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1. 发明公开

EP3339334A1 PROCESS FOR PRODUCING FLUOROPOLYMER 有权转让
公开(公告)号：EP3339334A1
公开(公告)日：2018-06-27
申请号：EP16839123.3
申请日：2016-08-12
申请人： Asahi Glass Company, Limited
发明人： SAITO, Susumu , HASHIMOTO, Wakako
IPC分类号： C08F6/10
CPC分类号： C08F14/185 , C08F6/001 , C08F6/10 , C08F24/00 , C08L27/12
摘要： To provide a process for producing a fluorinated polymer having a cyclic structure at a relatively low cost, by efficiently recovering, from a mixture containing a fluorinated polymer obtained by polymerizing a perfluoromonomer having a cyclic structure and an unreacted perfluoromonomer having a cyclic structure, the unreacted perfluoromonomer having a cyclic structure.
A monomer component containing a perfluoromonomer having a specific cyclic structure is polymerized in the presence of a polymerization initiator at a predetermined polymerization temperature to obtain a mixture containing a fluorinated polymer and an unreacted cyclic structure monomer, and the perfluoromonomer having a cyclic structure is recovered from the mixture at a temperature of at most the maximum ultimate temperature of the polymerization temperature + 12°C and at most the 10 hour half-life temperature of the polymerization initiator + 12°C under a pressure of less than the atmospheric pressure.

2. 发明授权

EP2913347B1 METHOD FOR PRODUCING FLUORINATED COPOLYMER 有权转让
标题翻译：生产含氟共聚物的方法
公开(公告)号：EP2913347B1
公开(公告)日：2017-11-29
申请号：EP13851640.6
申请日：2013-10-04
申请人： Asahi Glass Company, Limited
发明人： SAITO, Susumu , ABE, Kaori , SHIMOHIRA, Tetsuji
IPC分类号： C08F6/10 , B01J39/20 , B01J47/12 , C08F214/18 , C08F216/14 , C25B13/08
CPC分类号： C08J5/225 , B01J47/12 , C08F2/00 , C08F6/003 , C08F6/008 , C08F214/18 , C08F216/1408 , C08F216/1466 , C08F2216/1475 , C08J5/22 , C08J2329/10 , C25B13/04 , C25B13/08 , C08L27/12
摘要： To provide a process by which from a mixture containing a fluorinated copolymer, an unreacted monomer and a polymerization medium, the unreacted monomer and the polymerization medium can efficiently be recovered, and a lower polymer contained in the obtainable fluorinated copolymer can readily be reduced. A process for producing a fluorinated copolymer comprising (I) a step of polymerizing a fluorinated monomer having a carboxylic acid functional group or a sulfonic acid functional group and a fluorinated olefin in a polymerization medium to obtain a mixture containing a fluorinated copolymer, the unreacted monomer and the polymerization medium, (II) a step of continuously or intermittently transferring the mixture to an evaporation container equipped with a stirring machine and heating the mixture in the evaporation container with stirring to evaporate and recover the unreacted monomer and the polymerization medium and to obtain the fluorinated copolymer, and (III) a step of washing the fluorinated copolymer with a washing medium.

3. 发明公开

EP3239189A1 ELECTROLYTE MATERIAL, LIQUID COMPOSITION, AND MEMBRANE-ELECTRODE ASSEMBLY FOR SOLID POLYMER FUEL CELL 有权转让
标题翻译：用于固体聚合物燃料电池的电解质材料，液体组合物和膜电极组件
公开(公告)号：EP3239189A1
公开(公告)日：2017-11-01
申请号：EP15872948.3
申请日：2015-12-18
申请人： Asahi Glass Company, Limited
发明人： HOMMURA, Satoru , SAITO, Susumu , WATABE, Hiroyuki
IPC分类号： C08F8/12 , C08L29/10 , H01B1/06 , H01M8/02 , H01M8/10
CPC分类号： H01M8/1039 , C08F8/12 , C08F214/184 , C08J5/2237 , C08L29/10 , H01B1/06 , H01B1/122 , H01M4/926 , H01M8/02 , H01M8/10 , H01M8/1018 , H01M2008/1095
摘要： To provide a membrane/electrode assembly excellent in the power generation characteristics in a wide temperature range and a wide humidity range; an electrolyte material suitable for a catalyst layer of the membrane/electrode assembly; and a liquid composition suitable for forming a catalyst layer of the membrane/electrode assembly.
To use an electrolyte material which is formed of a polymer (H) obtained by converting precursor groups in a polymer (F) having structural units (A) based on a perfluoromonomer having a precursor group represented by the formula (g1), structural units (B) represented by the formula (u2), and structural units (C) based on tetrafluoroethylene, wherein the proportion of the structural units (A) is from 8 to 19 mol%, the proportion of the structural units (B) is from 65 to 80 mol%, and the proportion of the structural units (C) is from 1 to 27 mol%, to ion exchange groups.
摘要翻译：为了提供在宽温度范围和宽湿度范围内的发电特性优异的膜/电极组件; 适用于膜/电极组件的催化剂层的电解质材料; 以及适用于形成膜/电极组件的催化剂层的液体组合物。为了使用由基于具有由式（g1）表示的前体基团的全氟单体的具有结构单元（A）的聚合物（F）中的前体基团转化而获得的聚合物（H）形成的电解质材料，（A）所占的比例为8〜19摩尔％，所述结构单元（B）的比例为65〜65摩尔％，所述式（u2）所示的结构单元（B）和四氟乙烯基结构单元至80摩尔％，并且结构单元（C）的比例为1至27摩尔％。

4. 发明公开

EP2104170A1 SOLID POLYMER ELECTROLYTE MEMBRANE AND MEMBRANE ELECTRODE ASSEMBLY FOR SOLID POLYMER FUEL CELL 有权转让
标题翻译：用于固体聚合物燃料电池的固体聚合物电解质膜和膜电极组件
公开(公告)号：EP2104170A1
公开(公告)日：2009-09-23
申请号：EP07860256.2
申请日：2007-12-26
申请人： Asahi Glass Company, Limited
发明人： HONMURA, Satoru , SHIMOHIRA, Tetsuji , SAEKI, Takashi , SAITO, Susumu
IPC分类号： H01M8/02 , C08F8/26 , C08J5/22 , H01B1/06 , H01M8/10
CPC分类号： H01M8/04126 , H01M4/92 , H01M4/926 , H01M8/1004 , H01M8/1023 , H01M8/1039
摘要： A membrane/electrode assembly for a polymer electrolyte fuel cell capable of exhibiting high power generation performance constantly for a long period of time in a high temperature and low humidity environment, and a polymer electrolyte membrane whereby such a membrane/electrode assembly is obtainable.
A polymer electrode membrane 15, comprising a proton conductive polymer which has an electrical conductivity of at least 0.07 S/cm at a temperature of 80°C at a relative humidity of 40% and which has a water content of less than 15 mass; and a membrane/electrode assembly 10 comprising an anode 13 and a cathode 14 each having a catalyst layer 11, and a polymer electrolyte membrane 15 disposed between the anode 13 and the cathode 14.
摘要翻译：本发明提供一种高分子电解质型燃料电池用膜电极接合体及高分子电解质膜，其能够在高温低湿环境下长时间持续发挥高的发电性能，并且能够得到这样的膜电极接合体。聚合物电极膜15包含质子传导性聚合物，该质子传导性聚合物在80℃的温度和40％的相对湿度下具有至少0.07S / cm的电导率并且具有小于15质量的水含量; 以及包括均具有催化剂层11的阳极13和阴极14以及设置在阳极13和阴极14之间的聚合物电解质膜15的膜电极组件10。

5. 发明公开

EP3239215A1 METHOD FOR MANUFACTURING FLUORINE-CONTAINING POLYMER PARTICLES 有权转让
标题翻译：制备含氟聚合物颗粒的方法
公开(公告)号：EP3239215A1
公开(公告)日：2017-11-01
申请号：EP15872947.5
申请日：2015-12-18
申请人： Asahi Glass Company, Limited
发明人： SAITO, Susumu , HASHIMOTO, Wakako , SHIMOHIRA, Tetsuji , HAMAZAKI, Kazuo , OTSUGU, Satoshi , MATOBA, Hiroki
IPC分类号： C08J3/16 , C08F6/12
CPC分类号： C08F6/12 , C08F2/06 , C08F6/003 , C08J3/16 , C08L27/12
摘要： To provide a method capable of producing fluorinated polymer particles in which formation of fine particles or formation of large aggregates is sufficiently suppressed even in the case of a fluorinated polymer having high solubility in a solvent.
The method comprises the following steps (i) and (ii), being a method for producing particles of a fluorinated polymer (A) which has either one or both of structural units (u1) derived from tetrafluoroethylene and structural units (u2) having no sulfonic acid type functional group and having a cyclic structure and fluorine atoms, and which has structural units (u3) having a sulfonic acid type functional group, wherein the proportion of the structural units (u1) is from 0 to 82 mol% in all structural units (100 mol%) in the fluorinated polymer (A):
(i) a step of preparing solution or dispersion of the fluorinated polymer (A) having the above fluorinated polymer (A) dissolved or dispersed in a solvent (B), wherein the following conditions (i-1) and (i-2) are satisfied:
(i-1) the solvent (B) contains a good solvent (B2) wherein the solubility of the fluorinated polymer (A) is at least 30%,
(i-2) even when the above solution or dispersion of the fluorinated polymer (A) is passed through a filter of 200 mesh made of stainless steel, no residue remains on the filter,

(ii) a step of mixing the above solution or dispersion of the fluorinated polymer (A) and a solvent (C) to aggregate the fluorinated polymer (A) to form particles of the fluorinated polymer (A), wherein the following conditions (ii-1) to (ii-3) are satisfied:
(ii-1) the solvent (C) contains a poor solvent (C1) whereby the degree of swelling of the fluorinated polymer (A) is at most 100%,
(ii-2) the degree of swelling of the fluorinated polymer (A) by a mixed solvent (BC) of the solvent (B) and the solvent (C) is from 70 to 250%,
(ii-3) the ratio of the mass (Wc) of the solvent (C) to the mass (W B ) of the solvent (B) is from 1 to 5.
摘要翻译：本发明提供一种即使在溶剂中溶解性高的含氟聚合物的情况下也能够充分抑制微粒的形成或大的聚集体的形成的含氟聚合物粒子的制造方法。该方法包括以下步骤（i）和（ii），其是具有衍生自四氟乙烯的结构单元（u1）和不具有来自四氟乙烯的结构单元（u1）中的任一个或两个的结构单元（u2）的含氟聚合物磺酸型官能团并且具有环状结构和氟原子，并且具有磺酸型官能团的结构单元（u3），其中结构单元（u1）的比例在全部结构中为0至82摩尔％含氟聚合物（A）中的单元（100摩尔％）：（i）将含有上述含氟聚合物（A）的含氟聚合物（A）溶解或分散于溶剂（B）中而得到的含氟聚合物（A）满足下述条件（i-1）和（i-2）：（i-1）溶剂（B）含有氟系聚合物（A）的溶解度为30％以上的良溶剂（i-2）即使上述含氟聚合物（A）的溶液或分散体通过a （ii）将上述含氟聚合物（A）的溶液或分散液与溶剂（C）混合，使含氟聚合物（A）与聚合物（ii）含有下述条件（ii-1）〜（ii-3）的氟化聚合物（A）的粒子，（ii-1）溶剂（C）含有不良溶剂（B）与溶剂（C）的混合溶剂（BC）的含氟聚合物（A）的溶胀度为100％以下，（ii-2）含氟聚合物（ii-3）溶剂（C）的质量（Wc）与溶剂（B）的质量（WB）的比例为1〜5。

6. 发明授权

EP2896977B1 PLASTIC OPTICAL FIBER AND METHOD FOR ITS PRODUCTION 有权转让
标题翻译：塑料光纤及其生产方法
公开(公告)号：EP2896977B1
公开(公告)日：2017-08-16
申请号：EP13836368.4
申请日：2013-08-30
申请人： Asahi Glass Company, Limited
发明人： TANAKA, Toshiyuki , KASAHARA, Nobuyuki , SATO, Masakuni , YAMAMOTO, Hiroshi , SAITO, Susumu , SHIMOHIRA, Tetsuji , TAKANO, Yoshinobu , OTA, Naoto
IPC分类号： G02B6/00
CPC分类号： G02B6/02038 , B29C47/0004 , B29C47/0014 , B29C47/0057 , B29C47/065 , B29C47/92 , B29C2947/92704 , B29K2027/12 , B29L2011/0075 , G02B1/046 , G02B1/048 , G02B6/036 , C08L27/12 , C08L29/10

7. 发明授权

EP2460835B1 ELECTROLYTE MATERIAL, LIQUID COMPOSITION, AND MEMBRANE -ELECTRODE ASSEMBLY FOR POLYMER ELECTROLYTE FUEL CELL 有权转让
标题翻译：电解质材料，液体组成和膜电极组件燃料电池聚合物电解质
公开(公告)号：EP2460835B1
公开(公告)日：2014-06-25
申请号：EP10804324.1
申请日：2010-07-22
申请人： Asahi Glass Company, Limited
发明人： HOMMURA, Satoru , SAITO, Susumu , SHIMOHIRA, Tetsuji , WATAKABE, Atsushi
IPC分类号： C08F214/18 , C25B9/10 , H01B1/06 , H01M4/86 , H01M8/10
CPC分类号： C08F214/182 , H01B1/122 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M8/1081 , Y02P70/56

8. 发明授权

EP2368920B1 PROCESS FOR PRODUCING FLUOROPOLYMER PARTICLES 有权转让
标题翻译：用于生产含氟聚合物颗粒
公开(公告)号：EP2368920B1
公开(公告)日：2014-06-25
申请号：EP09834743.8
申请日：2009-12-15
申请人： Asahi Glass Company, Limited
发明人： SAITO, Susumu , SHIMOHIRA, Tetsuji , SAEKI, Takashi , TAYANAGI, Junichi
IPC分类号： C08F2/04 , C08F6/12 , C08F6/00 , C08F6/22 , C08F6/24 , C08F6/20 , C08L27/12 , C08F14/18
CPC分类号： C08F6/24 , C08F6/001 , C08F6/003 , C08F6/12 , C08F6/20 , C08F6/22 , C08F14/18 , C08L27/12 , C08F2/04

9. 发明公开

EP2460835A1 ELECTROLYTE MATERIAL, LIQUID COMPOSITION, AND MEMBRANE -ELECTRODE ASSEMBLY FOR POLYMER ELECTROLYTE FUEL CELL 有权转让
标题翻译： LE LE LE LE LE
公开(公告)号：EP2460835A1
公开(公告)日：2012-06-06
申请号：EP10804324.1
申请日：2010-07-22
申请人： Asahi Glass Company, Limited
发明人： HOMMURA, Satoru , SAITO, Susumu , SHIMOHIRA, Tetsuji , WATAKABE, Atsushi
IPC分类号： C08F214/18 , C25B9/10 , H01B1/06 , H01M4/86 , H01M8/10
CPC分类号： C08F214/182 , H01B1/122 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M8/1081 , Y02P70/56
摘要： It is to provide a membrane/electrode assembly excellent in the power generation characteristics under low or no humidity conditions and under high humidity conditions, and an electrolyte material suitable for a catalyst layer of the membrane/electrode assembly.
It is to use an electrolyte material, which comprises a polymer (H) having ion exchange groups converted from precursor groups in a polymer (F) having repeating units (A) having a precursor group represented by the formula (g1) and repeating units (B) based on a perfluoromonomer having a 5-membered ring, and having a density of at most 2.03 g/cm 3 , the polymer (H) having an ion exchange capacity of from 1.3 to 2.3 meq/g dry resin:

wherein Q 1 and Q 2 are a perfluoroalkylene group having an etheric oxygen atom, or the like, and Y is F or the like.
摘要翻译：本发明提供一种在低或无湿度条件下和高湿度条件下发电特性优异的膜/电极组件和适用于膜/电极组件的催化剂层的电解质材料。使用电解质材料，其包含在具有由式（g1）表示的前体基团和重复单元（重复单元）的重复单元（A）的聚合物（F）中由前体基团转化的离子交换基团的聚合物（H） B）基于具有5元环的全氟单体，密度为2.03g / cm 3以下，聚合物（H）的离子交换容量为1.3〜2.3meq / g干树脂：其中Q 1 Q 2为具有醚性氧原子的全氟亚烷基等，Y为F等。

10. 发明公开

EP2107073A1 POLYMER, SOLID POLYMER ELECTROLYTE MEMBRANE FOR SOLID POLYMER FUEL CELL, AND MEMBRANE ELECTRODE ASSEMBLY 有权转让
标题翻译：聚合物，FESTSTOFFPOLYMER-ELEKTROLYTMEMBRANFÜREINE FESTSTOFFPOLYMERBRENNSTOFFZELLE UND MEMBRAN-ELEKTRODEN-ANORDNUNG
公开(公告)号：EP2107073A1
公开(公告)日：2009-10-07
申请号：EP08703934.3
申请日：2008-01-25
申请人： Asahi Glass Company, Limited
发明人： SHIMOHIRA, Tetsuji , HAMAZAKI, Kazuo , SAITO, Susumu , HOMMURA, Satoru , KOTERA, Seigo
IPC分类号： C08F216/14 , H01B1/06 , H01M8/02 , H01M8/10
CPC分类号： H01B1/122 , C08F20/22 , C08F20/38 , C08F214/18 , C08J5/2237 , C08J2327/12 , H01M8/1023 , H01M8/1039 , H01M2300/0082
摘要： To provide a polymer electrolyte membrane for polymer electrolyte fuel cells, which has a low electrical resistance, high heat resistance and is strong against repeats of swelling and shrinkage; and a membrane/electrode assembly having high power generation performance and excellent in durability.
For a polymer electrolyte membrane 15, a polymer comprising units (U1) and units (U2) is used:

Q 1 , Q 2 , Q 3 : a perfluoroalkylene group or the like; R f1 , R f2 : a perfluoroalkyl group; X 1 , X 2 : an oxygen atom or the like; a, b: 0 or the like; Y 1 , Y 2 : a fluorine atom or the like; and s, t: 0 to 1.
摘要翻译：为了提供一种聚合物电解质燃料电池用聚合物电解质膜，它具有低的电阻，高的耐热性，并且强烈的反应膨胀和收缩; 以及具有高发电性能并且耐久性优异的膜/电极组件。对于聚合物电解质膜15，使用包含单元（U1）和单元（U2）的聚合物：Q 1，Q 2，Q 3：全氟亚烷基等; R f1，R f2：全氟烷基; X 1，X 2：氧原子等; a，b：0等; Y 1，Y 2：氟原子等; 和s，t：0至1。

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