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    • 2. 发明公开
    • PROCESS FOR THE MODIFICATION OF CURCUMA AROMATICA ESSENTIAL OIL
    • VERFAHREN ZUR MODIFIZIERUNG AROMATISCHERÄTHERISCHERÖLEAUS KURKUMA
    • EP2690969A1
    • 2014-02-05
    • EP12713320.5
    • 2012-03-01
    • Council of Scientific & Industrial Research
    • AGNIHOTRI, Vijai, KantSINGH, BikramBABU, Garikapati, Dyva, KiranCHAND, GopiSINGH, Rakesh, DeosharanAHUJA, Paramvir, Singh
    • A23L1/015C11B9/02
    • C11B9/0046A23L27/12C11B9/022
    • Curcuma aromatica essential oil is blue-black dark liquid with camphoraceous, woody, amber and spicy characteristic odour and is less valued in market, however the prepared value added products have very good shining color with the improved fragrance. The present invention relates to an efficient process for the modification of Curcuma aromatica essential oil to develop value added fragranced products, the process comprising the steps of mixing of essential oil with one solvent or a combination of more than one solvents, cooling the mixture over ice bath or at lower temperature at rotation of 1000 rpm or at simple magnetic stirrer at high speed, addition of reducing agent at different proportion at a certain time period for desired product, after completion of the reaction, addition of ice water to the reaction mixture to terminate the reaction, extracting the mixture using solvent for three to five times, washing the extractive with dilute acidic water and then with water, washed product was dried at lower temperature to obtain modified essential oils in order to develop fragranced products with recovery of 60 to 95% and use of the modified essential oil in the range between 0.05 to 100% in perfumery or allied industries.
    • 姜黄香精油是具有樟脑,木质,琥珀和辛辣特征气味的蓝黑色深色液体,在市场上价值较低,然而准备的增值产品具有非常好的发光颜色和改善的香味。 本发明涉及一种用于改良姜黄香精油以开发增值香料的有效方法,该方法包括以下步骤:将精油与一种溶剂或多种溶剂的组合混合,在冰上冷却混合物 浴或在1000rpm的旋转下或在简单磁力搅拌器下以较高的速度在较低的温度下,在所需产物的一定时间内以不同比例加入还原剂,反应完成后,向反应混合物中加入冰水 终止反应,用溶剂萃取混合物三至五次,用稀酸水洗涤萃取液,然后用水洗涤,将产物在较低温度下干燥,得到改性精油,以开发回收率为60〜 95%,在香料或有关行业使用0.05至100%之间的改性精油。