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    • 2. 发明公开
    • METHOD FOR PRODUCING ZIRCONIA SINTERED COMPACT
    • EP4219425A1
    • 2023-08-02
    • EP21872581.0
    • 2021-09-24
    • Kuraray Noritake Dental Inc.
    • MATSUURA, Atsushi
    • C04B35/486A61C5/70A61C13/083C04B35/64
    • The present invention provides a method of production of a zirconia sintered body by which a zirconia molded body or zirconia pre-sintered body having a plurality of layers containing different amounts of stabilizer is sintered in a short time period to produce a zirconia sintered body having hardly noticeable stripes between layers differing in yttria content. The present invention relates to a method for producing a zirconia sintered body, comprising a firing step of firing a zirconia molded body or a zirconia pre-sintered body,
      the zirconia molded body or the zirconia pre-sintered body comprising a plurality of layers containing a stabilizer,
      the plurality of layers including layers having different stabilizer contents,
      the firing step comprising at least three stages of temperature-increasing process including a first temperature-increasing step (H1), a second temperature-increasing step (H2), and a third temperature-increasing step (H3),
      the method satisfying HR2 = more than 0°C/min and less than 50°C/min, HR3 = 5 to 150°C/min, and HR3/HR2 > 1, where HR2 is a rate of temperature increase in H2, and HR3 is a rate of temperature increase in H3,
      the temperature-increasing process having start temperatures that are 1,000°C or less in H1, more than 1,250°C and 1,450°C or less in H2, and 1,450°C or more and 1,550°C or less in H3,
      the temperature-increasing process having end temperatures that are more than 1,250°C and 1,450°C or less in H1, 1,450°C or more and 1,550°C or less in H2, and 1,500°C or more and 1,750°C or less in H3.
    • 6. 发明公开
    • CURABLE COMPOSITION FOR DENTISTRY
    • EP4032522A1
    • 2022-07-27
    • EP20865424.4
    • 2020-09-18
    • Kuraray Noritake Dental Inc.
    • KAJIKAWA, TatsuyaHORIGUCHI, Hirotaka
    • A61K6/884A61K6/889
    • The present invention provides a dental curable composition, suited for applications such as dental composite resins, having a small polymerization shrinkage stress and a consistency to easily fill cavities, and that, in the form of a cured product, has excellent mechanical strength with low water absorbency while causing reduced wear on opposing teeth. The present invention relates to a dental curable composition comprising a polymerizable monomer (A), a filler (B), and a polymerization initiator (C),
      the polymerizable monomer (A) containing a polyfunctional (meth)acrylic monomer (A-1) having no aromatic ring but having a moiety (X) constituted by an alkoxylene repeating unit having 1 to 15 carbon atoms, and a polyfunctional (meth)acrylic monomer (A-2) having an aromatic ring but no hydroxyl group,
      the moiety (X) having a C/O of 2.5 to 10 as a ratio of a total number of carbon atoms and a total number of oxygen atoms in the moiety (X),
      the moiety (X) having a backbone with a total of 25 to 60 constituent carbon atoms and oxygen atoms altogether,
      the polyfunctional (meth)acrylic monomer (A-1) being 3 to 60 parts by mass in 100 parts by mass of the polymerizable monomer (A).
    • 7. 发明公开
    • METHOD FOR PRODUCING ZIRCONIA SINTERED COMPACT
    • EP4008699A1
    • 2022-06-08
    • EP20848494.9
    • 2020-07-31
    • Kuraray Noritake Dental Inc.
    • SAKAMOTO, HiroyukiKATO, ShinichiroMATSUURA, Atsushi
    • C04B35/486A61K6/818
    • The present invention provides a method that is for producing a zirconia sintered body and by which a zirconia molded body or a zirconia pre-sintered body is sintered in a short period of time, the zirconia sintered body reproducing an aesthetic requirement and strength of an ideal dental prosthesis at the same levels as those of a zirconia sintered body obtained by general firing. The present invention relates to a method for producing a zirconia sintered body, comprising a step of firing a zirconia molded body or a zirconia pre-sintered body, wherein: the firing step comprises at least three temperature increase steps including a first temperature increase step (H1), a second temperature increase step (H2), and a third temperature increase step (H3); a temperature increase rate in the first temperature increase step (H1) is defined as HR1, a temperature increase rate in the second temperature increase step (H2) is defined as HR2, and a temperature increase rate in the third temperature increase step (H3) is defined as HR3; HR1 = 50 to 500°C/min, HR2 = 11 to 300°C/min, HR3 = 10 to 299°C/min, HR1 > HR2, and HR2/HR3 > 1 are satisfied; starting temperatures in the temperature increase steps are room temperature to 500°C in H1, 900 to 1250°C in H2, and 1300 to 1550°C in H3; and reaching temperatures in the temperature increase steps are 900 to 1250°C in H1, 1300 to 1550°C in H2, and 1400 to 1650°C in H3.