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2. 发明公开

EP2554537A4 METHOD FOR PRODUCING CARBAMATE COMPOUND, CARBAMATE COMPOUND, AND METHOD FOR PRODUCING ISOCYANATE COMPOUND USING SAME 审中-公开
标题翻译：制造方法氨基甲酸酯，氨基甲酸盐和工艺SO制备异氰酸酯
公开(公告)号：EP2554537A4
公开(公告)日：2015-08-05
申请号：EP11765331
申请日：2011-03-15
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , NAGASAKI YUKO , OKAMOTO HIDEKAZU
IPC分类号： C07C269/04 , C07C263/04 , C07C265/14 , C07C271/20 , C07C271/24
CPC分类号： C07C271/24 , C07C263/04 , C07C269/04 , C07C271/20 , C07C2601/14 , C07C265/14
摘要： The present invention relates to a method of producing a carbamate compound, comprising reacting a fluorine-containing carbonic diester compound represented by formula (1) and a non-aromatic diamine compound represented by formula (2) without using a catalyst, to thereby produce a carbamate compound represented by formula (3), and a method of producing an isocyanate compound represented by formula (20) from the carbamate compound without using a catalyst, wherein R represents a fluorine-containing monovalent aliphatic hydrocarbon group, and A represents a divalent aliphatic hydrocarbon group, a divalent alicyclic hydrocarbon group or a divalent aromatic-aliphatic hydrocarbon group. [Chem. 2] €ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒH 2 N-A-NH 2 €ƒ€ƒ€ƒ€ƒ€ƒ(2) [Chem. 4] €ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒ€ƒO=C=N-A-N=C=O€ƒ€ƒ€ƒ€ƒ€ƒ(20)
摘要翻译：本发明涉及一种制备氨基甲酸酯化合物，该方法包括使由下式表示的含氟的碳酸二酯化合物（1）和（2）不使用催化剂由下式表示的非芳族二胺化合物，从而制造的方法由式（3）表示的氨基甲酸酯化合物，以及在从所述氨基甲酸酯化合物由式（20）表示的异氰酸酯化合物的制造不使用催化剂的方法，worinřdarstellt一价的含氟脂肪烃基，并且A darstellt二价脂族烃基，二价脂环族烃基或二价芳族 - 脂族烃基。 [化学式 2]ƒ€€€ƒƒƒ€€€ƒƒƒ€€ƒh2 N-A-NH 2€€ƒƒƒ€€ƒƒ€（2）[化学式 4]ƒ€€€ƒƒƒ€€€ƒƒƒ€€ƒO= C = N-A-N = C = Oƒ€€€ƒƒƒ€€ƒ（20）

3. 发明公开

EP1679298A4 FLUORINE-CONTAINING ETHER COMPOUND 审中-公开
标题翻译： FLUORHALTIGE ETHERVERBINDUNG
公开(公告)号：EP1679298A4
公开(公告)日：2006-11-02
申请号：EP04793259
申请日：2004-10-29
申请人： ASAHI GLASS CO LTD
发明人： IWAYA MASAO , OHARU KAZUYA , TAKAGI HIROKAZU , OKAMOTO HIDEKAZU
IPC分类号： C07C43/12 , C09K5/00
CPC分类号： C09K5/00
摘要： Disclosed is a novel fluorine-containing ether compound which is useful as an inert medium. Specifically disclosed is a compound represented by the formula (1) below, such as a compound represented by the formula (1a) below or a compound represented by the formula (1b) below. R OCFR CFR OR (1) F(CF2)4OCF(CF3)CF(CF3)O(CF2)4F (1a) F(CF2)6OCF(CF3)CF(CF3)O(CF2)6F (1b) In the formula (1), R represents a straight-chain perfluoroalkyl group having 4-7 carbon atoms and R represents a fluorine atom or a trifluoromethyl group.

4. 发明公开

EP1462435A4 PROCESS FOR PRODUCING DIENE COMPOUND 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VON DIENVERBINDUNGEN
公开(公告)号：EP1462435A4
公开(公告)日：2006-05-03
申请号：EP02790732
申请日：2002-12-12
申请人： ASAHI GLASS CO LTD
发明人： IWAYA MASAO , OKAMOTO HIDEKAZU , OHARU KAZUYA
IPC分类号： C07C17/361 , C07C41/44 , C07C43/17 , C07C51/58 , C08F16/32 , C08F36/20 , C07C21/19 , C07C45/51 , C07C49/227
CPC分类号： C08F36/20 , C07C17/361 , C07C41/44 , C07C51/58 , C08F16/32 , C07C21/18 , C07C57/76 , C07C57/66 , C07C43/17
摘要： A specific diene compound (1) having high-purity is obtained, without using any special reagent or complicated technique, from a mixture of the diene compound (1) and a compound (2) which is difficult to separate by distillation and has the same molecular weight and molecular formula as the compound (1). The method comprises treating a mixture comprising CR1R2=CR3CFR4CR5R6OCR7=CR8R9 (1) and CFR1R2CR3=CR4CR5R6OCR7=CR8R9 (2) to cause the compound (2) to undergo the Claisen rearrangement and then separating the diene compound (1) from the product of the Claisen rearrangement. Alternatively, it comprises conducting the Claisen rearrangement, converting the product of the Claisen rearrangement into a derivative, and then separating the diene compound (1) from the derivative. In the formulae, R1 to R9 each is fluorine, etc.
摘要翻译：由二烯化合物（1）和难以通过蒸馏分离的化合物（2）的混合物得到高纯度的特定二烯化合物（1），而不使用任何特殊的试剂或复杂的技术，并具有相同的分子量和分子式作为化合物（1）。该方法包括处理包含CR1R2 = CR3CFR4CR5R6OCR7 = CR8R9（1）和CFR1R2CR3 = CR4CR5R6OCR7 = CR8R9（2）的混合物，以使化合物（2）进行克莱森重排，然后将二烯化合物（1）从克莱森重排。或者，它包括进行克莱森重排，将克莱森重排产物转化为衍生物，然后将二烯化合物（1）与衍生物分离。式中，R1至R9各自为氟等。

5. 发明公开

EP3109303A4 COMPOSITION FOR HEAT CYCLE SYSTEM, AND HEAT CYCLE SYSTEM 有权转让
公开(公告)号：EP3109303A4
公开(公告)日：2017-12-27
申请号：EP15752553
申请日：2015-02-19
申请人： ASAHI GLASS CO LTD
发明人： FUJII KATSUYA , YAMAMOTO HIROSHI , UENO KATSUYA , OKAMOTO HIDEKAZU , FUKUSHIMA MASATO , MITSUOKA HIROAKI , TASAKA MAI
IPC分类号： C10M171/02 , C09K5/04 , C10M105/38 , C10M107/24 , C10N20/00 , C10N20/02 , C10N30/04 , C10N30/06 , C10N30/10 , C10N40/30
CPC分类号： C09K5/045 , C09K2205/122 , C09K2205/126 , C09K2205/22 , C10M105/04 , C10M105/18 , C10M105/36 , C10M105/38 , C10M105/52 , C10M171/008 , C10M2203/024 , C10M2205/0285 , C10M2207/0406 , C10M2207/2825 , C10M2207/2835 , C10M2209/105 , C10M2209/1075 , C10M2209/1085 , C10M2211/0225 , C10M2213/043 , C10N2220/302 , C10N2240/30 , F25B31/002 , F25B43/00 , F25B2500/222
摘要： To provide a composition for a heat cycle system having less influence over the ozone layer, having a low global warming potential and having excellent durability, and a heat cycle system. A composition for a heat cycle system comprising a working fluid containing trifluoroethylene and difluoromethane, and a lubricating oil, wherein the interaction distance (Ra 1123 ) between trifluoroethylene and the lubricating oil as determined from the Hansen solubility parameters is shorter than the interaction distance (Ra 32 ) between difluoromethane and the lubricating oil.

6. 发明公开

EP3100998A4 METHOD FOR PRODUCING TRIFLUOROETHYLENE 有权转让
标题翻译： VERFAHREN ZUR HERSTELLUNG VON TRIFLUOR乙炔
公开(公告)号：EP3100998A4
公开(公告)日：2017-08-23
申请号：EP15743584
申请日：2015-01-29
申请人： ASAHI GLASS CO LTD
发明人： NAKAMURA MASAHIKO , OKAMOTO HIDEKAZU
IPC分类号： C07C17/25 , C07C21/18
CPC分类号： C07C17/25 , B01J8/1818 , B01J8/1827 , B01J23/02 , B01J27/232 , B01J2208/0007 , B01J2208/00407 , B01J2208/00415 , C09K5/045 , C09K2205/126 , C07C21/18
摘要： To produce trifluoroethylene stably with a high selectivity by reacting 1,1,1,2-tetrafluoroethane with a solid reactant efficiently while formation of by-products such as polymer carbon is suppressed. A material gas containing 1,1,1,2-tetrafluoroethane is made to flow through a layer consisting of a particulate solid reactant having an average particle size of from 1 µm to 5,000 µm to bring the solid reactant and 1,1,1,2-tetrafluoroethane into contact with each other in a state where the layer consisting of the solid reactant is fluidized.
摘要翻译：通过使1,1,1,2-四氟乙烷与固体反应物高效地反应，同时抑制聚合物碳等副产物的生成，以高选择率稳定地制造三氟乙烯。使包含1,1,1,2-四氟乙烷的原料气体流过由平均粒径为1μm〜5000μm的颗粒状固体反应物构成的层，使固体反应物和1,1,1， 2-四氟乙烷在由固体反应物构成的层流动的状态下彼此接触。

7. 发明公开

EP2371793A4 PROCESSES FOR PRODUCTION OF 1,1-DICHLORO-2,3,3,3-TETRA- FLUOROPROPENE AND 2,3,3,3-TETRAFLUOROPROPENE 有权
标题翻译：用于生产1,1-二氯2,3,3,3-四氟丙烷和2,3,3,3-四氟丙烯
公开(公告)号：EP2371793A4
公开(公告)日：2012-08-01
申请号：EP09835050
申请日：2009-12-25
申请人： ASAHI GLASS CO LTD
发明人： OKAMOTO HIDEKAZU , SASAO YASUYUKI
IPC分类号： C07C17/25 , C07B61/00 , C07C17/23 , C07C21/18
CPC分类号： C07C17/23 , C07C17/25 , C07C21/18
摘要： To provide a simple and economical process for producing 1,1-dichloro-2,3,3,3-tetrafluoropropene, which does not require purification of the raw material component obtained in the form of a mixture of isomers, and a process for producing 2,3,3,3-tetrafluoropropene from the product thereby obtained. A process for producing 1,1-dichloro-2,3,3,3-tetrafluoropropene, characterized by bringing a mixture of dichloropentafluoropropane isomers which contains 1,1-dichloro-2,2,3,3,3-pentafluoropropane into contact with an aqueous alkali solution in the presence of a phase transfer catalyst, and thereby selectively dehydrofluorinating only the 1,1-dichloro-2,2,3,3,3-pentafluoropropane in the mixture, and a process for producing 2,3,3,3-tetrafluoropropene from the 1,1-dichloro-2,3,3,3-tetrafluoropropene thereby obtained.

8. 发明公开

EP1655278A4 METHOD FOR PRODUCING FLUORINE-CONTAINING ALKYL ETHER 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VON FLUORHALTIGEM ALKYLETHER
公开(公告)号：EP1655278A4
公开(公告)日：2006-11-29
申请号：EP04771338
申请日：2004-08-06
申请人： ASAHI GLASS CO LTD
发明人： NAGAI MASAZUMI , OKAMOTO HIDEKAZU , OHARU KAZUYA
IPC分类号： C07C41/06 , C07C43/12
CPC分类号： C07C41/06 , C07C43/123
摘要： A method for producing a fluorine-containing alkyl ether is disclosed wherein a sufficient reaction rate can be attained even under mild conditions. This method enables to efficiently perform post-processes such as distillation following the reaction. After introducing a polar non-protic solvent, a fluorine-containing ether, a catalyst, a fluorine-containing alkyl alcohol and a fluorinated olefin into a reaction vessel, the fluorine-containing alkyl alcohol and the fluorinated olefin are reacted with each other so as to produce a fluorine-containing alkyl ether. In this method for producing a fluorine-containing alkyl ether, the mass ratio between the polar non-protic solvent and the fluorine-containing ether introduced in the reaction vessel (polar non-protic solvent/fluorine-containing ether) is from 5/95 to 80/20.
摘要翻译：公开了一种制备含氟烷基醚的方法，其中即使在温和条件下也可以获得足够的反应速率。该方法能够有效地进行反应后的蒸馏等后处理。向反应容器内导入极性非质子性溶剂，含氟醚，催化剂，含氟烷基醇和氟化烯烃后，使含氟烷基醇和氟化烯烃反应生成含氟烷基醚。在该含氟烷基醚的制造方法中，反应容器中导入的极性非质子性溶剂与含氟醚的质量比（极性非质子性溶剂/含氟醚）为5/95 到80/20。

9. 发明公开

EP1630151A4 METHOD FOR PRODUCING FLUORINE-CONTAINING ALKYL ETHER 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VON FLUORHALTIGEM ALKYLETHER
公开(公告)号：EP1630151A4
公开(公告)日：2006-10-11
申请号：EP04735982
申请日：2004-06-03
申请人： ASAHI GLASS CO LTD
发明人： OKAMOTO HIDEKAZU , NAGAI MASAZUMI , OHARU KAZUYA
IPC分类号： C07C41/06 , C07C43/12
CPC分类号： C07C41/06 , C07C43/123
摘要： A method for producing a fluorine-containing alkyl ether wherein a fluorine-containing alkyl alcohol and a fluorinated olefin are reacted in the presence of a solvent and a catalyst is characterized in that the fluorine-containing alkyl alcohol and the fluorinated olefin are continuously supplied into a reaction chamber, a reaction product including the fluorine-containing alkyl alcohol is continuously drawn out from the reaction chamber, and the reaction is conducted while keeping the concentration of the fluorine-containing alkyl alcohol in the reaction chamber at 7 mass% or less relative to the total organic component existent in the reaction chamber. With this method, a high-purity fluorine-containing alkyl ether can be produced at high reaction rate on an industrial scale.
摘要翻译：在溶剂和催化剂存在下使含氟烷基醇和氟化烯烃反应的含氟烷基醚的制造方法，其特征在于，将含氟烷基醇和氟化烯烃连续供给在反应室内连续地从反应室中取出含有含氟烷基醇的反应产物，一边将反应室内的含氟烷基醇的浓度保持在7质量％以下，一边进行反应到存在于反应室中的全部有机组分。用这种方法，可以在工业规模上以高反应速率生产高纯度的含氟烷基醚。

10. 发明公开

EP1300386A4 METHOD FOR PRODUCING FLUORINE-CONTAINING COMPOUND 有权
标题翻译：用于生产含氟化合物
公开(公告)号：EP1300386A4
公开(公告)日：2005-10-05
申请号：EP01947976
申请日：2001-07-11
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , TATEMATSU SHIN , ITO MASAHIRO , SHIRAKAWA DAISUKE , IWAYA MASAO , OKAMOTO HIDEKAZU
IPC分类号： C07C51/58 , C07C55/40 , C07C59/135 , C07C67/307 , C07C69/63 , C07C69/708 , C07C41/18 , C07C43/17 , C07C67/287
CPC分类号： C07C69/708 , C07C51/58 , C07C55/40 , C07C59/135 , C07C67/307 , C07C69/63
摘要： A method for producing a fluorine-containing compound, characterized in that a compound (1) is reacted with a compound (2) to produce a compound (3) having a fluorine content of 30 mass % or more, the compound (3) is fluorinated in a liquid phase to produce a compound (4), and a compound (5) and/or a compound (6) are produced through the cleavage reaction of an ester bonding of the compound (4): HOCH2-RA-CH2OH (1), XCOR?B (2), RBCOOCH¿2-RA-CH2OCOR?B (3), RBFCOOCH¿2-RAF-CF2OCORBF (4), FCO-RAF-COF (5), RBF-COF (6).

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