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    • 5. 发明公开
    • PREPARATION OF RARE EARTH PERMANENT MAGNET MATERIAL
    • 稀土永磁材料的制备
    • EP3109869A1
    • 2016-12-28
    • EP16157102.1
    • 2016-02-24
    • Tianhe (Baotou) Advanced Tech Magnet Co., Ltd.
    • DIAO, ShulinDONG, YiYI, HaiboFAN, YuelinMIAO, JuchangWU, ShujieYUAN, YiCHEN, YaYUAN, Wenjie
    • H01F1/057H01F41/02
    • H01F1/055B22F3/24B22F9/023B22F9/04B22F2003/248B22F2009/044H01F1/0536H01F1/0577H01F41/0293
    • The present invention provides a method for preparing a rare earth permanent magnet material. The preparation method of the present invention comprises atomizing spray process and infiltrating process, wherein the atomizing-sprayed sintered rare earth magnet is placed in a closed container before infiltrating. Through the atomizing spray process a solution containing a heavy rare earth element is coated on the surface of a sintered R1-Fe(Co)-B-A-X-M rare earth magnet, and after baking, heat treatment is performed to infiltrate the sprayed heavy rare earth element to the grain boundary phase of the sintered rare earth magnet. The preparation method of the present invention saves the amount of a heavy rare earth element used in the conventional process, and the production cost. In addition, the preparation method of the present invention could, in the premise that the remanence decreases very little, significantly increase coercive force of the magnet, and apparently decrease the remanence temperature coefficient and coercive force temperature coefficient of the magnet, and apparently improve resistance of the magnet against demagnetization at a high temperature.
    • 本发明提供了一种制备稀土永磁材料的方法。 本发明的制备方法包括雾化喷射工艺和渗透工艺,其中雾化喷射的烧结稀土磁体在渗透前置于密闭容器内。 通过雾化喷射工艺,将含有重稀土元素的溶液涂覆在烧结的R1-Fe(Co)-BAXM稀土磁体的表面上,并且在烘烤之后,进行热处理以使喷射的重稀土元素渗透到 烧结稀土磁体的晶界相。 本发明的制备方法节省了常规工艺中使用的重稀土元素的量和生产成本。 另外,本发明的制备方法可以在剩磁减少很少的前提下,显着增加磁体的矫顽力,明显降低磁体的剩磁温度系数和矫顽力温度系数,明显提高电阻 的磁体在高温下抗退磁。