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1. 发明公开

EP1585711A1 SOLUBLE FERTILIZER COMPOSITIONS COMPRISING CALCIUM AND/OR MAGNESIUM PHOSPHATES 有权
标题翻译：水溶性肥料组合物钙和/或镁含磷酸盐的
公开(公告)号：EP1585711A1
公开(公告)日：2005-10-19
申请号：EP04702404.7
申请日：2004-01-15
申请人： Rotem Amfert Negev Ltd.
发明人： JOSEF, Alexander , TUBOV, Shula , ZUKERMAN, Itshak
IPC分类号： C05B7/00 , C05B9/00 , C05B21/00
CPC分类号： C05B7/00 , C05B9/00
摘要： The present invention provides fertilizer compositions c omprising calcium and magnesium phosphates together with alkali metal double phosphates, and process for their preparation. The solid composition is freely flowing and well soluble

2. 发明公开

EP0610136A1 Process for the manufacture of pure amorphous silica from rocks 失效
标题翻译： Verfahren zur Herstellung von reinen amorphenKieselsäurenaus Gesteinen。
公开(公告)号：EP0610136A1
公开(公告)日：1994-08-10
申请号：EP94400218.7
申请日：1994-02-02
申请人： ROTEM AMFERT NEGEV LTD.
发明人： Iosef, Alexander
IPC分类号： C01B33/193
CPC分类号： C01B33/193 , C01P2002/02 , C01P2006/11 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： A process for the manufacture of pure amorphous silica from rocks containing non-crystalline silica is described. The process comprises the steps of:
(a) dissolution of said rock in an alkaline solution comprising sodium hydroxide and sodium carbonate, obtaining a solution of sodium silicate; (b) precipitation of pure amorphous silica by adding sodium bicarbonate into said sodium silicate and co-producing sodium carbonate, the weight ratio between SiO₂ and Na₂O in said dissolution step is in the range of between 0.5 to 3.0; and (c) the sodium carbonate sclution is transformed into crystalline sodium bicarbonate, by a salting out reaction with sodium chloride, being recycled to the process. According to a preferred embodiment, the alkaline solution is obtained by the caustification of sodium carbonate with calcium hydroxide. The preferred concentration of sodium hydroxide in said dissolution step is in the range of 4% to 14% by weight.
摘要翻译：描述了从含有非结晶二氧化硅的岩石制造纯无定形二氧化硅的方法。该方法包括以下步骤：（a）将所述岩石溶解在包含氢氧化钠和碳酸钠的碱性溶液中，得到硅酸钠溶液; （b）通过向所述硅酸钠中加入碳酸氢钠并共同生产碳酸钠沉淀纯无定形二氧化硅，所述溶解步骤中SiO 2与Na 2 O的重量比在0.5至3.0的范围内; 和（c）通过与氯化钠的盐析反应将碳酸钠溶液转化成结晶碳酸氢钠，再循环到该方法中。根据优选的实施方案，碱性溶液是通过用氢氧化钙对碳酸钠进行除碱而得到的。所述溶解步骤中优选的氢氧化钠浓度在4重量％至14重量％的范围内。

3. 发明公开

EP0240635A1 Process for the manufacture of disodium phosphate 失效转让
标题翻译： Verfahren zur Herstellung von Natriummonohydrogenphosphat。
公开(公告)号：EP0240635A1
公开(公告)日：1987-10-14
申请号：EP86304443.4
申请日：1986-06-10
申请人： NEGEV PHOSPHATES LTD.
发明人： Iosef, Alexander , Bar-On, Menachem
IPC分类号： C01B25/30
CPC分类号： C01B25/303
摘要： A process for the manufacture of disodium phosphate of a high purity without utilising organic solvents. Monosodium sulfate is reacted, at a temperature in the range of 40 to 100°C with a phosphate constituent selected from phosphate rock, dicalcium phosphate or mixtures thereof, in the presence of phosphoric acid. The common metal impurities, organic matter and fluorides present in the starting phosphate rock are substantially complete eliminated with the solid gypsum or dicalcium phosphate resulted thereto. After separating said solid, the filtrate is treated in two neutralization stages: first by a calcium constituent selected from calcium carbonate, calcium hydroxide or mixtures thereof and separating the formed dicalcium phosphate, followed by a 'second neutralization with an alkali sodium constitu- lent selected from sodium hydroxide, sodium carbonate and sodium bicarbonate or mixtures thereof at a pH in the range of 8.0 to 9.5. From the resulted filtrate, pure disodium phosphate is obtained by crystallisation.
摘要翻译：一种制造高纯度磷酸二钠而不使用有机溶剂的方法。在磷酸的存在下，硫酸硫酸钠与选自磷酸盐岩，磷酸二钙或其混合物的磷酸盐成分在40至100℃的温度下反应。存在于起始磷酸盐岩中的普通金属杂质，有机物质和氟化物基本上完全被固体石膏或磷酸二钙所消除。在分离所述固体之后，将滤液在两个中和阶段进行处理：首先用选自碳酸钙，氢氧化钙或其混合物的钙成分进行处理，分离所形成的磷酸二钙，然后用选自氢氧化钠的碱金属钠组分进行第二次中和，碳酸钠和碳酸氢钠或其混合物，pH在8.0至9.5的范围内。从所得滤液中，通过结晶获得纯磷酸二钠。

4. 发明公开

EP0208422A2 Process for the manufacture of monopotassium phosphate 有权转让
标题翻译：生产磷酸一钾的方法
公开(公告)号：EP0208422A2
公开(公告)日：1987-01-14
申请号：EP86304442.6
申请日：1986-06-10
申请人： NEGEV PHOSPHATES LTD.
发明人： Iosef, Alexander , Bar-On, Menachem
IPC分类号： C01B25/30
CPC分类号： C01B25/301 , C01B25/303
摘要： A process for the manufacture of monopotassium phosphate of a high purity without utilizing organic solvents. Monopotassium sulfate is reacted, at a temperature in the range of 40 to 100°C with a phosphate constituent selected from phosphate rock, dicalcium phosphate or mixtures thereof in the presence of phosphoric acid. The common metal impurities, organic matter and fluorides present in the starting phosphate rock are substantially eliminated, with the calcium sulfate resulted thereto. After separating out the calcium sulfate, the filtrate is neutralised to a pH in the range of 3 to 7, with a calcium-containing compound comprising Ca(OH) 2 , CaO or CaC0 3 , or mixtures thereof. From the filtrate obtained, pure monopotassium phosphate is crystallised out.
摘要翻译：不使用有机溶剂制造高纯度磷酸一钾的方法。在磷酸存在下，硫酸二钾在40-100℃的温度下与选自磷酸盐岩，磷酸二钙或其混合物的磷酸盐组分反应。存在于起始磷酸盐岩石中的普通金属杂质，有机物质和氟化物基本上被消除，随之产生硫酸钙。分离出硫酸钙后，用含钙化合物（包括Ca（OH）2，CaO或CaCO 3或其混合物）将滤液中和至3-7的pH。从得到的滤液中，将纯的磷酸一钾结晶出来。

5. 发明公开

EP2225187A2 PREPARATION OF A POTASSIUM PHOSPHATE BASED COMPOSITION 有权
标题翻译：制造组合物磷酸钾BASE
公开(公告)号：EP2225187A2
公开(公告)日：2010-09-08
申请号：EP08856584.1
申请日：2008-11-13
申请人： Rotem Amfert Negev Ltd.
发明人： JOSEF, Alexander , ZUKERMAN, Itshak
IPC分类号： C05B17/00 , C05D1/00 , C01B25/26
CPC分类号： C05B7/00 , C01B25/306 , C05G3/0088
摘要： Abstract Provided is a freely flowing particulate fertilizer essentially consisting of potassium phosphate of the formula K3H3(PO4)2 and of less than 8 wt% water. The stable and not caking fertilizer is characterized by an XRD signal corresponding to 2-theta of about 70°. An economic process for making the fertilizer is also provided.

6. 发明公开

EP1216092A1 SILICON-CONTAINING TITANIUM DIOXYDE, METHOD FOR PREPARING THE SAME AND CATALYTIC COMPOSITIONS THEREOF 有权
标题翻译：改性二氧化钛，制备的方法和催化剂组合物含有它的
公开(公告)号：EP1216092A1
公开(公告)日：2002-06-26
申请号：EP99939588.2
申请日：1999-08-23
申请人： Rotem Amfert Negev Ltd.
发明人： MIRSKY, Ya'acov , GORLOVA, Marina N.
IPC分类号： B01J21/06 , B01J21/08 , C01G23/047 , C01B17/04
CPC分类号： B01J21/063 , B01J21/08 , C01B17/0434 , C01B17/0465 , C01P2002/70 , C01P2002/85 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C09C1/3653
摘要： A method for preparing thermally stable, silicon-containing titanium dioxide, said method comprising the reaction of titanium hydroxide or titanium dioxide with a silica sol, under conditions which prevent the coagulation of silica particles in said sol, to obtain silicon-containing titanium hydroxide or silicon-containing titanium dioxide, and in the case of silicon-containing titanium hydroxide, heat treating the same to obtain silicon-containing titanium dioxide.

7. 发明公开

EP0719748A2 Process for the manufacturing of sulfur-containing fertilizers 失效
标题翻译： Verfahren zur Herstellung von schwefelenthaltendenDüngemitteln
公开(公告)号：EP0719748A2
公开(公告)日：1996-07-03
申请号：EP95402939.3
申请日：1995-12-26
申请人： ROTEM AMFERT NEGEV LTD.
发明人： Stern, Shmuel , Ben-Yoseph, Eli
IPC分类号： C05G3/00 , B01J2/00 , C05B17/00 , C05B19/00
CPC分类号： C05G3/0023
摘要： The invention relates to a process for obtaining sulfur-containing fertilizers. According to the invention, a substrate containing fertilizer particles is heated to a temperature above the melting point of sulfur and subsequently by admixing with the sulfur, the latter is melted by the heat provided by said preheated fertilizer particles, producing a homogeneous coating on the fertilizer particles. According to a preferred embodiment the temperature at which the fertilizer particles are heated will be in the range of 140°C to 280°C. Other materials may be added either into the phosphate or to the resulted mixture, having the purpose to modify the physical nature of the sulfur. The sulfur availability from the coated fertilizer particles may be adjusted by varying the temperature at which the fertilizer particles are heated. Typical examples of fertilizers useful for the process are: phosphate rock, superphosphate, monopotassium phosphate, triple superphosphate and potassium chloride.
摘要翻译：本发明涉及一种获得含硫肥料的方法。根据本发明，将含有肥料颗粒的底物加热到高于硫熔点的温度，随后通过与硫混合，后者由所述预热的肥料颗粒提供的热量熔化，在肥料上产生均匀的涂层粒子。根据优选的实施方案，肥料颗粒被加热的温度将在140℃至280℃的范围内。其它材料可以添加到磷酸盐或所得混合物中，目的是改变物理硫的性质。可以通过改变肥料颗粒被加热的温度来调节来自涂覆的肥料颗粒的硫的可用性。用于该方法的肥料的典型实例是：磷酸盐岩，过磷酸钙，磷酸二氢钾，过磷酸三钙和氯化钾。

8. 发明公开

EP2867160A1 CONTINUOUS PROCESS FOR MANUFACTURING A NEUTRAL GRANULAR P/K FERTILIZER 有权
标题翻译：连续方法制造NEUTRAL GRAIN P / K-肥料
公开(公告)号：EP2867160A1
公开(公告)日：2015-05-06
申请号：EP13809225.9
申请日：2013-06-27
申请人： Rotem Amfert Negev Ltd.
发明人： AVIV, Talia , COHEN, Uri, Sasson , ORGIL, Doron , AROCH, Itsik
IPC分类号： C01B25/163 , C05D1/00 , C01B25/26 , C05B13/06 , B01D9/00 , B01D11/04
CPC分类号： C05B17/00 , C01B25/301 , C05B7/00 , C05B13/06
摘要： The invention provides a continuous process for manufacturing an essentially neutral phosphorus/potassium rich fertilizer from basic chemical commodities. The fertilizer is a freely-flowing particulate solid.

9. 发明公开

EP2867159A1 CONTINUOUS PROCESS FOR MANUFACTURING FREELY FLOWING SOLID ACIDIC P/K FERTILIZER 有权
标题翻译：连续法生产自由流动，固体和酸P /钾肥
公开(公告)号：EP2867159A1
公开(公告)日：2015-05-06
申请号：EP13808515.4
申请日：2013-06-27
申请人： Rotem Amfert Negev Ltd.
发明人： AVIV, Talia , COHEN, Uri Sasson , ORGIL, Doron , AROCH, Itsik
IPC分类号： C01B25/163 , C05D1/00 , C01B25/26 , C05B13/06 , B01D9/00 , B01D11/04 , C05D5/00
CPC分类号： C05B17/00 , C01B25/301 , C01B25/34 , C05B7/00 , C05B13/06 , C05D1/00 , C05D5/00 , C05G3/0088
摘要： The invention provides a continuous process for manufacturing a phosphorus/potassium fertilizer from basic chemical commodities. The fertilizer is a free-flowing solid, stable on storage, consisting mainly of a phosphate of formula ΚΗ
5 (Ρ0
4 )
2.

10. 发明授权

EP1585711B1 SOLUBLE FERTILIZER COMPOSITIONS COMPRISING CALCIUM AND/OR MAGNESIUM PHOSPHATES 有权
标题翻译：水溶性肥料组合物钙和/或镁含磷酸盐的
公开(公告)号：EP1585711B1
公开(公告)日：2006-05-03
申请号：EP04702404.7
申请日：2004-01-15
申请人： Rotem Amfert Negev Ltd.
发明人： JOSEF, Alexander , TUBOV, Shula , ZUKERMAN, Itshak
IPC分类号： C05B7/00 , C05B9/00 , C05B21/00
CPC分类号： C05B7/00 , C05B9/00
摘要： The present invention provides fertilizer compositions c omprising calcium and magnesium phosphates together with alkali metal double phosphates, and process for their preparation. The solid composition is freely flowing and well soluble

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