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    • 5. 发明公开
    • APPARATUS AND METHOD FOR PREPARING GLYCOL
    • 用于制备乙二醇的装置和方法
    • EP3219698A1
    • 2017-09-20
    • EP16844605.2
    • 2016-08-25
    • LG Chem, Ltd.
    • EOM, Sung ShikJUNG, Da WonKIM, Tae YunCHOI, Jung UkKO, Dong HyunKIM, Mi YoungCHOI, Min Ji
    • C07C29/80C07C29/82C07C29/14C07C31/20
    • C07C29/141B01D3/10B01D3/141B01D3/143B01J8/02B01J19/245B01J2208/027B01J2219/24C07C29/80C07C29/84C07C45/75C07C45/80C07C45/82C07C31/20C07C47/19
    • The present disclosure relates to an apparatus for generating glycol and a method thereof. More particularly, the present disclosure relates to an apparatus for generating glycol including (a) an aldol reactor; (b) an extractor for extracting an aldol product, unsaturated aldehyde, using an organic solvent that is not mixed with water; (c) a distillation column for removing a raw material from a solution extract that is discharged from the extractor; (d) a hydrogenation reactor for hydrogenating a solution extract that is discharged from the distillation column; and (e) a divided-wall distillation column for isolating glycol from a hydrogenated solution product that is discharged from the hydrogenation reactor, wherein the hydrogenation reactor is a fixed-bed catalytic reactor that is filled with a copper-based catalyst, and a method of preparing the same.
      In accordance with the present disclosure, an economical apparatus for preparing glycol which reduces loss of a raw material and provides a high glycol yield while inhibiting generation of by-products, and a method of preparing the same are provided.
    • 本公开涉及用于产生乙二醇的设备及其方法。 更具体地说,本公开涉及用于产生二醇的装置,其包括(a)醇醛缩合反应器; (b)使用未与水混合的有机溶剂提取醛醇产物不饱和醛的提取器; (c)蒸馏塔,用于从提取器排出的溶液提取物中除去原料; (d)氢化反应器,用于氢化从蒸馏塔排出的溶液萃取物; 和(e)用于从加氢反应器排出的氢化溶液产物中分离乙二醇的分隔壁蒸馏塔,其中氢化反应器是填充有铜基催化剂的固定床催化反应器,和方法 准备相同。 根据本公开,提供了一种用于制备减少原料损失并提供高乙二醇收率同时抑制副产物生成的乙二醇的经济装置及其制备方法。