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81. 发明公开

EP0006698A1 Curable polysulfide polymer composition and process for the preparation of a shaped article therefrom 有权
标题翻译：一种可固化的聚硫化物混合物及其制造方法从该混合物中的成型制品。
公开(公告)号：EP0006698A1
公开(公告)日：1980-01-09
申请号：EP79301073.7
申请日：1979-06-06
申请人： THIOKOL CORPORATION
发明人： Millen, Edward G. , Pypcznski, Frank K.
IPC分类号： C08L81/04 , C08J3/24
CPC分类号： C08L81/04 , C08G75/14
摘要： The use of polysulfide rubbers cured with zinc oxide and tetramethylthiuram disulfide and other sulfur containing cure accelerators for polyisoprene rubbers in hot applied processes and articles formed thereby are disclosed. The compositions are useful as hot applied sealants and in the extrusion of hoses and similar rubber articles.

82. 发明公开

EP0865417A1 IMPROVED HYDROGENOLYSIS OF 2,4,6,8,10,12-HEXABENZYL-2,4,6,8,10,12-HEXAAZATETRACYCLO 5.5.0.0?5,9 .0?3,11 ]DODECANE 失效
标题翻译： 2,4,6,8,10,12-六氢萘-2,4,6,8,10,12-六氢邻苯二酚的改进氢解5.5.0.0.5,9.0,0.3,11]十二烷
公开(公告)号：EP0865417A1
公开(公告)日：1998-09-23
申请号：EP96942112.0
申请日：1996-12-04
申请人： THIOKOL CORPORATION
发明人： WARDLE, Robert, B. , EDWARDS, W., Wayne
IPC分类号： B01J23 , C06B25 , C07B61 , C07D487
CPC分类号： C07D487/22
摘要： A process for the hydrogenolysis of 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo [5.5.0.0?5,9.03,11¿]dodecane ('HBIW') is disclosed in which a quantity of HBIW, cosolvent and a bromine source are placed into a reaction vessel. Acetic anhydride and a substantially water-free palladium catalyst are then rapidly added. The reaction vessel is purged of an atmosphere capable of reacting with hydrogen, and hydrogen is quickly introduced to convert the HBIW to tetraacetyl-dibenzylhexaazaisowurtzitane ('TADB'). The acetic anhydride is added immediately prior to hydrogen introduction so that it does not have time to react with the HBIW to form an acetylated derivative prior to commencement of the desired hydrogenation reaction. The process requires very little palladium catalyst, preferably less than 10 % wt./wt. based on the HBIW substrate. The TADB, precipitated on the palladium hydrogenation catalyst, is subjected to a second hydrogenation step using formic acid solvent in the presence of hydrogen to form tetraacetyldiformylhexaazaisowurtzitane ('TADF').
摘要翻译： 2,4,6,8,10,12-六苄基-2,4,6,8,10,12-六氮杂四环[5.5.0.0,5,9.03,11]十二烷氢解（'HBIW' ），其中将一定量的HBIW，助溶剂和溴源置于反应容器中。然后迅速加入乙酸酐和基本上无水的钯催化剂。将反应容器清除能够与氢反应的气氛，并迅速引入氢气以将HBIW转化为四乙酰基 - 二苄基六氮杂异纤锌矿型结构烷烃（'TADB'）。在引入氢气之前立即加入乙酸酐，使得在开始期望的氢化反应之前没有时间与HBIW反应形成乙酰化衍生物。该方法需要非常少量的钯催化剂，优选少于10wt％/ wt。基于HBIW基板。在钯氢化催化剂上沉淀的TADB在氢存在下使用甲酸溶剂进行第二氢化步骤以形成四乙酰基二十六氮杂异纤锌矿型结构烷烃（'TADF'）。

83. 发明公开

EP0856004A1 IMPROVED SYNTHESIS OF 2,4,6,8,10,12-HEXABENZYL-2,4,6,8,10,12-HEXAAZATETRACYCLO[5.5.0.05,9 .03,11]DODECANE 失效
标题翻译：改进的2,4,6,8,10,12-六氢萘-2,4,6,8,10,12-六氮杂环十四烷的合成[5.5.0.05,9.03,11]十二烷
公开(公告)号：EP0856004A1
公开(公告)日：1998-08-05
申请号：EP96919476.0
申请日：1996-06-18
申请人： THIOKOL CORPORATION
发明人： CANNIZZO, Louis, F. , EDWARDS, William, W. , WARDLE, Robert, B. , HIGHSMITH, Thomas, K.
IPC分类号： C06B25 , C07D487
CPC分类号： C07D487/22 , C06B25/00
摘要： A process of synthesizing HBIW using a mineral acid, such as perchloric acid, as the acid catalyst is disclosed. According to the process, glyoxal, adjusted to a pH from 4 to 7, and benzylamine are reacted in the presence of the mineral acid for sufficient time to form HBIW. The resulting HBIW is then isolated according to conventional separation techniques.
摘要翻译：公开了使用无机酸如高氯酸作为酸催化剂来合成HBIW的方法。根据该方法，调节pH值从4到7的乙二醛和苄胺在无机酸存在下反应足够的时间以形成HBIW。然后根据常规分离技术分离得到的HBIW。

84. 发明公开

EP0790972A1 SYNTHESIS OF BIS(2,2-DINITROPROPYL)FORMAL (BDNPF) 失效
标题翻译：合成双（2,2-二硝基丙基）缩甲醛的
公开(公告)号：EP0790972A1
公开(公告)日：1997-08-27
申请号：EP95933058.0
申请日：1995-09-08
申请人： THIOKOL CORPORATION
发明人： HAMILTON, R., Scott , WARDLE, Robert, B.
IPC分类号： B01J27 , C07B61 , C07C201 , C07C205
CPC分类号： C07C201/12 , C07C205/29
摘要： A nonsolvent process of synthesizing bis(2,2-dinitropropyl)formal (BDNPF) is disclosed. In the process, 2,2-dinitropropanol (DNPOH) is reacted at low temperature with a formaldehyde source in the presence of a protic acid catalyst, such as H2SO4, HC1, H3PO4, or HBr. To inhibit byproduct formation, the reaction temperature is maintained from about -30 °C to 30 °C. Upon completion of the reaction, the reaction solution is quenched with water and washed with an aqueous hydroxide ion solution. The hydroxide ion concentration should be sufficient to neutralize the protic acid catalyst during the quenching step and to solubilize unreacted 2,2-dinitropropanol as well as other aqueous soluble byproducts in the reaction solution. The BDNPF product is extracted with a low boiling temperature polar organic solvent, such as methyl tert-butyl ether (MTBE) or equivalent solvent. The organic solvent is evaporated to yield usable BDNPF product. The resulting yield is at least 60 % based on the starting quantity of 2,2-dinitropropanol.

85. 发明公开

EP0767872A1 SOLID PROPELLANT DUAL PULSE ROCKET MOTOR LOADED CASE AND IGNITION SYSTEM AND METHOD OF MANUFACTURE 失效
标题翻译：固体推进剂双脉冲火箭发动机负载箱和点火系统及制造方法
公开(公告)号：EP0767872A1
公开(公告)日：1997-04-16
申请号：EP95917742.0
申请日：1995-04-28
申请人： THIOKOL CORPORATION
发明人： DOMBROWSKI, Daniel, C. , FREY, Thomas, J. , NEVRINCEAN, Andrew, G.
IPC分类号： F02K9
CPC分类号： F02K9/346 , F02K9/28 , F02K9/95
摘要： A solid propellant dual pulse rocket motor (10) has a pressure vessel (12) containing two pulse grains (24, 26) separated by a barrier insulator (32). An igniter assembly (36) disposed at a fore end (16) of the pressure vessel (12) selectively ignites a first pulse grain (24) from a central cavity (34). The igniter assembly (36) also ignites a second pulse grain (26) by ejecting hot combustion gases onto the fore end of the grain.
摘要翻译：固体推进剂双脉冲火箭发动机（10）具有压力容器（12），该压力容器包含由阻挡绝缘体（32）分开的两个脉冲颗粒（24,26）。布置在压力容器（12）的前端（16）处的点火器组件（36）选择性地从中心腔（34）点燃第一脉冲颗粒（24）。点火器组件（36）还通过将热燃烧气体喷射到谷物的前端上来点燃第二脉冲谷粒（26）。

86. 发明公开

EP0710195A1 THERMITE COMPOSITIONS FOR USE AS GAS GENERANTS 失效
标题翻译：铝热组合物中的气体发生体
公开(公告)号：EP0710195A1
公开(公告)日：1996-05-08
申请号：EP94923537.0
申请日：1994-07-14
申请人： Thiokol Corporation
发明人： HINSHAW, Jerald, C. , BLAU, Reed, J.
IPC分类号： B60R21 , C06B33 , C06D5
CPC分类号： C06B33/00 , C06D5/06
摘要： A sodium-azide-free gas-generating composition includes an oxidizable inorganic fuel, such as a metal, and an oxidizing agent containing oxygen and a metal. The fuel and the oxidizing agent are selected such that water vapor is produced upon reaction between the inorganic fuel and the oxidizing agent. Although a number of inorganic fuels can be employed, a suitable fuel can be a transition metal, another element such as silicon, boron, aluminum, magnesium, an intermetallic compound, hydrides of these metals and mixtures thereof. The oxidizing agent comprises a metal hydroxide, a metal hydrous oxide, a metal oxide hydrate, a metal oxide hydroxide, or mixtures thereof. The fuel and oxidizing agent are selected such that essentially no gases other than water vapor are produced.

87. 发明公开

EP0695283A1 PROPELLANT FORMULATIONS BASED ON DINITRAMIDE SALTS AND ENERGETIC BINDERS 失效
标题翻译：基于DINITRAMIDSALZEN和高能粘合剂燃料组合物
公开(公告)号：EP0695283A1
公开(公告)日：1996-02-07
申请号：EP94915823.0
申请日：1994-04-19
申请人： THIOKOL CORPORATION
发明人： HINSHAW, Carol J. , WARDLE, Robert B. , HIGSHSMITH, Tom K.
IPC分类号： C06B33 , C06B25 , C06B31 , C06B45 , C06D5
CPC分类号： C06B31/00 , C06B25/34 , C06B45/105
摘要： Composite propellant formulations are disclosed having a dinitramide salt oxidizer, such as ammonium dinitramide, an energetic binder, such as poly(glycidyl nitrate), a reactive metal, such as aluminum, and other typical propellant ingredients such as curatives and stabilizers. The disclosed propellant formulations are able to combust aluminum efficiently, possess high burn rates, and produce little or no HCl exhaust gases.

88. 发明授权

EP0485099B1 Isotactic poly(glycidyl nitrate) and synthesis thereof 失效
标题翻译：相同的全同立构聚硝酸盐和制造
公开(公告)号：EP0485099B1
公开(公告)日：1995-12-20
申请号：EP91309964.4
申请日：1991-10-29
申请人： THIOKOL CORPORATION
发明人： Willer, Rodney L. , Stern, Alfred G. , Day, Robert S.
IPC分类号： C08G65/28 , C08G65/22 , C07D303/16
CPC分类号： C08G65/22 , C07D303/16

89. 发明公开

EP0686135A1 BORE MITIGANTS FOR SOLID PROPELLANT ROCKET MOTORS 失效
标题翻译： BOHRDÄMPFER固体燃料火箭发动机
公开(公告)号：EP0686135A1
公开(公告)日：1995-12-13
申请号：EP94905318.0
申请日：1993-11-23
申请人： THIOKOL CORPORATION
发明人： HATCH, Robert, L. , TAYLOR, Robert, D. , HINSHAW, Jerald, C.
IPC分类号： C06B45 , F02K9 , F42B39
CPC分类号： F02K9/38 , C06B45/00 , F42B39/14
摘要： Methods and materials for modifying rocket motors to render them safer are disclosed. The invention is primarily related to placing within the bore of a rocket motor a sufficient quantity of a material mitigant such that if the rocket motor receives an unintended impact, the material mitigates the effects of the impact, and prevents ignition or explosion of the propellant. The material mitigant may take a number of forms; however, polymer foams and fibers of various types have been found to work well. It is presently preferred that the material mitigants have a density of not less than approximately 0.04 grams/cc. Examples of such materials include polyurethane foam, polystyrene, and Kevlar® fibers. It is also preferred that the material mitigant not be reactive with the propellant in the rocket motor. While the material mitigant is configured such that it absorbs fragments or energy of propellant dislodged by the impact, at the same time it does not interfere with the normal ignition and operation of the rocket motor.

90. 发明公开

EP0603382A1 PROCESS FOR MAKING HIGH PURITY HYDROXYLAMMONIUM NITRATE 失效
标题翻译：工艺生产高纯度硝酸羟基铵。
公开(公告)号：EP0603382A1
公开(公告)日：1994-06-29
申请号：EP93916470.0
申请日：1993-06-14
申请人： THIOKOL CORPORATION
发明人： LEVINTHAL, Michael, L. , WILLER, Rodney, L. , PARK, Dennis, J. , BRIDGES, Ronnelle
IPC分类号： C01B21 , C06B31 , C06B47
CPC分类号： C06B31/00 , C01B21/1445 , C01B21/1454 , C06B47/00
摘要： Procédé de production de sels oxydants énergétiques et de solutions de ces sels. L'invention se rapporte en particulier à des procédés de production de solutions aqueuses de nitrate d'hydroxylammonium de grande pureté, destinées à être utilisées pour produire des poudres à canon liquides. Le processus sans alcool ci-décrit produit du nitrate d'hydroxylammonium sans alcool de grande pureté par la neutralisation d'une solution aqueuse d'acide nitrique (20-70 % en poids/poids) avec une solution aqueuse d'hydroxylamine sans alcool à des températures allant de -50 °C à des valeurs supérieures à la température ambiante. Ce processus permet d'obtenir la solution aqueuse de nitrate d'hydroxylammonium sans alcool de grande pureté en une concentration utilisable. Ce processus est économique, peu polluant et de mise en oeuvre facile.

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