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1. 发明公开

EP2864283A1 PROCESS FOR THE PRODUCTION OF ACETIC ACID 有权
标题翻译：生产乙酸的方法
公开(公告)号：EP2864283A1
公开(公告)日：2015-04-29
申请号：EP13809835.5
申请日：2013-06-21
申请人： LyondellBasell Acetyls, LLC
发明人： HALLINAN, Noel, C. , SALISBURY, Brian, A. , BRTKO, Wayne, J. , FITZPATRICK, Michael, E.
IPC分类号： C07C51/573 , C07C53/08 , B01J23/46 , B01J19/24
CPC分类号： C07C51/50 , C07C51/12 , C07C53/08
摘要： A process for producing acetic acid includes: obtaining hydrogen iodide in an acetic acid production system; and continually introducing a complexing agent into the system, wherein the complexing agent and hydrogen iodide interact to form a complex.
摘要翻译：生产乙酸的方法包括：在乙酸生产系统中获得碘化氢; 并不断将络合剂引入该体系中，其中络合剂和碘化氢相互作用形成络合物。

2. 发明公开

EP3645495A1 REACTION CONTROL IN ACETIC ACID PROCESSES 有权
公开(公告)号：EP3645495A1
公开(公告)日：2020-05-06
申请号：EP18743293.5
申请日：2018-06-28
申请人： LyondellBasell Acetyls, LLC
发明人： HALLINAN, Noel, C. , HEARN, John, D. , MATHEWS, Ryan, J. , SALISBURY, Brian, A. , WHITE, Daniel, F.
IPC分类号： C07C51/12 , C07C53/08 , B01J19/00 , G01N21/00

3. 发明公开

EP2914570A1 REMOVAL OF ALDEHYDES IN ACETIC ACID PRODUCTION 有权
标题翻译：醛在乙酸生产分离
公开(公告)号：EP2914570A1
公开(公告)日：2015-09-09
申请号：EP13850770.2
申请日：2013-10-29
申请人： LyondellBasell Acetyls, LLC
发明人： HALLINAN, Noel, C. , SALISBURY, Brian, A.
IPC分类号： C07C51/42 , C07C57/04 , B01J19/24
CPC分类号： C07C51/44 , C07C51/47 , C07C53/08
摘要： A system and method for removing acctaldchydc from an acetic acid system, including providing a solution from the acetic acid system, the stream having methyl iodide and acetaldehyde, and contacting the solution with an ion-exchange resin and/or liquid catalyst.

4. 发明授权

EP3250543B1 RECOVERY OF ACETIC ACID 有权
公开(公告)号：EP3250543B1
公开(公告)日：2019-08-28
申请号：EP16716316.1
申请日：2016-01-27
申请人： LyondellBasell Acetyls, LLC
发明人： SALISBURY, Brian, A. , DESHPANDE, Sanjeev , FITZPATRICK, Michael, E. , HALLINAN, Noel, C. , HEARN, John, D.
IPC分类号： C07C51/12 , C07C51/493 , C07C53/08

5. 发明授权

EP2630471B1 ACETIC ACID PRODUCTION PROCESS 有权转让
公开(公告)号：EP2630471B1
公开(公告)日：2018-11-14
申请号：EP11776664.2
申请日：2011-10-18
申请人： LyondellBasell Acetyls, LLC
发明人： SALISBURY, Brian, A. , HALLINAN, Noel, C.
IPC分类号： G01N21/65 , C07C51/12 , C07C13/08
CPC分类号： G01N21/65 , C07C51/12 , G01N2021/8416 , C07C53/08
摘要： Disclosed is a method for controlling an acetic acid production process. The method comprises: (i) reacting methanol and carbon monoxide in the presence of a carbonylation catalyst, a catalyst stabilizer, methyl iodide, water, and methyl acetate to produce a reactor mixture which comprises the catalyst, the catalyst stabilizer, methanol, carbon monoxide, carbon dioxide, methyl iodide, methyl acetate, water, and acetic acid; (ii) measuring the concentration of a component of the reactor mixture by Raman spectroscopic analysis; and (iii) adjusting the component concentration in the reactor mixture in response to the measured concentration. The method of the invention is particularly useful for measuring and controlling the concentration of carbon monoxide in the reactor liquid mixture.

6. 发明授权

EP2069281B1 PURIFICATION OF ACETIC ACID 有权
公开(公告)号：EP2069281B1
公开(公告)日：2018-10-03
申请号：EP07811151.5
申请日：2007-08-07
申请人： LyondellBasell Acetyls, LLC , Millennium Petrochemicals Inc.
发明人： SAWYER, Gary, A. , BRTKO, Wayne, J. , HANES, Ronnie, M. , SALISBURY, Brian, A.
IPC分类号： C07C51/487 , C07C53/08
CPC分类号： C07C51/487 , C07C53/08
摘要： A method for removing aldehyde impurities from an acetic acid stream is disclosed. The method comprises reacting aldehyde impurities with a hydroxyl compound in a drying distillation column or a combined column to form corresponding acetals. The acetals are subsequently removed as heavy impurities from acetic acid by distillation.

7. 发明公开

EP3250543A1 RECOVERY OF ACETIC ACID 有权
标题翻译：乙酸的回收
公开(公告)号：EP3250543A1
公开(公告)日：2017-12-06
申请号：EP16716316.1
申请日：2016-01-27
申请人： LyondellBasell Acetyls, LLC
发明人： SALISBURY, Brian, A. , DESHPANDE, Sanjeev , FITZPATRICK, Michael, E. , HALLINAN, Noel, C. , HEARN, John, D.
IPC分类号： C07C51/12 , C07C51/493 , C07C53/08
CPC分类号： C07C51/12 , B01J31/0225 , B01J31/10 , B01J2231/49 , C07C51/44 , C07C51/493 , Y02P20/127 , C07C53/08
摘要： The present technology relates to the production and recovery of acetic acid. The recovery processes may include providing a first process stream including acetic acid and greater than 250 ppm of propionic acid; separating at least a portion of the propionic acid from the acetic acid within the first process stream to provide an acetic acid stream including acetic acid and less than 250 ppm of propionic acid and a bottoms stream including propionic acid and acetic acid; reacting the bottoms stream to form a product stream including components of respectively lower boiling points than corresponding components in the bottoms stream; and separating components of the product stream to form an overhead stream including one or more acetates and a bottoms stream including one or more propionates.

8. 发明公开

EP3197855A1 IMPROVED CATALYST STABILITY AND CORROSION PREVENTION IN ACETIC ACID PRODUCTION PROCESS 有权
标题翻译：乙酸生产过程中催化剂稳定性和腐蚀预防的改进
公开(公告)号：EP3197855A1
公开(公告)日：2017-08-02
申请号：EP15771474.2
申请日：2015-09-21
申请人： LyondellBasell Acetyls, LLC
发明人： HALLINAN, Noel, C. , SALISBURY, Brian, A. , WHITE, Daniel, F. , RAMAGE, David, L. , FERN, Jared, T.
IPC分类号： C07C51/12 , C07C53/08
CPC分类号： C07C51/12 , B01J27/20 , C07C53/08
摘要： Processes for producing acetic acid herein generally include contacting methanol and carbon monoxide in the presence of a reaction medium under carbonylation conditions sufficient to form acetic acid, the reaction medium including a carbonylation catalyst selected from rhodium catalysts, iridium catalysts and palladium catalysts; from 1 wt. % to 14 wt. % water; and a plurality of additives, in-situ generated derivatives of the plurality of additives or combinations thereof; the plurality of additives including a first additive including one or more phosphine oxides and a second additive selected from heteropolyacids, metal salts and combinations thereof, the heteropolyacids represented by the formula HnM12XO40, wherein H is hydrogen, M is selected from tungsten and molybdenum, X is selected from phosphorous and silicon and O is oxygen and n is 3 or 4, the metal salts are selected from transition metal salts, lanthanide metal salts and combinations thereof; and recovering acetic acid from the process.
摘要翻译：本文制备乙酸的方法通常包括在足以形成乙酸的羰基化条件下，在反应介质存在下使甲醇和一氧化碳接触，反应介质包括选自铑催化剂，铱催化剂和钯催化剂的羰基化催化剂; 从1wt。％至14wt。％水; 和多种添加剂，所述多种添加剂或其组合的原位产生的衍生物; 所述多种添加剂包括含有一种或多种氧化膦和选自杂多酸，金属盐及其组合的第一添加剂的第一添加剂，由式HnM12XO40表示的杂多酸，其中H是氢，M选自钨和钼，X 选自磷和硅，O为氧且n为3或4，所述金属盐选自过渡金属盐，镧系金属盐及其组合; 并从该过程中回收乙酸。

9. 发明授权

EP2470489B1 PREPARATION OF ACETIC ACID 有权转让
标题翻译：乙酸的制备
公开(公告)号：EP2470489B1
公开(公告)日：2018-04-11
申请号：EP10737396.1
申请日：2010-07-19
申请人： LyondellBasell Acetyls, LLC , Equistar Chemicals, LP
发明人： FITZPATRICK, Michael, E. , NGUYEN, Chuc, Tu , BRTKO, Wayne, J. , SALISBURY, Brian, A.
IPC分类号： C07C51/44 , C07C51/12
CPC分类号： C07C51/12 , C07C51/44 , C07C53/08
摘要： A method for reducing aldehydes in an acetic acid production process is disclosed. The acetic acid is produced by reacting methanol and carbon monoxide in the presence of a carbonylation catalyst. The method comprises reacting an aldehyde-containing stream with an alcohol to form an acetal-containing stream. An acetal-enriched stream is separated from the acetal-containing stream and then hydrolyzed to form a hydrolysis mixture comprising the alcohol and the aldehydes. The alcohol is isolated from the hydrolysis mixture and used to react with the aldehyde-containing stream to form the acetal-containing stream. The invention reduces aldehydes in the acetic acid produced.

10. 发明授权

EP2681183B1 ACETIC ACID PRODUCTION PROCESS 有权转让
标题翻译：醋酸生产工艺
公开(公告)号：EP2681183B1
公开(公告)日：2015-03-25
申请号：EP12716782.3
申请日：2012-02-27
申请人： LyondellBasell Acetyls, LLC
发明人： SALISBURY, Brian, A. , HALLINAN, Noel, C.
IPC分类号： C07C51/12 , C07C53/08 , C07C51/44 , C07C51/48 , B01J19/00 , G01N21/65
CPC分类号： C07C51/12 , C07C51/44 , C07C51/48 , G01N21/65 , G01N2021/8416 , C07C53/08

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