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1. 发明授权

EP0024197B1 Process for the preparation of copper quinolinate 失效
标题翻译：制备喹啉的方法
公开(公告)号：EP0024197B1
公开(公告)日：1983-05-25
申请号：EP80302782.0
申请日：1980-08-13
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Yoshihiro, Hitano , Kenji, Itoh , Ikegami, Seishi , Matsumoto, Mansuke
IPC分类号： C07D213/807
CPC分类号： C07D213/80

2. 发明公开

EP0124377A3 Chromogenic compounds 失效
标题翻译：染色体化合物
公开(公告)号：EP0124377A3
公开(公告)日：1985-08-14
申请号：EP84302885
申请日：1984-04-30
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Ikegami, Seishi , Amako, Takamichi
IPC分类号： C07D307/94 , C07D491/107 , B41M05/12 , B41M05/26 , C07D307/00 , C07D221/00 , C07D241/00
CPC分类号： B41M5/145 , B41M5/327 , C07D307/94 , C07D491/10
摘要： Chromogenic fluorene-9-spiro-lactones have the formula:
where R 1 , R 2 , R 3 , R 4 and E have defined meaning. The compounds can be made by diazotizing and then effecting a ring closing reaction on the corresponding precursor primary amino-substituted phthalide, furopyridine or furopyrazine. Compounds where E is a group of the formula
and R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are each C 1 -C 4 alkyl groups are preferred. The compounds are chromogenic and can be used in pressure and/or heat sensitive record material. They give lightfast blue to green colours when reacted with electron accepting co-reactants. The coloured forms exhibit marked absorption in the near infrared making them particularly useful in OCR detection systems.

3. 发明授权

EP0034943B1 Process for the preparation of copper quinolinate 失效
标题翻译：制备喹啉酸铜的方法
公开(公告)号：EP0034943B1
公开(公告)日：1983-07-13
申请号：EP81300755.6
申请日：1981-02-24
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Hatano, Yoshihiro , Ikegami, Seishi
IPC分类号： C07D213/807
CPC分类号： C07D213/803 , C07D213/80

4. 发明公开

EP0034943A2 Process for the preparation of copper quinolinate 失效
标题翻译：一种制备Kupferchinolinat过程。
公开(公告)号：EP0034943A2
公开(公告)日：1981-09-02
申请号：EP81300755.6
申请日：1981-02-24
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Hatano, Yoshihiro , Ikegami, Seishi
IPC分类号： C07D213/807
CPC分类号： C07D213/803 , C07D213/80
摘要： A process for the preparation of copper quinolinate in which quinoline is oxidised by hydrogen peroxide in sulphuric acid in the presence of copper sulphate in which the reaction is carried out at a pressure of less than 400 mm Hg. The reduced pressure enables the reaction to be performed at higher temperatures and with greater control; also the reaction time is shortened and the yield improved.
Copper quinolinate is used to prepare quinolinic acid which is the starting material for some chromogenic materials used in the pressure-sensitive record material field.

5. 发明授权

EP0124377B1 Chromogenic compounds 失效
标题翻译：色素化合物
公开(公告)号：EP0124377B1
公开(公告)日：1991-09-25
申请号：EP84302885.3
申请日：1984-04-30
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Ikegami, Seishi , Amako, Takamichi
IPC分类号： C07D307/94 , C07D491/107 , B41M5/145 , B41M5/26
CPC分类号： B41M5/145 , B41M5/327 , C07D307/94 , C07D491/10

6. 发明授权

EP0080814B1 Chromogenic compounds 失效
标题翻译：染色体化合物
公开(公告)号：EP0080814B1
公开(公告)日：1986-10-15
申请号：EP82305948.0
申请日：1982-11-09
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Kumagae, Yojiro , Iwasaki, Yasuhisa
IPC分类号： C07D213/50 , C07D401/06 , C07D471/04 , B41M5/16 , B41M5/18
CPC分类号： C07D401/14 , B41M5/136 , B41M5/323 , C07D213/50 , C07D471/04

7. 发明公开

EP0124377A2 Chromogenic compounds 失效
标题翻译：色素变异体
公开(公告)号：EP0124377A2
公开(公告)日：1984-11-07
申请号：EP84302885.3
申请日：1984-04-30
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Ikegami, Seishi , Amako, Takamichi
IPC分类号： C07D307/94 , C07D491/107 , B41M5/145 , B41M5/26
CPC分类号： B41M5/145 , B41M5/327 , C07D307/94 , C07D491/10
摘要： Chromogenic fluorene-9-spiro-lactones have the formula:
where R 1 , R 2 , R 3 , R 4 and E have defined meaning. The compounds can be made by diazotizing and then effecting a ring closing reaction on the corresponding precursor primary amino-substituted phthalide, furopyridine or furopyrazine. Compounds where E is a group of the formula
and R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are each C 1 -C 4 alkyl groups are preferred. The compounds are chromogenic and can be used in pressure and/or heat sensitive record material. They give lightfast blue to green colours when reacted with electron accepting co-reactants. The coloured forms exhibit marked absorption in the near infrared making them particularly useful in OCR detection systems.
摘要翻译：显色芴-9-螺 - 内酯具有下式：其中R 1，R 2，R 3，R 4和E具有定义的含义。化合物可以通过重氮化制备，然后在相应的前体伯氨基取代的苯酞，呋喃啶或呋喃并吡嗪上进行闭环反应。其中E为式（CHEM）和R 1，R 2，R 3，R 4，R 5和R 6的基团的化合物优选为C 1 -C 4烷基。这些化合物是显色的，可用于压力和/或热敏记录材料。当与电子接受共反应物反应时，它们呈现快速的蓝色至绿色。着色形式在近红外表现出明显的吸收，使得它们在OCR检测系统中特别有用。

8. 发明公开

EP0024197A1 Process for the preparation of copper quinolinate 失效
标题翻译：一种制备chinolinsaurem铜工艺。
公开(公告)号：EP0024197A1
公开(公告)日：1981-02-25
申请号：EP80302782.0
申请日：1980-08-13
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Yoshihiro, Hitano , Kenji, Itoh , Ikegami, Seishi , Matsumoto, Mansuke
IPC分类号： C07D213/807
CPC分类号： C07D213/80
摘要： A process for the preparation of copper quinolinate in which quinoline is oxidized by hydrogen peroxide in 10 to 30% sulphuric acid in the presence of copper sulphate at a temperature of 55 to 75°C, the molar ratio of sulphuric acid to quinoline being greater than 1 : 1. The concentration and amount of sulphuric acid enable greater control of the reaction temperature and result in copper quinoiate in improved yield and purity.
Copper quinolinate is used to prepare quinolinic acid which is the starting material for some chromogenic materials used in the pressure-sensitive record material field.

9. 发明公开

EP0080814A1 Chromogenic compounds 失效
标题翻译：生色化合物。
公开(公告)号：EP0080814A1
公开(公告)日：1983-06-08
申请号：EP82305948.0
申请日：1982-11-09
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Kumagae, Yojiro , Iwasaki, Yasuhisa
IPC分类号： C07D213/50 , C07D401/06 , C07D471/04 , B41M5/16 , B41M5/18
CPC分类号： C07D401/14 , B41M5/136 , B41M5/323 , C07D213/50 , C07D471/04
摘要： Chromogenic compounds have the general formula:
wherein X represents an optionally substituted aminophenyl, indolyl, julolidinyl, kairolyl, piperidinophenyl, pyr- rolidinophenyl, morpholinyl, carbazolyl or indolizinyl radical. These compounds can be used in pressure-sensitive and heat-sensitive record materials and manifold marking systems.

10. 发明公开

EP0034943A3 Process for the preparation of copper quinolinate 失效
标题翻译：制备喹喔啉的方法
公开(公告)号：EP0034943A3
公开(公告)日：1981-09-23
申请号：EP81300755
申请日：1981-02-24
申请人： YAMAMOTO KAGAKU GOSEI CO., LTD.
发明人： Hatano, Yoshihiro , Ikegami, Seishi
IPC分类号： C07D213/807
CPC分类号： C07D213/803 , C07D213/80
摘要： A process for the preparation of copper quinolinate in which quinoline is oxidised by hydrogen peroxide in sulphuric acid in the presence of copper sulphate in which the reaction is carried out at a pressure of less than 400 mm Hg. The reduced pressure enables the reaction to be performed at higher temperatures and with greater control; also the reaction time is shortened and the yield improved. Copper quinolinate is used to prepare quinolinic acid which is the starting material for some chromogenic materials used in the pressure-sensitive record material field.

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