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81. 发明公开

EP3559160A1 PROCESS FOR OXIDIZING THIOL COMPOUNDS IN A SINGLE VESSEL 有权
公开(公告)号：EP3559160A1
公开(公告)日：2019-10-30
申请号：EP17882943.8
申请日：2017-12-15
申请人： UOP LLC
发明人： TERTEL, Jonathan, A. , WONG, Susanna K.
IPC分类号： C10G27/06 , C10G19/02 , C10G19/08 , C07C319/24 , B01D17/02 , B01J10/00 , C07C319/28

82. 发明公开

EP3395796A1 A CRYSTALLINE TRIHYDRATE FORM OF (3S,3S ) 4,4 -DISULFANEDIYLBIS (3-AMINOBUTANE 1-SULFONIC ACID) 审中-公开
公开(公告)号：EP3395796A1
公开(公告)日：2018-10-31
申请号：EP18177972.9
申请日：2011-10-07
申请人： Quantum Genomics
发明人： BALAVOINE, Fabrice , MADEC, Jonathan , SCHNEIDER, Jean-Marie , COQUEREL, Gérard , COUVRAT, Nicolas , CARTIGNY, Yohann , PETIT, Marie-Noëlle
IPC分类号： C07C309/14 , C07C303/02 , C07C319/24 , C07C323/66 , C07C303/22
CPC分类号： C07C323/66 , C07B2200/13 , C07C303/22 , C07C319/24 , C07C309/14
摘要： The present invention relates to a new method for the preparation of (3S,3S') 4,4'-disulfanediylbis(3-aminobutane 1-sulfonic acid) in five steps from (S)-ethyl 2-(benzyloxycarbonylamino)-4-(neopentyloxysulfonyl)butanoate A .

83. 发明公开

EP3164382A1 PROCÉDÉ DE PRÉPARATION DE DISULFURE DE DIMÉTHYLE 有权
标题翻译： PROCÉDÉDEPRÉPARATIONDE DISULFURE DEDIMÉTHYLE
公开(公告)号：EP3164382A1
公开(公告)日：2017-05-10
申请号：EP15736579.2
申请日：2015-06-29
申请人： Arkema France
发明人： FREMY, Georges , BARRE, Patrice , RAYMOND, Jean-Michel
IPC分类号： C07C319/02 , C07C319/24 , C07C321/04 , C07C321/14
CPC分类号： C07C319/24 , C01B32/75 , C07C319/02 , C07C319/06 , C07C321/04 , C07C321/14
摘要： The present invention relates to a method for preparing dimethyl disulphide, in batches or continuously, preferably continuously, said method including at least the following steps: a) reacting at least one hydrocarbon feedstock in the presence of hydrogen sulphide (H
2 S) and optionally sulphur (S) such as to form carbon disulphide (CS
2 ) and hydrogen (H
2 ); b) reacting said carbon disulphide (CS
2 ) by hydrogenation in the presence of said hydrogen (H
2 ) obtained in step a), such as to form methyl mercaptan (CH
3 SH), hydrogen sulphide(H
2 S) and optionally hydrogen (H
2 ); c) optionally, but preferably, recirculating said hydrogen sulphide (H
2 S) formed in step b) to step a); d) reacting the methyl mercaptan formed in step b) with sulphur such as to form dimethyl disulphide and hydrogen sulphide; e) optionally recirculating the hydrogen sulphide formed during step d) to step a); and f) recovering the dimethyl disulphide.
摘要翻译：本发明涉及分批或连续，优选连续地制备二甲基二硫化物的方法，所述方法至少包括以下步骤：a）使至少一种烃原料在硫化氢（H 2 S）和任选的硫（ S）以形成二硫化碳（CS2）和氢气（H2）; b）通过在步骤a）中获得的所述氢（H 2）存在下氢化所述二硫化碳（CS 2），例如形成甲硫醇（CH 3 SH），硫化氢（H 2 S）和任选氢（H 2）; c）任选但优选地，将步骤b）中形成的所述硫化氢（H 2 S）再循环至步骤a）; d）使步骤b）中形成的甲硫醇与硫反应以形成二甲基二硫化物和硫化氢; e）任选将步骤d）中形成的硫化氢再循环至步骤a）; 和f）回收二甲基二硫化物。

84. 发明授权

EP2890674B1 PRÉPARATION DE DISULFURES SYMÉTRIQUES ET DISSYMÉTRIQUES PAR DISTILLATION RÉACTIVE DE MÉLANGES DE DISULFURES 有权
标题翻译：通过DISULFIDGEMISCHEN催化反应精馏对称和不对称二硫化物的生产
公开(公告)号：EP2890674B1
公开(公告)日：2016-12-07
申请号：EP13762191.8
申请日：2013-08-27
申请人： Arkema France
发明人： FREMY, Georges
IPC分类号： C07C319/24 , C07C319/28 , C07C321/14
CPC分类号： C07C319/24 , B01J19/122 , B01J2219/1203 , C07C319/28 , Y02P20/127 , C07C321/14

85. 发明公开

EP3080079A1 OXIDATION OF 2-MERCAPTOETHANOL 有权
标题翻译： 2-巯基乙醇的氧化
公开(公告)号：EP3080079A1
公开(公告)日：2016-10-19
申请号：EP14816166.4
申请日：2014-12-09
申请人： BASF SE
发明人： VAUTRAVERS, Nicolas , TELES, Joaquim Henrique
IPC分类号： C07C319/24 , C07C323/12
CPC分类号： C07C319/24 , C07C323/12 , C10M135/24 , C10M2219/084
摘要： The present invention relates to a process for the preparation of bis-(2-hydroxyethyl)-disulfide by oxidizing 2-mercaptoethanol with oxygen in a reaction mixture comprising at least one homogeneously distributed iron comprising salt or complex as catalyst and at least one tertiary amine, to bis-(2-hydroxyethyl)-disulfide, obtainable with the process, and to the use of this bis-(2-hydroxyethyl)-disulfide as intermediate in the manufacture of chemical compounds, such as lubricant additives and in the tertiary oil recovery.

86. 发明公开

EP2053085A1 COMPOUNDING AGENT FOR RUBBER VULCANIZATION CONTAINING AMINE SALT COMPOUND OF CARBOXYLIC ACID GROUP-CONTAINING DISULFIDE, METHOD FOR PRODUCING THE SAME, RUBBER COMPOSITION CONTAINING THE SAME, AND PNEUMATIC TIRE USING THE SAME IN RUBBER FOR BELT COAT AND/OR BELT EDGE CUSHION 有权
标题翻译： KautschukzusammensetzungfürLuftreifen
公开(公告)号：EP2053085A1
公开(公告)日：2009-04-29
申请号：EP07792560.0
申请日：2007-08-09
申请人： The Yokohama Rubber Co., Ltd.
发明人： CHOI, Wonmun , SHIMIZU, Yuuki
IPC分类号： C08L21/00 , B60C1/00 , B60C9/18 , C07C319/22 , C07C319/24 , C07C323/52 , C07C323/62 , C08K5/40
CPC分类号： C07C211/63 , B60C1/00 , C07C211/06 , C07C211/07 , C07C211/35 , C07C211/62 , C07C323/52 , C07C323/62 , C07C2601/14 , C08K5/372 , C08K5/375 , C08L21/00
摘要： A compounding agent for rubber vulcanization comprising an amine salt compound of a carboxylic acid group-containing disulfide having the formula (I):

wherein R 1 , R 2 and R 3 are independently hydrogen or a C 1 -C 20 organic group which may have a heteroatom and/or a substituent group, and X is a C 2 -C 20 organic group which may have a heteroatom and/or a substituent group, a method for producing the same and a rubber composition containing the same, capable of improving the vulcanization rate and vulcanized rubber physical properties, without having a detrimental effect on the scorch time.
摘要翻译：一种用于橡胶硫化的配混剂，其包含具有式（I）的含羧酸基的二硫化物的胺盐化合物：其中R 1，R 2和R 3独立地为氢或可以具有的C 1 -C 20有机基团杂原子和/或取代基，X是可具有杂原子和/或取代基的C 2 -C 20有机基团，其制备方法和含有该取代基的橡胶组合物，其能够改善硫化速率和硫化橡胶的物理性能，而不会对焦烧时间产生不利影响。

87. 发明公开

EP1694637A4 PROCESS FOR SYNTHESIZING DISULFIDES 审中-公开
标题翻译：方法合成二硫化物
公开(公告)号：EP1694637A4
公开(公告)日：2007-09-26
申请号：EP04818053
申请日：2004-12-17
申请人： BIONUMERIK PHARMACEUTICALS INC
发明人： KAWAMI KOH , TOKUDA OSAMU , NIIMOTO YOSHIHIDE
IPC分类号： C07C309/00 , C07C319/24 , C07C323/66 , C07C327/22
CPC分类号： C07C319/24 , C07C323/66
摘要： This invention relates to a process for producing a substantially pure disulfide compound of Formula (II) R5-S-S-R2 as disclosed herein, such as disodium 2,2'-dithiobis ethane sulfonate, by an efficient procedure from available, relatively inexpensive raw materials.

88. 发明公开

EP1499587A4 PROCESS FOR SYNTHESIZING PHARMACEUTICALLY ACTIVE DISULFIDE SALTS 失效转让
标题翻译：方法合成有效的药物DISULFIDSALZE的
公开(公告)号：EP1499587A4
公开(公告)日：2006-05-24
申请号：EP03724301
申请日：2003-04-29
申请人： BIONUMERIK PHARMACEUTICALS INC
发明人： KOCHAT HARRY
IPC分类号： C07C319/24 , C07C323/66 , C07C327/22 , C07F9/38 , C07C309/66 , C07F9/32
CPC分类号： C07C327/22 , C07C319/24 , C07F9/3808 , C07C323/66
摘要： A process for synthesizing pharmaceutically active disulfides, particularly Dimesna and certain derivatives thereof. The process includes reacting an alkylene salt with a sulfurating reagent, then alkalizing the intermediate and flowing oxygen through the mixture to produce the final compound in high yield.

89. 发明公开

EP1633705A1 OXIDATION VON MERCAPTOETHANOL 失效转让
标题翻译：氧化性巯基乙醇
公开(公告)号：EP1633705A1
公开(公告)日：2006-03-15
申请号：EP04724562.6
申请日：2004-03-31
申请人： Thioplast Chemicals GmbH & Co. Kg
发明人： ZEITLER, Michael , KOTTNER, Nils , BERGFELD, Manfred
IPC分类号： C07C319/24
CPC分类号： B01J31/0237 , B01J27/24 , B01J31/04 , B01J31/28 , B01J31/32 , B01J2231/70 , C07C319/24 , C07C323/12
摘要： The invention relates to a method for the production of dithiodiglycol, wherein mercaptoethanol is reacted with oxygen in the presence of ammonia and/or amines using manganese salts or copper salts containing oxygen or gas mixtures containing oxygen. The method supplies a uniform product having high yields; practically no intermediate products not obtained. Reaction time is extremely short. Overoxidation does not take place and there are no waste air and waste water problems.

90. 发明公开

EP1322597A4 PROCESS AND INTERMEDIATES 有权
标题翻译：过程和中间产品
公开(公告)号：EP1322597A4
公开(公告)日：2005-10-19
申请号：EP01975197
申请日：2001-09-12
申请人： SMITHKLINE BEECHAM CORP
发明人： ELDRIDGE ANN M , HIEBL JOHANN
IPC分类号： C07D207/404 , A61K47/48 , C07C319/22 , C07C319/24 , C07C323/52 , C07C323/60 , C07D207/46 , C07C231/10
CPC分类号： C07D207/46 , A61K47/6803 , C07C319/22 , C07C319/24 , C07C323/60 , C07C323/52
摘要： Processes for preparing N-methyl-L-alanine derivatives and novel intermediates of the process. The derivatives and intermediates are useful for preparing cell-binding agent/maytansinoid complexes.

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