toluene compound of formula (I) wherein at least one of R
1 , R
2 and R
3 is CI and wherein (R
a )
n designates that the benzene nucleus may have one or more substituents which may be same or different and are selected from the group consisting of H, CI, Br and - C
m H
2m+1 , n being 0 or an integer from 1 to 5, and m being an integer, preferably from 1 to 6, -hydrolyzing said compound with water in the presence of a metal oxide.

5. 发明公开

EP2258675A2 Fluorinated surfactants for making fluoropolymers 无效
标题翻译： Fluorinierte Tenside zur Herstellung von Fluorpolymeren
公开(公告)号：EP2258675A2
公开(公告)日：2010-12-08
申请号：EP10177030.3
申请日：2006-12-19
申请人： 3M Innovative Properties Company
发明人： Hintzer, Klaus , Juergens, Michael , Kaspar, Harald , Maurer, Andreas , Schwertfeger, Werner , Zipplies, Tilmann , Koenigsmann, Herbert
IPC分类号： C07C51/093 , C07C59/135 , B01F17/44
CPC分类号： C08F214/262 , B01F17/0035 , C07C51/41 , C07C59/135 , C08F2400/00 , C08F2500/24 , C08L71/02 , C09D127/12 , C08L2666/22
摘要： The invention provides a fluorinated surfactant having the general formula:

[R f -(O) t -CHF-(CF 2 ) n -COO-] i X i+ (I)

wherein R f represents a partially or fully fluorinated aliphatic group optionally interrupted with one or more oxygen atoms, t is 0 or 1 and n is 0 or 1, X i+ represents a cation having a valence i and i is 1, 2 or 3. The surfactant can be used in emulsion polymerization of fluoromonomers to prepare fluoropolymers.
摘要翻译：本发明提供了具有以下通式的氟化表面活性剂：ƒ€ƒ€ƒ€ƒ€ƒ€ƒ[R f - （O）t -CHF-（CF 2）n -COO-] i X i + ƒ€ƒ€ƒ€ƒ（I）其中R f表示任选被一个或多个氧原子间断的部分或完全氟化的脂族基团，t为0或1，n为0或1，X i +为阳离子其价态i和i为1,2或3.表面活性剂可用于含氟单体的乳液聚合以制备含氟聚合物。

6. 发明公开

EP1754697A1 Preparation of carboxylic acids 审中-公开
标题翻译： Verfahren zur Herstellung vonCarbonsäuren
公开(公告)号：EP1754697A1
公开(公告)日：2007-02-21
申请号：EP05017930.8
申请日：2005-08-18
申请人： Solvay S.A.
发明人： Mathieu, Veronique , Buyle, Olivier , Janssens, Francine
IPC分类号： C07C51/093 , C07C53/21 , C07C53/15
CPC分类号： C07C51/093 , C07C53/21 , C07C53/15
摘要： Carboxylic acids can be prepared by reacting compounds comprising a -CCl 2 F group, a CCIF 2 group or a CCl 3 group with sulfur trioxide and sulfuric acid. The reaction is especially suitable for the preparation of 3,3,3-trifluoropropionic acid from CF 3 -CH 2 -CCl 2 F, CF 3 -CH 2 -CCIF 2 , CF 3 -CH 2 -CCl 3 or a mixture of one or two thereof as starting material. Usually, oleum is used as the source for sulfur trioxide.
In a preferred embodiment, the starting material comprises CF 3 -CH 2 -CCl 2 F and/or CF 3 -CH 2 -CCIF 2 which is or are prepared in a fluorination reaction between CCl 3 -CH 2 -CCl 3 and HF. As a source for CCl 3 -CH 2 -CCl 2 , the product of the reaction between CH 2 =CCl 2 and CCl 4 is advantageously used.
摘要翻译：羧酸可以通过使包含-CCl 2 F基团，CCIF 2基团或CCl 3基团的化合物与三氧化硫和硫酸反应来制备。该反应特别适用于由CF 3 -CH 2 -CCl 2 F，CF 3 -CH 2 -CCIF 2，CF 3 -CH 2 -CCl 3或其混合物制备3,3,3-三氟丙酸或其两个作为起始材料。通常，使用发烟硫酸作为三氧化硫的来源。在优选的实施方案中，原料包含在CCl 3 -CH 2 -CCl 3和HF之间的氟化反应中制备的或CF 3 -CH 2 -CCl 2 F和/或CF 3 -CH 2 -CClF 2。作为CCl 3 -CH 2 -CCl 2的来源，有利地使用CH 2 = CCl 2和CCl 4之间的反应的产物。

7. 发明公开

EP0607824A2 Verfahren zur Herstellung mehrfach halogenierter Benzotrifluoride, Benzotrichloride und Benzoylchloride sowie neue Trihalogenbenzotrichloride und -benzoylchloride 失效
标题翻译：一种用于制备多卤代benzotrifluorides，benzotrichlorides和苯甲酰基和新Trihalogenbenzotrichloride和-benzoylchloride过程。
公开(公告)号：EP0607824A2
公开(公告)日：1994-07-27
申请号：EP94100203.2
申请日：1994-01-07
申请人： BAYER AG
发明人： Marhold, Albrecht, Dr. , Andres, Peter, Dr.
IPC分类号： C07C17/20 , C07C51/58 , C07C63/10 , C07C25/13 , C07C63/70 , C07C51/093
CPC分类号： C07C17/32 , A23K20/195 , B01J27/10 , B01J27/12 , B01J27/128 , C07C17/12 , C07C17/208 , C07C25/13 , C07C51/58 , C07C63/70
摘要： Mehrfach halogenierte Benzotrifluoride lassen sich mit Chloriden aus der Reihe der Friedel-Crafts-Katalysatoren zu den entsprechenden Benzotrichloriden umsetzen, die durch Wasser in Gegenwart von Eisen(III)-chlorid zu den entsprechenden Benzoylchloriden hydrolysiert werden können. Diese sind als Zwischenprodukte für die Herstellung von Wirkstoffen für Arzneimittel und Futterzusatzstoffe geeignet.
摘要翻译：乘卤代benzotrifluorides可以用来自Friedel-Crafts催化剂系列氯化物进行反应，得到相应的benzotrichlorides，这可以通过在水的铁的存在（III）氯化物，得到相应的苯甲酰氯水解。这些适合作为中间体，用于生产用于药物，饲料添加剂活性化合物。

8. 发明授权

EP0011288B1 p-tert.-Butylbenzotribromid und deren am Kern durch Halogen substituierte Derivate, Verfahren zu ihrer Herstellung sowie ihrer Verwendung 失效
标题翻译： P-TERT.-丁氧基苯并二恶英及其衍生物，其由卤素取代在环中，其制备方法如其使用。
公开(公告)号：EP0011288B1
公开(公告)日：1982-01-20
申请号：EP79104497.7
申请日：1979-11-14
申请人： HOECHST AKTIENGESELLSCHAFT
发明人： Landauer, Franz, Dr. , Schaeffer, Georg, Dr.
IPC分类号： C07C21/24 , C07C25/13 , C07C25/02 , C07C63/04 , C07C17/14 , C07C51/093
CPC分类号： C07C63/04 , C07C17/14 , C07C22/04 , C07C25/02 , C07C25/13 , C07C51/093

9. 发明授权

EP1853548B1 PROCESS FOR THE PREPARATION OF BENZOIC ACID DERIVATIVES VIA A NEW INTERMEDIATE OF SYNTHESIS 失效转让
标题翻译：用于生产苯甲酸一个新的合成中间体
公开(公告)号：EP1853548B1
公开(公告)日：2009-05-13
申请号：EP05804725.9
申请日：2005-12-01
申请人： MITENI S.p.A.
发明人： MONDINI, Simonetta, , DALL'AVA, Mirco, , GUERRATO, Alfredo,
IPC分类号： C07C201/08 , C07C205/12 , C07C205/58 , C07C51/093 , C07C63/70
CPC分类号： C07C201/12 , C07C205/12 , C07C205/58
摘要： The object of the invention is the preparation of 2-chloro-4-fluoro-5-nitrobenzoic acid and derivatives thereof, by nitration of 2-chloro-4-fuorobenzotrichloride and the conversion of the novel synthetic intermediate thus obtained into its acid form or derivatives thereof; a further object of the invention is the conversion of benzotrichloride synthetic intermediates into the corresponding benzotrifluoride derivatives.

10. 发明授权

EP0607824B1 Verfahren zur Herstellung mehrfach halogenierter Benzotrichloride und Benzoylchloride sowie neue, mehrfach halogenierte Benzotrichloride 失效
标题翻译：一种用于制备多卤代benzotrichlorides和苯甲酰基，新，多卤代benzotrichlorides过程
公开(公告)号：EP0607824B1
公开(公告)日：1998-04-22
申请号：EP94100203.2
申请日：1994-01-07
申请人： BAYER AG
发明人： Marhold, Albrecht, Dr. , Andres, Peter, Dr.
IPC分类号： C07C17/20 , C07C51/58 , C07C63/10 , C07C25/13 , C07C63/70 , C07C51/093
CPC分类号： C07C17/32 , A23K20/195 , B01J27/10 , B01J27/12 , B01J27/128 , C07C17/12 , C07C17/208 , C07C25/13 , C07C51/58 , C07C63/70

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