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    • 6. 发明公开
    • Method for manufacturing optical fiber base material
    • 一种用于生产光学纤维基材的过程
    • EP2226302A3
    • 2012-07-11
    • EP10002146.8
    • 2010-03-03
    • Shin-Etsu Chemical Co., Ltd.
    • Yoshida, Makoto
    • C03B37/014
    • C03B37/0142C03B2207/06C03B2207/12C03B2207/20C03B2207/36Y02P40/57
    • A method for manufacturing an optical fiber base material includes producing glass fine particles through a hydrolysis of a glass material gas in a flame created by an oxidizing gas and a combustible gas. The method uses a burner including: a central gas discharge port that ejects a gas containing an oxidizing gas; a plurality of small-diameter gas discharge ports that are arranged in a concentric circle with the central gas discharge port so as to externally surround the central gas discharge port, where the plurality of small-diameter gas discharge ports eject a gas containing an oxidizing gas; a combustible gas discharge port that is concentrically arranged with the central gas discharge port so as to externally surround the central gas discharge port, where the combustible gas discharge port has the plurality of small-diameter gas discharge port arranged therein and the combustible gas discharge port ejects a combustible gas; and an oxidizing gas discharge port that is concentrically arranged with the central gas discharge port so as to externally surround the combustible gas discharge port, the oxidizing gas discharge port ejecting an oxidizing gas. Here, a relation of V 1 > V 2 > V 3 > V 4 is satisfied where V 1 denotes a gas flow speed at the central gas discharge port, V 2 denotes a gas flow speed at the plurality of small-diameter gas discharge ports, V 3 denotes a gas flow speed at the combustible-gas discharge port, and V 4 denotes a gas flow speed at the oxidizing gas discharge port.
    • 9. 发明公开
    • Method of producing synthetic quartz glass for excimer laser
    • Verfahren zur Herstellung von synthetischem QuarzglasfürExcimer-Laser
    • EP2208715A2
    • 2010-07-21
    • EP10250087.3
    • 2010-01-19
    • Shin-Etsu Chemical Co., Ltd.
    • Maida, Shigeru c/oSpecilty Chical Research CenterOtsuka, Hisatou c/oSpecilty Chical Research Center
    • C03B19/14
    • C03B19/1453C03B19/1469C03B2201/075C03B2201/21C03B2207/20Y02P40/57
    • Disclosed is a method of producing a synthetic quartz glass for excimer laser by depositing on a target silica particulates obtained by subjecting a silica raw material to vapor-phase hydrolysis or oxidative decomposition in an oxyhydrogen flame in a vacuum sintering furnace to form a porous silica base material, vitrifying the porous silica base material, and subjecting the vitrified material to hot forming, an annealing treatment and a hydrogen doping treatment, wherein the vitrification of the porous silica base material includes: (a) a step of holding a vacuum pressure at or below 20.0 Pa in a temperature range from 400°C, inclusive, to 900°C, exclusive; (b) a step of holding a vacuum pressure at or below 10.0 Pa in a temperature range from 900°C, inclusive, to 1100°C, exclusive; and (c) a step of holding a vacuum pressure at or below 3.0 Pa in a temperature range from 1100°C to a transparent-vitrification temperature.
    • 公开了一种通过在真空烧结炉中在氧氢火焰中使二氧化硅原料进行气相水解或氧化分解而获得的目标二氧化硅微粒上沉积以制备准分子激光的合成石英玻璃的方法,以形成多孔二氧化硅基质 材料,使多孔二氧化硅基材玻璃化,并对玻璃化物进行热成型,退火处理和氢掺杂处理,其中多孔二氧化硅基材的玻璃化包括:(a)将真空压力保持在或 低于20.0Pa,温度范围为400℃以上,900℃以下; (b)在900℃以上至1100℃的温度范围内保持真空压力为10.0Pa以下的工序; 和(c)在1100℃至透明玻璃化温度的温度范围内保持真空压力等于或低于3.0Pa的步骤。
    • 10. 发明公开
    • Method of fabricating an optical fiber preform and a burner therefor
    • 一种用于生产预成型件的光学纤维和燃烧器的过程
    • EP2098489A1
    • 2009-09-09
    • EP09002895.2
    • 2009-02-27
    • Shin-Etsu Chemical Co., Ltd.
    • Yoshida, Makoto
    • C03B37/014
    • C03B37/01815C03B37/0142C03B37/018C03B2207/06C03B2207/20Y02P40/57
    • A method of fabricating an optical fiber preform, capable of depositing glass particles with high deposition rate without reducing deposition efficiency and fabricating an optical fiber preform having little bubbles using a burner having a simple structure, is provided. In the invention, a mixed gas of a glass raw material gas with a combustion assisting gas is ejected from an annular nozzle of a burner having a coaxially multiple tube structure, and a burnable gas is ejected from an inner nozzle located inside the annular nozzle. Alternatively, a mixed gas of a glass raw material gas with a burnable gas may be ejected from an annular nozzle, and a combustion assisting gas is ejected from an inner nozzle located inside the annular nozzle. In each case of the above, the burnable gas and the combustion assisting gas, respectively, are ejected from outer nozzles located outside the annular nozzle.
    • 制造上的光纤预制件,其能够沉积具有高沉积速率的玻璃颗粒不降低的沉积效率,并具有使用具有简单结构的燃烧器气泡少的光纤母材的制造的方法,提供了一种。 在本发明中,玻璃原料气体与燃烧辅助气体的混合气体从在具有同轴多管结构的燃烧器的环形设计喷嘴喷出,以及一个可燃气体从位于环形设计喷嘴内的帧内喷嘴喷出。 可替代地,具有可燃气体的玻璃原料气体的混合气体可以从环形设计的喷嘴喷出,以及一个燃烧辅助气体从位于环形设计喷嘴内的帧内喷嘴喷出。 在上文中,可燃气体和助燃辅助气体的每种情况下,分别由位于环形设计喷嘴外部外喷嘴喷出。