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1. 发明公开

EP1066346A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：活性染料化合物
公开(公告)号：EP1066346A1
公开(公告)日：2001-01-10
申请号：EP99916317.3
申请日：1999-04-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
IPC分类号： C09B62/02 , C09B62/503 , C09B62/20 , C09B62/04
CPC分类号： C09B62/4401 , C09B62/02 , C09B62/20
摘要： Reactive dye having a Fixation Value (F) on cellulosic substrates of 95 % or greater as measured by the Fixation Value Technical Test Method (at 2:1 standard depth). In addition, the compounds herein have high Exhaustion Values (E), high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing 'soaping off process' and therefore simplying the post dyeing 'soaping off process' traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：通过固色值技术测试方法（在2：1标准深度）测量，在纤维素基材上固定值（F）为95％或更高的活性染料。此外，本文中的化合物具有高耗竭值（E），高效率值（T）并且在减少流出物中的废染料方面显示出显着的改进，增加染料对基底的亲和力，增加染料 - 基底共价键合，增加在室温下染色底物的能力，减少在染色后“皂洗过程”中被除去的染料的量，并因此简化传统上与用纤维活性染料染色棉花相关联的染色后“皂洗过程”，以及减少相邻的白色织物。另外，上面制备的化合物提供更强烈的染色并且需要较少量的盐用于染色棉基质。

2. 发明公开

EP1066345A1 REACTIVE DYE COMPOUNDS 有权
标题翻译：活性染料化合物
公开(公告)号：EP1066345A1
公开(公告)日：2001-01-10
申请号：EP99916316.5
申请日：1999-04-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
IPC分类号： C09B62/02 , C09B62/503
CPC分类号： C09B62/02 , C09B62/4401
摘要： A reactive dye compound comprising: a) at least one chromophore moiety; b) at least one nitrogen-containing heterocycle; c) a linking group to link each chromophore moiety to each nitrogen-containing heterocycle; characterised in that at least one nitrogen-containing heterocycle is substituted with at least one thio-derivative and at least one quaternized nitrogen derivative. The reactive dye compounds of the invention have high Exhaustion Values, high Fixation Values, particularly on cellulosic substrates such as cotton, and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing 'soaping off process' and therefore simplifying the post dyeing 'soaping off process' traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：一种活性染料化合物，其包含：a）至少一个发色团部分; b）至少一个含氮杂环; c）将每个发色团部分连接到每个含氮杂环的连接基团; 其特征在于至少一个含氮杂环被至少一个硫代衍生物和至少一个季铵化氮衍生物取代。本发明的活性染料化合物具有高排放值，高定影值，特别是在纤维素基质例如棉上，并且在减少流出物中废染料方面显示出显着的改进，增加染料对基质的亲和力，增加染料 - 基质共价增加在室温下染色基材的能力，减少在染色后“皂洗过程”中除去的染料量，并由此简化传统上与用纤维活性染料染色棉相关的染色后“皂洗过程”和减少相邻白色织物的污染。另外，上面制备的化合物提供更强烈的染色并且需要较少量的盐用于染色棉基质。

3. 发明公开

EP1066347A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：活性染料化合物
公开(公告)号：EP1066347A1
公开(公告)日：2001-01-10
申请号：EP99916314.0
申请日：1999-04-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
IPC分类号： C09B62/36 , C09B62/02 , A61K7/13 , D06P1/382
CPC分类号： C09B62/36 , A61K8/4926 , A61K8/494 , A61K8/4953 , A61Q5/065 , C09B62/02
摘要： This invention relates to reactive dye compounds, and more especially to reactive dye compounds comprising a chromophore and a nitrogen-containing heterocycle comprising at least one thio-substituent. The reactive dye compounds of the present invention are particularly suitable for dyeing hair.
摘要翻译：本发明涉及活性染料化合物，更具体涉及包含发色团和含有至少一个硫取代基的含氮杂环的活性染料化合物。本发明的活性染料化合物特别适用于染发。

4. 发明授权

EP1066343B1 REACTIVE DYE COMPOUNDS 有权
标题翻译：活性染料化合物
公开(公告)号：EP1066343B1
公开(公告)日：2003-07-16
申请号：EP99916315.7
申请日：1999-04-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
IPC分类号： C09B62/00
CPC分类号： C09B62/20
摘要： Reactive Dye compound having formula (I) wherein: D is a chromophore group; L is a linking moiety; Q is a quaternized nitrogen derivative; X and Y are independently selected from chlorine, bromine, fluorine or hydrogen; A is selected from halogen, preferably chlorine or fluorine; provided that at least one of X and Y is fluorine; A is selected from halogen, preferably chlorine or fluorine; and salts and esters thereof. The reactive dye compounds of the invention have high Exhaustion Values, high Fixation Values, particularly on cellulosic substrates such as cotton, and show significant improvements in terms of reducing spend dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing "soaping off process" and therefor simplying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：具有式（I）的活性染料化合物，其中：D是发色团; L是连接部分; Q是季铵化的氮衍生物; X和Y独立地选自氯，溴，氟或氢; A选自卤素，优选氯或氟; 条件是X和Y中的至少一个是氟; A选自卤素，优选氯或氟; 及其盐和酯。本发明的活性染料化合物具有高排放值，高定影值，特别是在纤维素基质例如棉上，并且在减少流出物中花费染料方面显示出显着的改进，增加染料对基质的亲和力，增加染料 - 基质共价增加在室温下染色基材的能力，减少在染色后“皂洗过程”中除去的染料的量，并因此简化传统上与用纤维活性染料染色棉相关的染色后“皂洗过程”和减少相邻白色织物的污染。另外，上面制备的化合物提供更强烈的染色并且需要较少量的盐用于染色棉基质。

5. 发明公开

EP1179033A1 REACTIVE DYE COMPOUNDS 有权
标题翻译：活性染料
公开(公告)号：EP1179033A1
公开(公告)日：2002-02-13
申请号：EP00932245.4
申请日：2000-05-10
申请人： The Procter & Gamble Company
发明人： LEWIS, David, Malcolm , HE, Wei, Dong , YOUSAF, Taher, Iqbal , GENAIN, Gilles, Yves, Marie, Fernand
IPC分类号： C09B62/503
CPC分类号： C09B62/503 , C09B62/51
摘要： A reactive dye compound comprising: (a) at least one chromophore moiety; (b) at least one SO2C2H4 group which is attached to the chromophore moiety either directly via the sulphur atom of the SO2C2H4 group or a linking group L; characterised in that at least one SO2C2H4 group is substituted on its terminal carbon atom with at least one Y group wherein Y is -A(CO)R* wherein A is selected from O or S and wherein R' contains at least one terminal nucleophilic group, such as OH, NH2, SH, COOH, N, NHR?1 and NR1R2¿ wherein R?1 and R2¿ may be the same or different and may be selected from C1-C4 alkyl; and salts thereof. Also claimed is a process of manufacture of the compounds herein and products obtainable by the process. The compounds herein have high Exhaustion Values (E), high Fixation Values (F) and high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing 'soaping off process' and therefore simplifying the post dyeing 'soaping off process' traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.

6. 发明公开

EP1066343A1 REACTIVE DYE COMPOUNDS 有权
标题翻译：活性染料
公开(公告)号：EP1066343A1
公开(公告)日：2001-01-10
申请号：EP99916315.7
申请日：1999-04-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
IPC分类号： C09B62/00
CPC分类号： C09B62/20
摘要： Reactive Dye compound having formula (I) wherein: D is a chromophore group; L is a linking moiety; Q is a quaternized nitrogen derivative; X and Y are independently selected from chlorine, bromine, fluorine or hydrogen; A is selected from halogen, preferably chlorine or fluorine; provided that at least one of X and Y is fluorine; A is selected from halogen, preferably chlorine or fluorine; and salts and esters thereof. The reactive dye compounds of the invention have high Exhaustion Values, high Fixation Values, particularly on cellulosic substrates such as cotton, and show significant improvements in terms of reducing spend dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing 'soaping off process' and therefor simplying the post dyeing 'soaping off process' traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.

7. 发明授权

EP1066345B1 REACTIVE DYE COMPOUNDS 有权
标题翻译：活性染料化合物
公开(公告)号：EP1066345B1
公开(公告)日：2003-03-12
申请号：EP99916316.5
申请日：1999-04-01
申请人： THE PROCTER & GAMBLE COMPANY
发明人： BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
IPC分类号： C09B62/02 , C09B62/503
CPC分类号： C09B62/02 , C09B62/4401

8. 发明公开

EP1230454A1 COTTON FABRIC WITH DURABLE PROPERTIES 审中-公开
标题翻译：对恒特点棉织物
公开(公告)号：EP1230454A1
公开(公告)日：2002-08-14
申请号：EP00965472.4
申请日：2000-09-27
申请人： THE PROCTER & GAMBLE COMPANY
发明人： SIVIK, Mark, Robert , HUBESCH, Bruno, Albert , BERNAERTS, An , LEWIS, David, Malcolm
IPC分类号： D06M13/355 , D06M13/358 , D06M13/364 , D06M15/03
CPC分类号： C11D3/044 , C11D3/10 , C11D3/227 , C11D3/228 , C11D3/28 , C11D3/349 , C11D3/364 , D06M13/355 , D06M13/358 , D06M13/364 , D06M13/44 , D06M15/03 , D06M23/06 , D06M2101/06 , D06M2200/20
摘要： The present invention relates to compositions and a process which utilizes said compositions for providing cellulosic fabric and cellulosic fabric blends with durable press, said process comprising the steps of contacting fabric with a composition comprising: a) from about 0.1 % to about 20 % by weight, of a cellulose modifying compound having formula (I) wherein R is a backbone linking unit; each R1 is independently i) a cellulose reactive moiety; ii) a polysaccharide unit; iii) s-triazine units having formula (II); iv) pyrimidine units having formula (III); v) cyclotriphosphazene units having formula (IV); vi) and mixtures thereof; wherein R2 is hydrogen, C¿1?-C4 alkyl, or R?1¿; X is -N-, -CH-, or mixtures thereof; the index m is from 0 to 5, the index n is from 0 to 5; b) from about 0.01 % to about 10 % by weight, of a crosslinking catalyst; and c) the balance carriers and other adjunct ingredients. The compositions of the present invention can take the form of laundry detergent compositions, fabric post-laundry spray-on compositions, and the like.

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