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1. 发明授权

EP0830928B1 Resin composition and mold made from such resin, for forming fibrous material 失效
标题翻译：和树脂的混合物组成的该树脂模具的用于成型的纤维材料
公开(公告)号：EP0830928B1
公开(公告)日：2002-06-26
申请号：EP97202879.9
申请日：1997-09-19
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Haruta, Yuichi , Takase, Hideaki , Watanabe, Tsuyoshi , Ukachi, Takashi
IPC分类号： B29C33/38 , B29C67/00 , B29C70/30 , G03C9/08
CPC分类号： C08F2/48 , B29C33/3842 , B29C64/135 , B29K2105/16 , C08F22/105

2. 发明公开

EP0848292A1 Photo-curable resin composition 失效
标题翻译： PhotohärtbareHarzzusammensetzung
公开(公告)号：EP0848292A1
公开(公告)日：1998-06-17
申请号：EP97203869.9
申请日：1997-12-09
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Watanabe, Tsuyoshi , Yamamura, Tetsuya , Takeuchi, Akira , Ukachi, Takashi
IPC分类号： G03F7/027 , G03F7/029 , G03C9/08
CPC分类号： G03F7/038 , G03F7/0037 , G03F7/027 , G03F7/029
摘要： A novel photo-curable resin composition capable of providing a three-dimensional object having excellent mechanical strength and high dimensional accuracy when used in a photo-fabrication process. The resin composition is also capable of providing a three-dimensional object with excellent stability in shape and properties in a photo-fabrication process. The photo-curable composition comprises:

(A) a compound represented by the formula (1)

(B) a compound having a cyclohexene oxide structure;
(C) a cationic photo-initiator;
(D) an ethylenically unsaturated monomer;
(E) a radical photo-initiator; and
(F) a polyol having three or more hydroxyl groups.
摘要翻译：一种新型光固化树脂组合物，当用于光致制造工艺时，能够提供具有优异的机械强度和高尺寸精度的三维物体。树脂组合物还能够提供在光致制造工艺中在形状和性质上具有优异稳定性的三维物体。光固化性组合物包含：（A）由式（1）表示的化合物（B）具有环氧环己烷结构的化合物; （C）阳离子光引发剂; （D）烯属不饱和单体; （E）自由基光引发剂; 和（F）具有三个或更多个羟基的多元醇。

3. 发明授权

EP0848293B1 Photo-curable resin composition 失效
标题翻译：光固化性树脂组合物
公开(公告)号：EP0848293B1
公开(公告)日：2002-07-03
申请号：EP97203870.7
申请日：1997-12-09
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Watanabe, Tsuyoshi , Yamamura, Tetsuya , Haruta, Yuichi , Ukachi, Takashi
IPC分类号： G03F7/027 , G03F7/029 , G03C9/08
CPC分类号： G03F7/029 , G03F7/0037

4. 发明授权

EP0848294B1 Photo-curable resin composition used for photo-fabrication of three-dimensional objects 无效
标题翻译： PhotohärtbareHarzzusammensetzung zur Verwendung zum Photo-Herstellen dreidimensionaler Objekte
公开(公告)号：EP0848294B1
公开(公告)日：2001-09-19
申请号：EP97203898.8
申请日：1997-12-12
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Yamamura, Tetsuya , Watanabe, Tsuyoshi , Takeuchi, Akira , Ukachi, Takashi
IPC分类号： G03F7/038 , G03F7/075 , G03C9/08
CPC分类号： G03F7/0757 , B33Y10/00 , B33Y70/00 , G03F7/0037 , G03F7/038 , G03F7/0755

5. 发明公开

EP0830928A2 Resin composition and mold made from such resin, for forming fibrous material 失效
标题翻译： Harzmischung und aus diesem Harz bestehender Formwerkzeug zur Formung von faserartigem材料
公开(公告)号：EP0830928A2
公开(公告)日：1998-03-25
申请号：EP97202879.9
申请日：1997-09-19
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Haruta, Yuichi , Takase, Hideaki , Watanabe, Tsuyoshi , Ukachi, Takashi
IPC分类号： B29C33/38 , B29C67/00 , B29C70/30
CPC分类号： C08F2/48 , B29C33/3842 , B29C64/135 , B29K2105/16 , C08F22/105
摘要： Process for the manufacture of a mold for making products from fibrous materials by performing a combination of steps of

(1) applying a thin layer of resin on a supporting stage
(2) selectively irradiating the thin layer of resin as to cure a selected part of said resin
(3) applying a further thin layer of resin, and repeating steps (2) and (3) as to obtain a three dimensional shap eof a plurality of cured layers, optionally combined with either one of the steps of washing and post-curing the three dimensional shape, as to obtain the mold, wherein the resin composition upon cure has good water resistant properties, and is preferably formulated from constituents comprises at least one photoreaction monomer at least one photoinitiator at least one filler.
摘要翻译：一种用于制造由纤维材料制造产品的模具的方法，该模具通过以下步骤的组合进行：（1）在支撑台上施加薄层树脂，选择性地照射树脂薄层，以固化所选择的部分所述树脂（3）施加另一薄层树脂，并且重复步骤（2）和（3）以获得多个固化层的三维形状，任选地与洗涤和后处理的任一步骤组合，固化三维形状以获得模具，其中固化时的树脂组合物具有良好的防水性能，并且优选由组分配制包含至少一种光反应单体至少一种光引发剂至少一种填料。

6. 发明公开

EP1213612A2 Radiation curable resin composition, manufacturing process and article made using such a composition 失效
标题翻译：下照射固化树脂组合物，制作工艺，以及由该组合物生成的对象
公开(公告)号：EP1213612A2
公开(公告)日：2002-06-12
申请号：EP01000758.1
申请日：1997-09-19
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Haruta, Yuichi , Takase, Hideaki , Ukachi, Takashi , Watanabe, Tsuyoshi
IPC分类号： G03C9/08 , G03F7/029 , C08G59/68 , B29K105/16 , B29K33/00 , B29K63/00
CPC分类号： C08F2/48 , B29C33/3842 , B29C64/135 , B29K2105/16 , C08F22/105
摘要： The resin composition of this invention is a radiation curable resin composition used for manufacturing a fibrous material forming mold by laminate fabricating using selective irradiation with light. This resin composition contains a filler dispersed in a liquid constituent comprising at least an ethylenically unsaturated monomer and a photoinitiator. The liquid constituent preferably additionnally comprises a cationic polymerizable organic compound. Preferably the filler is an inorganic filler, and it can be surface-treated with a silane. Preferably the ethylenically unsaturated monomer comprises at least a polyfunctional monomer having three or more acrylate functions. Preferably the cationic polymerizable organic compound is composed of 50% or more of an epoxy containing compound.
摘要翻译：本发明的树脂组合物是用于制造纤维材料使用选择性照射光形成由层叠体制造模具中的可辐射固化树脂组合物。该树脂组合物含有分散在液体组分至少烯属不饱和单体和光引发剂包括填料。液体组分优选additionnally包含阳离子聚合性有机化合物。优选地，所述填料是无机填料，并且可以用硅烷进行表面处理。优选地，所述烯属不饱和单体包括至少一个具有三个或更多个丙烯酸酯官能团的多官能单体。优选地，所述阳离子聚合性有机化合物是由含有环氧化合物的50％或更多。

7. 发明公开

EP0831373A3 Photo-curable resin compositions and process for preparing a resin-based mold 失效
标题翻译：用于制造树脂基模光固化性树脂组合物和过程
公开(公告)号：EP0831373A3
公开(公告)日：1999-12-29
申请号：EP97202886.4
申请日：1997-09-19
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Watanabe, Tsuyoshi , Haruta, Yuichi , Takase, Hideaki , Ukachi, Takashi
IPC分类号： G03F7/027
CPC分类号： G03F7/0037 , G03F7/027 , G03F7/038
摘要： A photo-curable resin composition suitable as a material for photo-fabricating. The composition can produce cured products with excellent mechanical strength and high heat resistance. Further disclosed is a process for fabricating a resin-based mold which provides superior molding dimensional precision and superb repetition durability. The composition comprises (A) a compound having a cyclohexene oxide structure, (B) a cationic photo-initiator, (C) an ethylenically unsaturated polymer, (D) a radical photo-initiator, and (E) spherical silica particles, and the heat distortion temperature of the cured resin produced from the photo-curable resin composition is 100°C or higher. The process comprises preparing a resin-based mold comprising a plurality of integrally laminated layers of cured resin by repeating the step of forming a cured resin layer by selectively irradiating a photo-curable material with light, wherein the photo-curable material is the above-mentioned photo-curable resin composition.

8. 发明公开

EP0830928A3 Resin composition and mold made from such resin, for forming fibrous material 失效
标题翻译：树脂混合物并从该树脂现有模具用于模制的纤维材料
公开(公告)号：EP0830928A3
公开(公告)日：1999-02-03
申请号：EP97202879.9
申请日：1997-09-19
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Haruta, Yuichi , Takase, Hideaki , Watanabe, Tsuyoshi , Ukachi, Takashi
IPC分类号： B29C33/38 , B29C67/00 , B29C70/30
CPC分类号： C08F2/48 , B29C33/3842 , B29C64/135 , B29K2105/16 , C08F22/105
摘要： Process for the manufacture of a mold for making products from fibrous materials by performing a combination of steps of
(1) applying a thin layer of resin on a supporting stage (2) selectively irradiating the thin layer of resin as to cure a selected part of said resin (3) applying a further thin layer of resin, and repeating steps (2) and (3) as to obtain a three dimensional shap eof a plurality of cured layers, optionally combined with either one of the steps of washing and post-curing the three dimensional shape, as to obtain the mold, wherein the resin composition upon cure has good water resistant properties, and is preferably formulated from constituents comprises at least one photoreaction monomer at least one photoinitiator at least one filler.

9. 发明公开

EP0848294A1 Photo-curable resin composition used for photo-fabrication of three-dimensional objects 无效
标题翻译： PhotohärtbareHarzzusammensetzung zur Verwendung zum Photo-Herstellen dreidimentionaler Objekte
公开(公告)号：EP0848294A1
公开(公告)日：1998-06-17
申请号：EP97203898.8
申请日：1997-12-12
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Yamamura, Tetsuya , Watanabe, Tsuyoshi , Takeuchi, Akira , Ukachi, Takashi
IPC分类号： G03F7/038 , G03F7/075 , G03C9/08
CPC分类号： G03F7/0757 , B33Y10/00 , B33Y70/00 , G03F7/0037 , G03F7/038 , G03F7/0755
摘要： A photocurable resin composition suitable for photo-fabrication. The resin composition capable of being promptly cured by photo-irradiation, thereby reducing fabricating time and providing cured products having excellent mechanical strength and minimized shrinkage during curing to ensure high dimensional accuracy. The composition comprises (A) an oxetane compound, (B) an epoxy compound, and (C) a cationic photo-initiator.
摘要翻译：适用于光加工的光固化树脂组合物。该树脂组合物能够通过光照射迅速固化，从而缩短制造时间并提供具有优异机械强度和固化期间最小化收缩率的固化产品，以确保高尺寸精度。组合物包含（A）氧杂环丁烷化合物，（B）环氧化合物和（C）阳离子光引发剂。

10. 发明公开

EP0831373A2 Photo-curable resin compositions and process for preparing a resin-based mold 失效
标题翻译：用于制造树脂基模光固化性树脂组合物和过程
公开(公告)号：EP0831373A2
公开(公告)日：1998-03-25
申请号：EP97202886.4
申请日：1997-09-19
申请人： DSM N.V. , JAPAN SYNTHETIC RUBBER CO., LTD. , Japan Fine Coatings Co., Ltd.
发明人： Watanabe, Tsuyoshi , Haruta, Yuichi , Takase, Hideaki , Ukachi, Takashi
IPC分类号： G03F7/027
CPC分类号： G03F7/0037 , G03F7/027 , G03F7/038
摘要： A photo-curable resin composition suitable as a material for photo-fabricating. The composition can produce cured products with excellent mechanical strength and high heat resistance. Further disclosed is a process for fabricating a resin-based mold which provides superior molding dimensional precision and superb repetition durability. The composition comprises (A) a compound having a cyclohexene oxide structure, (B) a cationic photo-initiator, (C) an ethylenically unsaturated polymer, (D) a radical photo-initiator, and (E) spherical silica particles, and the heat distortion temperature of the cured resin produced from the photo-curable resin composition is 100°C or higher. The process comprises preparing a resin-based mold comprising a plurality of integrally laminated layers of cured resin by repeating the step of forming a cured resin layer by selectively irradiating a photo-curable material with light, wherein the photo-curable material is the above-mentioned photo-curable resin composition.
摘要翻译：适合作为用于光制造的材料的光固化性树脂组合物。该组合物可以产生固化产品具有优良的机械强度和高耐热性。进一步游离缺失盘是用于制造基于树脂的模具，其提供优异的成型尺寸精度和高超的反复耐久性的方法。所述组合物包含（A）具有氧化环己烯结构的化合物，（B）阳离子光引发剂，（C）烯属不饱和聚合物，（D）自由基光引发剂，和（E）的球状二氧化硅粒子，并且从光固化性树脂组合物生产的固化树脂的热变形温度为100℃或更高。该方法包括制备基于树脂的模具通过重复通过选择性地照射光的光固化材料，worin光固化材料上形成的固化树脂层的步骤包括固化树脂整体层压层上的多个是上文提到的光固化性树脂组合物。

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