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1. 发明公开

EP2448668A2 VERFAHREN ZUR REGENERATION EINES KATALYSATORS 审中-公开
标题翻译：方法再生的催化剂
公开(公告)号：EP2448668A2
公开(公告)日：2012-05-09
申请号：EP10726478.0
申请日：2010-06-16
申请人： Evonik Oxeno GmbH
发明人： BÖING, Christian , RÖTTGER, Dirk , BUKOHL, Reiner , WINTERBERG, Markus , MASCHMEYER, Dietrich
IPC分类号： B01J23/02 , B01J23/92 , B01J38/06 , C07C1/20 , C07C1/24 , B01J21/12
CPC分类号： B01J38/06 , B01J21/12 , B01J23/02 , B01J23/92
摘要： The invention relates to a method for regenerating catalysts, containing mixed oxides from the group of alkali metals and/or alkaline earth metals, aluminum oxide and silicon oxide, characterized in that the regeneration has the following features: i) treating the catalyst in situ, ii) bringing the catalyst in contact with water, iii) treating the catalyst in a temperature range of 100 to 400°C, iv) treating the catalyst in a pressure range of 0.1 to 2 MPa, v) treating the catalyst over a time period of 0.1 to 24 h, vi) treating the catalyst with a specific catalyst load of 0.1 to 100 h
-1 .

2. 发明公开

EP2475458A1 VERFAHREN ZUR OLIGOMERISIERUNG VON OLEFINEN 有权
标题翻译： PROCEDURE烯烃齐聚
公开(公告)号：EP2475458A1
公开(公告)日：2012-07-18
申请号：EP10741985.5
申请日：2010-08-12
申请人： Evonik Oxeno GmbH
发明人： BÖING, Christian , MASCHMEYER, Dietrich , WINTERBERG, Markus , BUCHHOLZ, Stefan , MELCHER, Berthold , HAUMANN, Marco , WASSERSCHEID, Peter
IPC分类号： B01J31/30 , C07C2/32 , C10G50/00
CPC分类号： C10G50/00 , B01J21/04 , B01J21/066 , B01J21/08 , B01J21/10 , B01J21/18 , B01J21/185 , B01J31/0274 , B01J31/0279 , B01J31/0281 , B01J31/0284 , B01J31/0288 , B01J31/0292 , B01J31/143 , B01J31/2234 , B01J31/2404 , B01J31/26 , B01J35/023 , B01J35/1019 , B01J35/1042 , B01J2231/20 , B01J2231/323 , B01J2531/847 , B82Y30/00 , C07C2/32 , C07C2/36 , C07C2531/24 , C10G2300/1088 , C10G2300/70 , C10G2400/22 , C07C11/02
摘要： The invention relates to a catalyst system comprising: a) a carrier material, selected from at least one of the following materials: silicon dioxide, aluminum oxide, magnesium oxide, zirconium oxide and mixed oxides thereof, carbon nanotubes; b) an ionic fluid; c) a catalytically active compound containing nickel; d) an activator selected from the group of Lewis acids having alkylating properties. The invention further relates to the use of the catalyst systems according to the invention in the oligomerisation of unsaturated hydrocarbon mixtures.

3. 发明授权

EP2448892B1 VERFAHREN ZUR HERSTELLUNG VON GERUCHSARMEM N-BUTAN 有权转让
标题翻译：用于生产低气味正丁烷
公开(公告)号：EP2448892B1
公开(公告)日：2013-07-10
申请号：EP10720622.9
申请日：2010-05-21
申请人： Evonik Oxeno GmbH
发明人： LÜKEN, Hans-Gerd , KAIZIK, Alfred , WINTERBERG, Markus , BÜSCHKEN, Wilfried , FRIDAG, Dirk
IPC分类号： C07C7/10 , C07C7/163 , C07C9/10
CPC分类号： C07C9/10 , C07C7/10 , C07C7/163

4. 发明公开

EP2590913A1 VERFAHREN ZUR SELEKTIVEN HYDRIERUNG VON MEHRFACH UNGESÄTTIGTEN KOHLENWASSERSTOFFEN IN OLEFINHALTIGEN KOHLENWASSERSTOFFGEMISCHEN 审中-公开
标题翻译：过程在多个烯烃HC混合物不饱和烃选择性加氢
公开(公告)号：EP2590913A1
公开(公告)日：2013-05-15
申请号：EP11728795.3
申请日：2011-06-09
申请人： Evonik Oxeno GmbH
发明人： BÖING, Christian , WINTERBERG, Markus , LAIBLIN, Tobias , SCHILLING, Gunnar , GARSTKA, Wolfgang , KREIDLER, Burkard , MASCHMEYER, Dietrich , BUKOHL, Reiner
IPC分类号： C07C7/163 , C10G45/32
CPC分类号： C07C5/05 , C07C7/163 , C07C2523/44 , C10G45/32 , C10G45/40 , C07C11/08 , C07C11/10
摘要： The invention relates to a method for the parallel selective hydrogenation of unbranched, polyunsaturated C4-hydrocarbons and branched, polyunsaturated C5-hydrocarbons in hydrocarbon mixtures while minimizing hydrogenation and isomerization of the olefins present in the flow.

5. 发明公开

EP2448893A2 HERSTELLUNG VON ISOBUTEN DURCH SPALTUNG VON MTBE 有权转让
标题翻译：通过分解MTBE，现代制造异丁烯
公开(公告)号：EP2448893A2
公开(公告)日：2012-05-09
申请号：EP10725455.9
申请日：2010-06-16
申请人： Evonik Oxeno GmbH
发明人： WINTERBERG, Markus , RÖTTGER, Dirk , RIX, Armin , BUKOHL, Reiner , LUH, Walter , WIEDERHOLD, Holger , SCHILLING, Gunnar , BÖING, Christian
IPC分类号： C07C11/09
CPC分类号： C07C11/09 , C07C1/20
摘要： The invention relates to a method for producing isobutene by cracking MTBE, wherein the following steps are carried out: a) MTBE synthesis; reacting isobutene-containing hydrocarbon mixtures (II) with methanol (III), contained in one or more methanol-containing streams (VIII, IX), on acidic ion exchangers obtaining a stream (IV) containing MTBE and TBA, b) MTBE separation; separating a stream (V) containing MTBE and TBA from stream (IV) by means of distillation, c) MTBE cracking; cracking the stream (V) on a heterogenic catalyst in the gas phase, thus obtaining a stream (VI) which contains at least isobutene, methanol, MTBE, water, and optionally TBA, d) isobutene separation; separating the stream (VI) by means of distillation, thus obtaining a stream (VII) containing more than 50 mass % of the amounts of methanol, TBA, and water contained in stream (VI), and a stream (XVII) containing isobutene, e) water separation; separating, water from the stream (VII) to below 1 mass % by means of distillation, thus obtaining a stream (VIII), f) recirculating; complete or partial recirculation of the methanol-containing stream (VIII) into the MTBE synthesis. The invention further relates to a tube bundle device comprising the following elements: i) tube bundle, ii) tube bottom, iii) deflection plates, iv) inner shell, iv) pressure bearing outer shell, comprising at least one inlet and outlet, vi) shell chamber, comprising a fluid releasing or absorbing heat, characterized in that the inner shell is connected to the deflection plates attached over the length of the tube bundle without a gap, or with a small gap, and is connected to the tube bottom, wherein the fluid present in the shell chamber encloses the inner shell on both sides.

6. 发明公开

EP2435389A1 AUFBEREITUNG EINES 3-METHYL-1-BUTEN-HALTIGEN GEMISCHES 审中-公开
标题翻译： AUFBERETEUNG EINES 3-METHYL-1-BUTEN-HALTIGEN GEMISCHES
公开(公告)号：EP2435389A1
公开(公告)日：2012-04-04
申请号：EP10717632.3
申请日：2010-04-29
申请人： Evonik Oxeno GmbH
发明人： WINTERBERG, Markus , KAIZIK, Alfred , RIX, Armin , GRASS, Michael , BÜSCHKEN, Wilfried , BECKER, Marc
IPC分类号： C07C1/24 , C07C7/04 , C07C11/10
CPC分类号： C07C7/04 , C07C1/24 , C07C7/06 , C07C11/10
摘要： The invention relates to a method for preparing a mixture containing water, 3-methyl-1-butene, and at least one other methyl butene. Said method involves the provision of the mixture; the primary distillation of the mixture in order to produce a gaseous primary head product containing methyl butene and water, and a water-free primary sump product containing 3-methyl-1-butene; the condensation of the gaseous primary head product such that a condensate comprising a liquid aqueous phase and a liquid organic phase is produced; the separation of the condensate into a liquid, aqueous phase and a liquid organic phase; the ejection of the liquid aqueous phase; the reintroduction of the organic phase into the primary distillation process; and finally the secondary distillation of the water-free primary sump product of the primary distillation, such that a secondary head product consisting of 3-methyl-1-butene and a secondary sump product is produced. The secondary head product produced has a purity that enables it to be used directly as a monomer or comonomer for producing polymers or copolymers.
摘要翻译：本发明是一种处理含有水，3-甲基-1-丁烷和至少一种其它甲基丁烯的混合物的方法。该方法包括对该混合物进行一次蒸馏，得到含有甲基丁烯和水的气态主要塔顶产物和含有3-甲基-1-丁烯的无水初级底物产物; 气态一级塔顶产物的冷凝，以产生包含液态水相和液体有机相的冷凝物; 将冷凝液分离成液态水相和液体有机相; 液体水相的排出; 将有机相再循环至初级蒸馏; 最后从一次蒸馏中二次蒸馏无水初级底部产物，得到包含3-甲基-1-丁烯和二级底部产物的二级塔顶产物。获得的二次塔顶产物具有使其能够直接用作制备聚合物或共聚物的单体或共聚单体的纯度。

7. 发明公开

EP2435388A2 HERSTELLUNG VON 3-METHYLBUT-1-EN DURCH DEHYDRATISIERUNG VON 3-METHYLBUTAN-1-OL 审中-公开
标题翻译： HERSTELLUNG VON 3-METHYLBUT-1-EN DURCH DEHYDRATISIERUNG VON 3-METHLLUTUT-1-OL
公开(公告)号：EP2435388A2
公开(公告)日：2012-04-04
申请号：EP10716338.8
申请日：2010-04-28
申请人： Evonik Oxeno GmbH
发明人： KAIZIK, Alfred , QUANDT, Thomas , GRASS, Michael , WINTERBERG, Markus , BÜSCHKEN, Wilfried
IPC分类号： C07C1/24 , C07C11/10
CPC分类号： C07C1/24 , C07C11/10
摘要： The object of the invention is a method for producing 3-methylbut-1-en by means of dehydrating 3-methylbutane-1-ol at an aluminum-containing oxide in a temperature range of 200 to 450°C in the gaseous or liquid/gaseous mixture phase, characterized by an aluminum-containing oxide having mostly mesoporous pore structure is being used, which: a) relative ratio of macropores is less than 15%; b) contribution of the pore diameter has a monomodal maximum in the region of the mesopores of 3.6 to 50 nm; c) average pore diameter of all pores in the region of the meso- and macropores ranges from 5 to 20 nm; d) composition consists of gamma-aluminum oxide of more than 80%.
摘要翻译：本发明涉及通过在含有氧化铝的200〜450℃的温度范围内，在气相或混合液/液中脱水3-甲基-1-丁醇来制备3-甲基-1-丁烯的方法，气相，其特征在于具有主要介孔孔结构的含铝氧化物，其具有：a）大孔的相对比例小于15％; b）细孔直径的分布在介孔范围为3.6〜50nm的单峰最大值; c）所有孔的平均孔径在5〜20nm的介孔和大孔的范围内; d）组合物包含大于80％的γ-氧化铝。

8. 发明公开

EP2300397A2 VERFAHREN ZUR HERSTELLUNG VON ISOBUTEN DURCH SPALTUNG VON MTBE-HALTIGEN GEMISCHEN 失效转让
标题翻译：受理并MTBE，含混合物的分离PRODUCING异丁烯
公开(公告)号：EP2300397A2
公开(公告)日：2011-03-30
申请号：EP09779508.2
申请日：2009-05-19
申请人： Evonik Oxeno GmbH
发明人： WINTERBERG, Markus , RÖTTGER, Dirk , BUKOHL, Reiner , WIEDERHOLD, Holger , LUH, Walter
IPC分类号： C07C1/20 , C07C11/09
CPC分类号： C07C1/20 , C07C7/04 , C07C2521/12 , C07C2523/02 , C07C11/09
摘要： The invention relates to a process for production of isobutene from MTBE-containing mixtures which comprises the following steps a) cracking, in a reactor R, a mixture obtained from an MTBE-containing feedstock (1a) and/or an MTBE-containing stream (13, 5), delivering a stream (6) of reaction products consisting of isobutene, methanol, MTBE and also by‑products, wherein these consist of a1) high boilers having a boiling range above 55°C at a pressure of 0.1 MPa; a2) medium boilers having a boiling range from 12 to 55°C at a pressure of 0.1 MPa; and a3) low boilers having a boiling range below 12°C at a pressure of 0.1 MPa; b) separation of stream (6) by distillation into a stream (7) which contains the product isobutene and low boilers and a stream (8) which contains MTBE, methanol, medium boilers and high boilers; c) separating the stream (8) by distillation obtaining an MTBE-containing stream (10, 12) and a methanol-containing high-boiler stream (9, 11); d) recirculating an MTBE-containing stream (10, 12, 13) to step a) of the process, wherein the medium-boilers are completely or partially separated off from the medium-boiler-rich streams (10, 12) upstream of step d).

10. 发明公开

EP2630110A2 VERFAHREN ZUR AUFREINIGUNG VON MTBE-HALTIGEN GEMISCHEN SOWIE ZUR HERSTELLUNG VON ISOBUTEN DURCH SPALTUNG VON MTBE-HALTIGEN GEMISCHEN 有权
标题翻译：方法净化MTBE，含混合工和通过MTBE，含混合物的分离异丁烯生产
公开(公告)号：EP2630110A2
公开(公告)日：2013-08-28
申请号：EP11772921.0
申请日：2011-10-12
申请人： Evonik Oxeno GmbH
发明人： WINTERBERG, Markus , RÖTTGER, Dirk , RIX, Armin , BUKOHL, Reiner , BÖING, Christian
IPC分类号： C07C41/42 , C07C41/06 , C07C43/04 , C07C1/20 , C07C11/09
CPC分类号： C07C41/42 , C07C1/20 , C07C7/10 , C07C43/046 , C07C11/09
摘要： The invention relates to a method for the efficient purification of MTBE-containing mixtures and for producing isobutene by cleavage of MTBE-containing mixtures. Technical MTBE is separated by distillation into a C4- and C5-hydrocarbon-containing top product, an acetone, methanol and MTBE-containing side cut, and an MTBE-containing bottom product.

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