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1. 发明公开

EP3031777A1 ZEOLITE, AND PRODUCTION METHOD AND USE THEREFOR 审中-公开
标题翻译： ZEOLITH UND HERSTELLUNGSVERFAHREN SOWIE VERWENDUNGDAFÜR
公开(公告)号：EP3031777A1
公开(公告)日：2016-06-15
申请号：EP14834021.9
申请日：2014-08-04
申请人： Mitsubishi Chemical Corporation , Mitsubishi Plastics, Inc.
发明人： CHEN, Haijun , TAKEWAKI, Takahiko , MATSUO, Takeshi
IPC分类号： C01B39/48 , B01D53/94 , B01J29/76
CPC分类号： B01J29/76 , B01D53/9418 , B01D2251/2062 , B01D2251/2067 , B01D2251/208 , B01D2255/20761 , B01D2255/50 , B01D2258/012 , B01J37/10 , B01J2229/183 , C01B39/48
摘要： The present invention provides a novel high-silica zeolite having a high molar ration of a tetravalent element (Y) to a trivalent element (X) in terms of oxide. A zeolite, comprising at least a trivalent element X and a tetravalent element Y, wherein a molar ratio n = YO 2 /X 2 O 3 in terms of oxide is 9.5 or more, and the zeolite comprises an RHO-type structure, or comprising at least a trivalent element X and a tetravalent element Y, wherein a molar ratio n = YO 2 /X 2 O 3 in terms of oxide is 9.5 or more, and a characteristic X-ray diffraction pattern.
This zeolite is produced by hydrothermal synthesis of a zeolite from an aqueous gel that is prepared by adding a mixed solution comprising a crown ether, an alkali, and water to a solution containing an aluminum atom material, and by then dropwise adding a liquid containing a silicon atom material.
摘要翻译：本发明提供一种与氧化物换算为三价元素（X）的四价元素（Y）摩尔比高的新型高硅沸石。包含至少三价元素X和四价元素Y的沸石，其中以氧化物计的n = YO 2 / X 2 O 3的摩尔比为9.5以上，沸石包含RHO型结构，或包含至少三价元素X和四价元素Y，其中以氧化物换算的n = YO 2 / X 2 O 3的摩尔比为9.5以上，特征X射线衍射图。该沸石是通过将水性凝胶的水热合成由通过将包含冠醚，碱和水的混合溶液加入到含有铝原子的溶液中制备的沸石而制成的，然后逐滴加入含有硅原子材料。

2. 发明公开

EP3124435A1 METHOD FOR PRODUCING TRANSITION METAL-CONTAINING ZEOLITE, TRANSITION METAL-CONTAINING ZEOLITE OBTAINED BY SAID METHOD, AND EXHAUST GAS PURIFYING CATALYST USING SAID ZEOLITE 审中-公开
标题翻译：用于生产ÜBERGANGSMETALLHALTIGEM型分子筛所述方法GOT含有过渡金属沸石催化剂和排放与所述沸石
公开(公告)号：EP3124435A1
公开(公告)日：2017-02-01
申请号：EP15767784.0
申请日：2015-02-27
申请人： Mitsubishi Plastics, Inc.
发明人： KIMURA, Takahide , HOTTA, Yuusuke , KIYONO, Kenichi , TAKEWAKI, Takahiko , MATSUO, Takeshi
IPC分类号： C01B39/54 , B01D53/94 , B01J20/18 , B01J29/85 , B01J37/04 , B01J37/10
CPC分类号： B01J29/85 , B01D53/02 , B01D53/261 , B01D53/8628 , B01D53/9418 , B01D2253/108 , B01D2255/20761 , B01D2255/50 , B01D2257/80 , B01J20/18 , B01J20/3078 , B01J20/3085 , B01J35/04 , B01J37/0009 , B01J37/10 , B01J2229/18 , B01J2229/36 , C01B37/08 , C01B39/54 , F01N3/2803 , F01N2330/02 , F01N2370/04
摘要： Provided is a method for producing a transition-metal-containing silicoaluminophosphate that is highly suitable as a catalyst or an adsorbent and has excellent high-temperature hydrothermal durability and excellent water resistance, that is, excellent durability against water submersion (water-submersion durability), in a simple and efficient manner. A method for producing a transition-metal-containing zeolite, the method comprising a steam treatment step in which a transition-metal-containing zeolite is stirred at 710°C or more and 890°C or less in the presence of water vapor, the transition-metal-containing zeolite containing a transition metal in a zeolite having a framework structure including silicon atoms, phosphorus atoms, and aluminium atoms.
摘要翻译：本发明提供一种制造含过渡金属硅铝做的方法是非常适合作为吸附剂的催化剂或（水 - 浸没耐久性），并且具有优异的高温水热耐久性和优异的耐水性，所做的是，针对水浸没优异的耐久性的，简单的和有效的方式。一种用于生产含有过渡金属的沸石的方法，该方法包括蒸汽处理步骤，其中的含过渡金属沸石是在水蒸汽的存在下，在710℃或更高和890℃或以下搅拌，则含过渡金属沸石含在具有包含硅原子，磷原子和铝原子的骨架结构的沸石的过渡金属。

3. 发明公开

EP2724983A1 TRANSITION METAL-CONTAINING ZEOLITE 审中-公开
标题翻译： ÜBERGANGSMETALLMIT EINEM ZEOLITH
公开(公告)号：EP2724983A1
公开(公告)日：2014-04-30
申请号：EP12804306.4
申请日：2012-06-19
申请人： Mitsubishi Plastics, Inc.
发明人： CHEN, Haijun , TAKEWAKI, Takahiko , MATSUO, Takeshi
IPC分类号： C01B39/54 , B01D53/94 , B01J20/18 , B01J20/30 , B01J29/83
CPC分类号： C01B39/54 , B01D53/28 , B01D53/94 , B01D53/9418 , B01D2251/2062 , B01D2253/108 , B01D2253/1085 , B01D2253/25 , B01D2255/20738 , B01D2255/20761 , B01D2255/50 , B01D2255/9207 , B01J20/18 , B01J20/28064 , B01J20/3078 , B01J29/763 , B01J29/84 , B01J29/85 , B01J35/002 , B01J35/1023 , B01J37/10 , B01J2229/186 , Y10T428/2982
摘要： A transition-metal-containing silicoaluminophosphate zeolite having excellent high-temperature hydrothermal durability is easily and efficiently produced. A method for producing a transition-metal-containing zeolite that contains a silicon atom, a phosphorus atom, and an aluminum atom in at least its framework structure includes hydrothermal synthesis using an aqueous gel containing a silicon atom raw material, an aluminum atom raw material, a phosphorus atom raw material, a transition metal raw material, and a polyamine (other than diamines). A transition-metal-containing silicoaluminophosphate zeolite produced by hydrothermal synthesis using a zeolite raw material and the aqueous gel containing the transition metal raw material and the polyamine has excellent high-temperature hydrothermal durability and high catalytic activity.
摘要翻译：容易且有效地制造具有优异的高温水热耐久性的含过渡金属的硅铝磷酸盐沸石。至少在其骨架结构中含有硅原子，磷原子和铝原子的含过渡金属的沸石的制造方法包括使用含有硅原子原料的水性凝胶的水热合成，铝原子原料，磷原子原料，过渡金属原料和多胺（二胺以外）。使用沸石原料通过水热合成制造的含过渡金属的硅铝磷酸盐沸石和含有过渡金属原料和多胺的含水凝胶具有优异的高温水热耐久性和高催化活性。

4. 发明公开

EP2772299A1 STEAM-ADSORBING MATERIAL FOR ADSORPTION HEAT PUMP, METHOD FOR MANUFACTURING SAME, AND ADSORPTION HEAT PUMP USING SAME 审中-公开
标题翻译：阻燃剂FÜREINEADSORPTIONSWÄRMEPUMPE，HERSTELLUNGSVERFAHRENDAFÜRUNDADSORPTIONSWÄRMEPUMPEDAMIT
公开(公告)号：EP2772299A1
公开(公告)日：2014-09-03
申请号：EP12844182.1
申请日：2012-10-01
申请人： Mitsubishi Plastics, Inc.
发明人： CHEN, Haijun , TAKEWAKI, Takahiko
IPC分类号： B01D53/28 , B01J20/18 , B01J20/30 , C01B39/54 , F25B17/08
CPC分类号： B01J20/3085 , B01D53/28 , B01D2253/108 , B01J20/18 , B01J20/186 , B01J20/3078 , C01B39/54 , F25B17/08 , Y02P20/129
摘要： There is provided a water vapor adsorbent for adsorption heat pumps that has high adsorption and desorption performance and high water resistance, such as submersion resistance. The water vapor adsorbent contains a zeolite that contains at least a silicon atom, an aluminum atom, and a phosphorus atom in its framework structure and that has a framework density of 12.0 T/1,000 cubic angstroms or more and 16.0 T/1,000 cubic angstroms or less, wherein the water vapor adsorbent contains a group 11 metal of the periodic table, which constitutes 0.1% to 15% by weight of the zeolite. In the zeolite containing the group 11 metal, an ion of the group 11 metal substitutes for a Bronsted acid site, which promotes a hydrolysis reaction of the zeolite, and decreases the number of Bronsted acid sites of the zeolite, thereby improving the water resistance, such as submersion resistance, of the zeolite.
摘要翻译：提供了一种具有高吸附和解吸性能和高耐水性（如浸渍性）的吸附式热泵的水蒸气吸附剂。水蒸气吸附剂含有至少含有硅原子，铝原子和其骨架结构中的磷原子的沸石，其骨架密度为12.0T / 1,000立方或以上16.0T / 1,000立方或以上较少，其中水蒸汽吸附剂含有周期表第11族金属，其占沸石重量的0.1％至15％。在含有第11族金属的沸石中，第11族金属的离子代替布朗斯台德酸位，促进了沸石的水解反应，减少了沸石的布朗斯台德酸位数，提高了耐水性，例如沸石的浸渍电阻。

5. 发明公开

EP2684604A1 CATALYST, ELEMENT FOR NITROGEN OXIDE REMOVAL, AND SYSTEM FOR NITROGEN OXIDE REMOVAL 审中-公开
标题翻译：催化剂元素对废水氮氧化物系统的脱除氮氧化物
公开(公告)号：EP2684604A1
公开(公告)日：2014-01-15
申请号：EP12754467.4
申请日：2012-01-31
申请人： MITSUBISHI PLASTICS, INC.
发明人： MATSUO, Takeshi , NISHIOKA, Daisuke , TAKEWAKI, Takahiko , CHEN, Haijun , OSHIMA, Kazunori
IPC分类号： B01J29/85 , B01D53/94 , B01J37/02 , C01B37/04 , F01N3/10 , F01N3/28
CPC分类号： B01J29/85 , B01D53/9418 , B01D2251/2062 , B01D2251/2067 , B01D2255/20738 , B01D2255/20761 , B01D2255/50 , B01J29/7015 , B01J29/763
摘要： To provide an exhaust gas purification catalyst which has high nitrogen oxide removal performance at both an exhaust gas temperature of 200°C or lower and an exhaust gas temperature of 500°C or higher and high durability to the repetitive adsorption and desorption of water vapor. A catalyst contains zeolite having a framework structure containing at least aluminum atoms, phosphorus atoms, and silicon atoms and metal supported on the zeolite. The integrated intensity area of a signal intensity of -130 ppm to -92.5 ppm is 41% or more of the integrated intensity area of a signal intensity of -130 ppm to -50 ppm in the case of measuring a solid-state 29 Si-DD/MAS-NMR spectrum after water adsorption.
摘要翻译：以提供排气净化催化剂，其具有在两个200℃或更低的排气温度和在500℃或更高的废气温度和高耐用性于重复吸附和解吸水蒸气的高的氮氧化物除去性能。催化剂含有具有一个框架结构的含至少铝原子，磷原子，硅原子和金属负载于沸石的沸石。的-130 ppm至-92.5 ppm的信号强度的积分强度面积为-130 ppm至-50 ppm的信号强度的积分强度面积的41％或更多测量的固态29 Si的情况下水吸附后DD / MAS-NMR谱图。

6. 发明公开

EP2659975A1 CATALYST FOR NITROGEN OXIDE REMOVAL 审中-公开
标题翻译： KATALYSATOR ZUR ENTFERNUNG VON STICKOXIDEN
公开(公告)号：EP2659975A1
公开(公告)日：2013-11-06
申请号：EP11853414.8
申请日：2011-12-26
申请人： MITSUBISHI PLASTICS, INC.
发明人： MATSUO, Takeshi , TAKEWAKI, Takahiko , OSHIMA, Kazunori , CHEN, Haijun , NISHIOKA, Daisuke , TAGUSAGAWA, Caio
IPC分类号： B01J29/85 , B01D53/94 , B01J37/00 , B01J37/02 , F01N3/08 , F01N3/10 , F01N3/28
CPC分类号： B01J29/85 , B01D53/9418 , B01D2255/2092 , B01D2255/50 , B01D2255/707 , B01D2255/9202 , B01D2258/012 , B01D2258/014 , B01J29/7065 , B01J29/743 , B01J29/763 , B01J35/002 , B01J35/006 , B01J2229/186 , B01J2229/42 , C01B39/085 , C01B39/48 , C01B39/54
摘要： [Object] To provide a catalyst for nitrogen oxide removal having no degradation problem caused by adsorbed water when a temperature is raised sharply and exhibiting excellent nitrogen oxide removal performance and retentive characteristic thereof.
[Solution] A catalyst for nitrogen oxide removal, containing a metal-loading zeolite, wherein the zeolite contains a silicon atom, an aluminum atom, and a phosphorus atom in a framework structure, and the amount of water adsorption of the catalyst at 25°C and a relative vapor pressure of 0.5 is 0.05 to 0.2 (kg-water/kg-catalyst) or less. A method for manufacturing this catalyst for nitrogen oxide removal, the method including the steps of drying a mixed slurry containing a metal source, the zeolite, and metal oxide particles having an average particle diameter of 0.1 to 10 µm and/or an inorganic binder and calcining the resulting dry powder.
摘要翻译：提供一种当温度急剧上升且具有优异的氮氧化物去除性能和保持特性时，由吸附水引起的降解问题的氮氧化物除去催化剂。 [溶液]含有金属负载型沸石的氮氧化物除去用催化剂，其中沸石含有骨架结构中的硅原子，铝原子和磷原子，催化剂在25℃的水吸附量 C，相对蒸气压为0.5为0.05〜0.2（kg-水/ kg-催化剂）以下。一种制造用于除去氮氧化物的催化剂的方法，该方法包括以下步骤：干燥含有金属源，沸石和平均粒径为0.1至10μm的金属氧化物颗粒和/或无机粘合剂的混合浆料，以及煅烧所得干粉。

7. 发明授权

EP3214060B1 METHOD FOR PRODUCING HIGH-CONCENTRATION ALCOHOL 有权转让
公开(公告)号：EP3214060B1
公开(公告)日：2020-02-19
申请号：EP15855833.8
申请日：2015-06-29
申请人： Mitsubishi Chemical Corporation
发明人： MAEDA, Kazuhide , YAMAZAKI, Koichi , KAKIUCHI, Hiroyuki , TAHARA, Takeshi , TAKEWAKI, Takahiko
IPC分类号： C07C29/76 , C07C31/08 , B01D3/14 , B01D17/02 , B01D61/36 , B01D71/02 , B01D67/00

8. 发明公开

EP2402071A1 INORGANIC POROUS SUPPORT-ZEOLITE MEMBRANE COMPLEX, METHOD FOR PRODUCING SAME AND SEPARATION METHOD USING SAME 有权转让
标题翻译：无机多孔载体沸石膜复合，工艺用于生产和分离及其用途下
公开(公告)号：EP2402071A1
公开(公告)日：2012-01-04
申请号：EP10746352.3
申请日：2010-02-26
申请人： Mitsubishi Chemical Corporation
发明人： SUGITA, Miki , TAKEWAKI, Takahiko , OSHIMA, Kazunori , FUJITA, Naoko
IPC分类号： B01D71/02 , B01D61/36 , B01D69/10 , C01B39/04
CPC分类号： B01D71/028 , B01D53/228 , B01D67/0051 , B01D69/10 , B01D69/125 , B01D2323/12 , B01D2323/24
摘要： An object of the present invention is to provide a zeolite membrane composite satisfying both the treating amount and the separation performance at a practically sufficient level, which can be applied even in the presence of an organic material and can separate/concentrate an organic material-containing gas or liquid mixture and which is economic without requiring a high energy cost and is not limited in its application range; a production method thereof; and a separation or concentration method using the same. The present invention is an inorganic porous support-zeolite membrane composite, wherein the inorganic porous support contains a ceramic sintered body and the inorganic porous support-zeolite membrane composite has, as a zeolite membrane, a CHA-type zeolite crystal layer on the inorganic porous support surface.
摘要翻译：本发明的一个目的是提供同时满足处理量，并且在实用上足够的水平的分离性能，其可以甚至在有机材料的存在下施用，并且可以分离出沸石膜复合/集中于有机物质含有气体或液体混合物，所有这是经济而不需要高能量成本和在其应用范围不限; 其制造方法; 和使用该方法的分离或浓缩方法。本发明是一种无机多孔载体，沸石膜复合体，worin无机多孔载体中含有的陶瓷烧结体和无机多孔载体的沸石膜复合体具有作为沸石膜，在无机多孔CHA型沸石晶体层支撑面。

9. 发明公开

EP4239029A1 ZEOLITE, METHOD FOR PRODUCING ZEOLITE, COMPOSITION, LIQUID COMPOSITION, LIQUID SEALING AGENT, RESIN COMPOSITE MATERIAL, SEALING MATERIAL, METHOD FOR MANUFATUCTRING SEALING MATERIAL, AND DEVICE 审中-实审
公开(公告)号：EP4239029A1
公开(公告)日：2023-09-06
申请号：EP21886440.3
申请日：2021-11-02
申请人： Mitsubishi Chemical Corporation
发明人： OHNISHI, Ryohji , MATSUNAGA, Chie , KATAGIRI, Noriko , IKEDA, Masashi , MATSUI, Jun , TAKEWAKI, Takahiko
IPC分类号： C08L101/00 , C01B39/48 , C08K3/013 , C08K3/34 , C08L63/00 , H01L23/29 , H01L23/31
摘要： Provided is a liquid composition containing a resin and an inorganic filler, in which the inorganic filler contains a zeolite having a particle size of 1.0 µm or more and 10 µm or less and an inorganic filler having a particle size of 0.1 µm or more and less than 1.0 µm. It is possible to provide a liquid composition capable of lowering viscosity while lowering the thermal expansion coefficient of a cured product.

10. 发明公开

EP3318533A1 COPPER-SUPPORTED ZEOLITE AND EXHAUST-GAS PURIFICATION TREATMENT CATALYST CONTAINING SAID ZEOLITE 无效
标题翻译：铜支撑沸石和废气净化处理催化剂含所述沸石
公开(公告)号：EP3318533A1
公开(公告)日：2018-05-09
申请号：EP16817853.1
申请日：2016-06-27
申请人： MITSUBISHI CHEMICAL CORPORATION
发明人： HOTTA, Yuusuke , TAKEWAKI, Takahiko , MATSUO, Takeshi , KIYONO, Kenichi
IPC分类号： C01B39/54 , B01D53/94 , F01N3/10
CPC分类号： B01J29/763 , B01D53/94 , B01D53/9418 , B01D2255/50 , B01J35/0006 , B01J35/0026 , B01J35/1023 , C01B39/54 , F01N3/10 , Y02T10/24
摘要： Provided is a copper-supported SAPO having good performance as a catalyst and an adsorbent and having not only good high-temperature water-vapor durability, which is usually provided to silicoaluminophosphate zeolites (SAPO), but also good low-temperature water-vapor durability. A copper-supported zeolite comprising a zeolite having a framework structure that contains at least silicon atoms, phosphorus atoms, and aluminum atoms, and copper supported on the zeolite, wherein the copper-supported zeolite satisfies (1) to (3) below: (1) an amount of copper (in terms of copper atoms) supported on the copper-supported zeolite is 1.5% by weight or more and 3.5% by weight or less, (2) the copper-supported zeolite has an UV-Vis-NIR absorption intensity ratio of less than 0.35 as determined by a formula (I) below: Intensisty (22,000 cm -1 )/Intensity (12,500 cm -1 ) ... (I), and (3) a silicon atom content of the copper-supported zeolite satisfies a formula (II) below: 0.07 ≤ x ≤ 0.11 ... (II) where x represents a ratio of the number of moles of the silicon atoms to the total number of moles of the silicon atoms, the aluminum atoms, and the phosphorus atoms contained in the framework structure of the copper-supported zeolite.
摘要翻译：本发明提供一种作为催化剂和吸附剂的具有良好性能的铜负载SAPO，其不仅具有通常提供给硅铝磷酸盐沸石（SAPO）的良好的高温水蒸气耐久性，而且具有良好的低温水蒸气耐久性。一种铜支撑沸石，其特征在于，含有具有至少含有硅原子，磷原子和铝原子的骨架结构的沸石和担载在该沸石上的铜，其中，该铜担载沸石满足下述（1）〜（3）:( 1）铜担载沸石上负载的铜量（换算成铜原子）为1.5重量％以上3.5重量％以下，（2）铜担载沸石具有UV-Vis-NIR （I）确定的吸收强度比小于0.35：强度（22,000cm -1）/强度（12,500cm -1）...（I），和（3）铜的硅原子含量（II）满足下式（II）：0.07≤x≤0.11...（II）其中x表示硅原子的摩尔数与硅原子的总摩尔数之比，铝原子以及含铜沸石的骨架结构中所含的磷原子。

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