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1. 发明公开

EP3266816A1 FLAME-RETARDANT ENGINEERING PLASTIC AND PREPARATION METHOD THEREOF 审中-公开
标题翻译：阻燃工程塑料及其制备方法
公开(公告)号：EP3266816A1
公开(公告)日：2018-01-10
申请号：EP17160234.5
申请日：2017-03-10
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C08K5/5399 , C08L69/00
CPC分类号： C08L69/00 , C08K5/5399 , C08L55/02 , C08L63/00 , C08L2201/02 , C08L2205/03 , C09K21/12
摘要： The present invention provides a flame-retardant engineering plastic and a preparation method thereof. The flame-retardant engineering plastic contains a halogen-free flame retardant represented by the formula I as a component of raw materials. The addition of the flame retardant gives good flame retardancy and excellent mechanical properties to the engineered plastic. The engineering plastic is prepared by the raw materials comprising the following components in parts by mass: 40-60 parts of PC, 20-40 parts of epoxy resin, 10-20 parts of ABS and 5-15 parts of flame retardant. The engineering plastic prepared by the present invention has a bending strength which can be up to 82.4-84 MPa, a tensile strength of up to 65.7-66.6 MPa, a notched impact strength of up to 26.3-27 J/m, a melt index of 12.6-15, and an oxygen index of 26.2-27.5%, and thus has excellent mechanical properties and good flame retardancy.
摘要翻译：本发明提供一种阻燃工程塑料及其制备方法。该阻燃工程塑料含有由式I表示的无卤阻燃剂作为原料的组分。添加阻燃剂为工程塑料提供了良好的阻燃性和优异的机械性能。本发明的工程塑料是由下述组分组成的原料制成的：PC40-60份，环氧树脂20-40份，ABS10-20份，阻燃剂5-15份。本发明制备的工程塑料的弯曲强度可高达82.4-84MPa，拉伸强度高达65.7-66.6MPa，缺口冲击强度高达26.3-27J / m，熔体指数为12.6-15，氧指数为26.2-27.5％，因此具有优异的机械性能和良好的阻燃性。

2. 发明公开

EP3181608A1 AN EPOXY RESIN CURING AGENT AND PREPARATION METHODS AND USES THEREOF 审中-公开
标题翻译：一种环氧树脂固化剂及其制备方法和用途
公开(公告)号：EP3181608A1
公开(公告)日：2017-06-21
申请号：EP16167206.8
申请日：2016-04-27
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C08G59/42 , C08G59/68 , C08G63/19 , C08G63/50 , C08J5/24 , B32B15/092 , H05K1/03
CPC分类号： C07C69/94 , B32B15/092 , C08G59/4223 , C08G59/686 , C08G63/193 , C08G63/50 , C08J5/24 , C08J2363/00 , C09D163/00 , H05K1/0366 , H05K1/0373 , H05K3/4676 , H05K2201/012 , H05K2201/0209
摘要： The present invention relates to an epoxy resin curing agent having a structure of Formula I and preparation methods and uses thereof. The present invention makes a resin composition formed by the epoxy resin curing agent have good low dielectric properties by using an epoxy resin curing agent having a specific structure, and the cured products of the epoxy resin composition have low dielectric constant and dielectric loss and good heat resistance and are low dielectric materials having great economic properties and being environmental friendly.
摘要翻译：本发明涉及具有式I结构的环氧树脂固化剂及其制备方法和用途。本发明通过使用具有特定结构的环氧树脂固化剂使得由环氧树脂固化剂形成的树脂组合物具有良好的低介电性能，并且环氧树脂组合物的固化产物具有低介电常数和介电损耗以及良好的热量具有很高的经济性和环境友好性的低介电材料。

3. 发明公开

EP3216814A1 ISOCYANATE-MODIFIED EPOXY RESIN AND USES THEREOF 审中-公开
标题翻译：异氰酸酯改性环氧树脂及其用途
公开(公告)号：EP3216814A1
公开(公告)日：2017-09-13
申请号：EP16173252.4
申请日：2016-06-07
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C08G59/26 , C08G59/14
CPC分类号： C08G59/26 , C07D413/14 , C08G59/1477 , C08J5/043 , C08J5/24 , C08J2363/00 , C08J2363/02 , C08L63/00 , C08L2205/025
摘要： The present invention relates to an isocyanate-modified epoxy resin having a structure of Formula (I): in Formula (I), R is selected from divalent organic groups; n is an integer greater than or equal to zero; in Y, R 1 , R 2 , R 3 , R 4 , R 18 , R 19 , R 20 , R 21 are independently selected from organic groups; X is nothingness or is selected from divalent organic groups; and R 1 , R 2 , R 3 , R 4 , R 18 , R 19 , R 20 , R 21 are not hydrogen atoms at the same time. The epoxy resin of the present invention utilizes polyisocyanate containing more than 2 cyanate groups as a raw material for preparation and reacts it with resin monomer having epoxy group, thereby achieving the purpose of introducing oxazolidinonyl into epoxy resin monomer; in addition, the epoxy resin of the present invention is terminated by epoxy groups, making the provided epoxy resin components have high heat resistance and low dielectric properties.
摘要翻译：本发明涉及具有式（I）结构的异氰酸酯改性的环氧树脂：在式（I）中，R选自二价有机基团; n是大于或等于零的整数; 在Y中，R 1，R 2，R 3，R 4，R 18，R 19，R 20，R 21独立地选自有机基团; X不存在或者选自二价有机基团; 并且R1，R2，R3，R4，R18，R19，R20，R21不同时为氢原子。本发明的环氧树脂采用含有2个以上氰酸酯基的多异氰酸酯为原料制备，并与具有环氧基的树脂单体反应，达到将恶唑烷酮基引入环氧树脂单体的目的; 此外，本发明的环氧树脂被环氧基团封端，使得提供的环氧树脂组分具有高耐热性和低介电性能。

4. 发明公开

EP3187501A1 A PHOSPHAZENE COMPOUND, AND A COMPOSITION, A PREPREG AND A WIRING BOARD COMPRISING THE SAME 有权
标题翻译：一种磷腈化合物，以及一种组合物，一种预处理剂和一种包含该组合物的接线板
公开(公告)号：EP3187501A1
公开(公告)日：2017-07-05
申请号：EP16182164.0
申请日：2016-08-01
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C07F9/6593 , C08K5/5399
CPC分类号： C07F9/659 , C07F9/65815 , C08J5/24 , C08J2363/04 , C08J2467/00 , C08J2479/08 , C08K5/5399 , C08L2201/02 , C09K21/12
摘要： The present invention relates to a phosphazene compound and a composite metal laminate. The phosphazene compound with a partial structure of carboxylic esters has a structure as shown in formula (I). The present invention obtains a phosphazene compound with a partial structure of carboxylic esters using an M group having specific components. The cured products of the phosphazene compound have good flame retardancy, heat resistance, mechanical properties, flame retardancy, and low dielectric constant, and are a low dielectric flame retardant material having great economic properties and being environmental friendly.
摘要翻译：本发明涉及磷腈化合物和复合金属层压体。具有羧酸酯部分结构的磷腈化合物具有如式（I）所示的结构。本发明使用具有特定组分的M基团获得具有部分羧酸酯结构的磷腈化合物。磷腈化合物的固化产物具有良好的阻燃性，耐热性，机械性能，阻燃性和低介电常数，是一种经济性能优异且环境友好的低介电阻燃材料。

5. 发明授权

EP3187501B1 A PHOSPHAZENE COMPOUND, AND A COMPOSITION, A PREPREG AND A WIRING BOARD COMPRISING THE SAME 有权
公开(公告)号：EP3187501B1
公开(公告)日：2018-09-26
申请号：EP16182164.0
申请日：2016-08-01
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C07F9/6593 , C08K5/5399
CPC分类号： C07F9/659 , C07F9/65815 , C08J5/24 , C08J2363/04 , C08J2467/00 , C08J2479/08 , C08K5/5399 , C08L2201/02 , C09K21/12
摘要： The present invention relates to a phosphazene compound and a composite metal laminate. The phosphazene compound with a partial structure of carboxylic esters has a structure as shown in formula (I). The present invention obtains a phosphazene compound with a partial structure of carboxylic esters using an M group having specific components. The cured products of the phosphazene compound have good flame retardancy, heat resistance, mechanical properties, flame retardancy, and low dielectric constant, and are a low dielectric flame retardant material having great economic properties and being environmental friendly.

6. 发明公开

EP3272795A1 FLAME RETARDANT RESIN COMPOSITION, THERMOSETTING RESIN COMPOSITION, COMPOSITE METAL SUBSTRATE AND FLAME RETARDANT ELECTRONIC MATERIAL 有权转让
标题翻译：阻燃树脂组合物，热固性树脂组合物，复合金属基材和阻燃电子材料
公开(公告)号：EP3272795A1
公开(公告)日：2018-01-24
申请号：EP17173778.6
申请日：2017-05-31
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C08J5/24 , C08K5/21 , C08K5/3492 , C08K5/372 , C08K5/375 , C08K5/49 , C08K5/52 , C08K5/00 , C08K5/523 , C08K5/5313
摘要： The present invention provides a flame retardant resin composition, a thermosetting resin composition, a composite metal substrate and a flame retardant electronic material, wherein the flame retardant composition comprises a sulfur-containing flame retardant, a phosphorus-containing flame retardant and/or a nitrogen-containing flame retardant, and a halogen-free epoxy resin. The synergistic effect of the sulfur-containing flame retardant, phosphorus-containing flame retardant and nitrogen-containing flame retardant in the flame retardant composition of the present invention makes the resultant copper-clad laminate have better heat resistance, water resistance, adhesion, mechanical properties and electrical properties, while having better flame retardancy. While having better flame retardancy, the pouring sealant prepared therefrom has the characteristics of short dry time, low viscosity, good thermal conductivity and good stability, and is a kind of environmentally friendly flame retardant composition having a great economy.
摘要翻译：本发明提供一种阻燃剂树脂组合物，热固性树脂组合物，复合金属基材和阻燃电子材料，其中阻燃剂组合物包含含硫阻燃剂，含磷阻燃剂和/或氮含阻燃剂和无卤环氧树脂。含硫阻燃剂，含磷阻燃剂和含氮阻燃剂在本发明阻燃组合物中的协同效应使得所得覆铜层压板具有更好的耐热性，耐水性，粘合性，机械性能和电性能，同时具有更好的阻燃性。本发明制备的灌封胶虽然具有较好的阻燃性，但具有干燥时间短，粘度低，导热性能好，稳定性好的特点，是一种经济实惠的环保型阻燃剂组合物。

7. 发明公开

EP3093329A1 FLAME RETARDANT COMPOUNDS, HARDENERS AND POLYPHENOL-BASED EPOXY RESINS 审中-公开
标题翻译：多溴联苯醚
公开(公告)号：EP3093329A1
公开(公告)日：2016-11-16
申请号：EP16159045.0
申请日：2016-03-07
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C09K21/12 , C08L63/04 , C08K5/00 , C08K5/5399 , B32B15/092 , C08G79/025
CPC分类号： C08G59/4071 , B32B5/26 , B32B7/12 , B32B9/005 , B32B15/00 , B32B15/04 , B32B15/092 , B32B27/28 , B32B27/281 , B32B27/38 , B32B2255/02 , B32B2255/205 , B32B2260/021 , B32B2260/023 , B32B2260/046 , B32B2262/0276 , B32B2262/101 , B32B2262/106 , B32B2307/30 , B32B2307/306 , B32B2307/3065 , B32B2457/08 , C08G59/06 , C08G59/245 , C08G59/621 , C08G59/686 , C08G79/025 , C08K5/0066 , C08K5/3477 , C08K5/5399 , C08L63/00 , C08L63/04 , C09K21/12
摘要： The present invention discloses flame retardant compounds, hardeners and polyphenol-based epoxy resins. In the molecular structure, such flame retardant compounds contain phenolic hydroxyl groups, and groups M of nitrogen phosphorus skeleton consisting of unsaturated phosphorous and nitrogen atoms, wherein M contains at least 50 wt% of cyclotriphosphazene groups M 1 , at most 48 wt% of M 2 , which is a cyclic ring consisting of four or more phosphazene groups, and at most 48 wt% of non-cyclic polyphosphazene groups M 3 . Therefore, such flame retardant compounds have better flame retardancy, and the cured products thereof have better heat resistance, water resistance, cohesiveness, mechanical property and electrical property. Additionally, such compounds can improve flame retardancy, economy and envionmental friendly protection when applied in composite metal laminates and circuit boards.
摘要翻译：本发明公开了阻燃化合物，硬化剂和多酚类环氧树脂。在分子结构中，这种阻燃化合物含有酚羟基和由不饱和磷和氮原子组成的氮磷骨架M，其中M含有至少50重量％的环三磷腈基M 1，至多48重量％的M 2是由四个以上的磷腈基组成的环状，以及最多48重量％的非环状聚磷腈基M 3。因此，这种阻燃化合物具有更好的阻燃性，其固化物具有更好的耐热性，耐水性，粘结性，机械性能和电性能。此外，当复合金属层压板和电路板应用时，这种化合物可以改善阻燃性，经济性和环境友好的保护。

8. 发明公开

EP3272802A1 FLAME-RETARDANT RESIN COMPOSITION, THERMOSETTING RESIN COMPOSITION, FLAME-RETARDANT ENGINEERING PLASTIC AND COMPOSITE METAL SUBSTRATE 有权转让
标题翻译：阻燃树脂组合物，热固性树脂组合物，阻燃工程塑料和复合金属基材
公开(公告)号：EP3272802A1
公开(公告)日：2018-01-24
申请号：EP17179033.0
申请日：2017-06-30
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C08K5/21 , C08K5/3492 , C08K5/372 , C08K5/523 , C08K5/5313 , C08L55/02 , C08L67/02 , C08L69/00 , C08K5/375 , C08J5/24 , C08K5/52
摘要： The present invention provides a flame-retardant resin composition, a thermosetting resin composition, a flame-retardant engineering plastic and a composite metal substrate. The flame-retardant resin composition comprises a sulfur-containing flame retardant, a phosphorus-containing flame retardant and/or a nitrogen-containing flame retardant, and a halogen-free epoxy resin. The sulfur-containing flame retardant, phosphorus-containing flame retardant and nitrogen-containing flame retardant in the flame-retardant resin composition of the present invention play a synergistic effect, making the prepared copper clad laminate have good flame retardancy, and also good heat resistance, water resistance, adhesion, mechanical properties and electrical properties, and making the prepared engineering plastic have good flame retardancy and good mechanical properties, and thus the flame-retardant resin composition of the present invention is a kind of flame-retardant composition with large economy and friendly environment.
摘要翻译：本发明提供阻燃性树脂组合物，热固性树脂组合物，阻燃性工程塑料和复合金属基材。阻燃树脂组合物包含含硫阻燃剂，含磷阻燃剂和/或含氮阻燃剂以及不含卤素的环氧树脂。本发明阻燃树脂组合物中的含硫阻燃剂，含磷阻燃剂和含氮阻燃剂具有协同效应，使得制备的覆铜箔层压板具有良好的阻燃性，且耐热性也较好耐水性，附着力，机械性能和电性能，使得制得的工程塑料具有良好的阻燃性和良好的机械性能，因此本发明的阻燃树脂组合物是一种经济性大的阻燃组合物友好的环境。

9. 发明公开

EP3263576A1 PHOSPHAZENE COMPOUND CONTAINING ESTER GROUP, PREPARATION METHOD AND USE THEREOF 审中-公开
标题翻译：含有酯基的磷苯化合物，其制备方法和用途
公开(公告)号：EP3263576A1
公开(公告)日：2018-01-03
申请号：EP17173316.5
申请日：2017-05-29
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C07F9/6593 , B32B15/00 , H05K1/00
CPC分类号： C07F9/65815 , B32B15/00 , C08J5/24 , C08J2363/00 , C09K21/12 , H05K1/024 , H05K1/0373 , H05K2201/012 , H05K2203/122
摘要： The present invention relates to a phosphazene compound containing an ester group having a structure of formula (I). The present invention grafts ester groups to phosphazene compounds and makes terminal grafted hydroxyl and carboxyl groups reacted with polymer matrix, producing an improvement of flame retardancy and a reduction of dielectric constant at the same time when the phosphazene compound is introduced into polymer matrix. Since N and P atoms are directly bonded into the polymer matrix by a reaction rather than addition and combination means in the prior art, there is no reduced mechanical properties of the matrix due to the addition of flame retardants.
摘要翻译：本发明涉及含有具有式（I）结构的酯基的磷腈化合物。本发明将酯基接枝到磷腈化合物上并使端基接枝的羟基和羧基与聚合物基体反应，在将磷腈化合物引入聚合物基体的同时，产生阻燃性的提高和介电常数的降低。由于N和P原子通过反应直接键合到聚合物基体中而不是现有技术中的添加和组合手段，因此由于添加了阻燃剂而没有降低基体的机械性能。

10. 发明公开

EP3190119A1 PHOSPHAZENE COMPOUND COMPRISING CYANO GROUP, PREPARATION METHOD AND USES THEREOF 审中-公开
标题翻译：包含氰基的磷苯化合物，其制备方法和用途
公开(公告)号：EP3190119A1
公开(公告)日：2017-07-12
申请号：EP16182165.7
申请日：2016-08-01
申请人： Guangdong Guangshan New Materials Co., Ltd.
发明人： PAN, Qingchong
IPC分类号： C07F9/6593 , C08K5/5399
CPC分类号： C07F9/659 , C07F9/65815 , C08J5/24 , C08J2379/00 , C08J2467/00 , C08J2479/08 , C08K5/5399 , C08L2201/02 , C09K21/12
摘要： The present invention relates to a phosphazene compound comprising cyano group having a molecular structure of Formula (I); wherein, Y and Y' are independently selected from organic groups; M 1 and M 2 are independently selected from phosphazene groups, and M 1 contains m 1 phosphorus atoms, and M 2 contains m 2 phosphorus atoms; X 1 , X 1 ', X 2 , X 3 and X 4 are independently selected from any one of the sixth main-group elements; R and R' are independently selected from divalent organic groups; a is an integer greater than or equal to 0; b is an integer greater than or equal to 1; and c is an integer greater than or equal to 0; and a+b=2m 1 , d+2=2m 2 . The present invention achieves a synergistic effect with P and N of phosphazene group by introducing cyano group to the phosphazene group, and thus improves thermal stability and flame retardancy of the phosphazene compound, and the compatibility thereof with other components is excellent. The resin composition comprising the phosphazene compound of the present invention has good heat resistance, water resistance, adhesive properties and mechanical properties, and thus the application thereof is widened.
摘要翻译：本发明涉及包含具有式（I）的分子结构的氰基的磷腈化合物; 其中，Y和Y'独立地选自有机基团; M1和M2独立地选自磷腈基团，M1含有m1个磷原子，M2含有m2个磷原子; X1，X1'，X2，X3和X4独立地选自第六主族元素中的任何一个; R和R'独立地选自二价有机基团; a是大于或等于0的整数; b是大于或等于1的整数; c是大于或等于0的整数; a + b = 2m1，d + 2 = 2m2。本发明实现了与P和磷腈基团的N协同效果通过引入氰基向磷腈基团，并因此改善热稳定性和磷腈化合物的阻燃性，而且兼容性它们与其它组分是非常好的。包含本发明的磷腈化合物的树脂组合物具有良好的耐热性，耐水性，粘合性和机械性能，因此其应用被拓宽。

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