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71. 发明授权

EP2006250B1 Verfahren zur Herstellung von SiH-haltigen Silanen 有权
标题翻译：一种用于含SiH的硅烷的制备方法
公开(公告)号：EP2006250B1
公开(公告)日：2013-03-06
申请号：EP08156877.6
申请日：2008-05-26
申请人： Wacker Chemie AG
发明人： Geisberger, Gilbert , Wewers, Wolfgang
IPC分类号： C01B33/04 , C01B33/107 , C07F7/08 , C07F7/12
CPC分类号： C07F7/123 , C01B33/043 , C01B33/10773 , C07F7/126 , Y02P20/127

72. 发明公开

EP2537579A3 Vorrichtung und Verfahren zur Temperaturbehandlung von korrosiven Gasen 有权
标题翻译：的装置和方法腐蚀性气体的热处理
公开(公告)号：EP2537579A3
公开(公告)日：2013-01-23
申请号：EP12170852.3
申请日：2012-06-05
申请人： Wacker Chemie AG
发明人： Ellinger, Norbert , Wiesbauer, Josef , Ring, Robert
IPC分类号： B01J12/00 , C01B33/107 , B01J19/02 , F24H3/00
CPC分类号： B01J19/02 , B01J19/002 , B01J19/0073 , B01J19/087 , B01J2219/00135 , B01J2219/00268 , B01J2219/0813 , B01J2219/0815 , B01J2219/0828
摘要： Die Erfindung betrifft eine Vorrichtung zur Temperaturbehandlung von korrosiven Gasen, umfassend eine Kammer zum Aufheizen von Gasen, in der sich wenigstens vier Heizelemente oder vier Gruppen von Heizelementen aus einem elektrisch leitfähigen Material befinden, wobei jedes Heizelement oder jede Gruppe von Heizelementen an ein separat regel- und/oder steuerbares Teilsystem eines elektrischen Energienetzes angeschlossen ist und dabei durch direkten Stromdurchgang beheizbar ist, wobei jedes getrennt regel-und/oder steuerbare Heizelement oder jede getrennt regel-und/oder steuerbare Gruppe von Heizelementen auf mindestens einen entweder gleichen oder abweichenden Wert eines Parameters aus der Gruppe bestehend aus Temperatur, Heizleistung, Strom, Spannung, Widerstand oder auf eine andere durch die Vorrichtung beeinflussbare Prozessgröße des Heizelementes steuer- oder regelbar ist, wobei wenigstens vier regel- und/oder steuerbare Teilsysteme galvanisch gegen Erde isoliert sind. Ebenso betrifft die Erfindung ein entsprechendes Verfahren zur Temperaturbehandlung von korrosiven Gasen.

73. 发明公开

EP2526052A1 VERWENDUNG EINES DRUCKBETRIEBENEN KERAMISCHEN WÄRMETAUSCHERS ALS INTEGRALER BESTANDTEIL EINER ANLAGE ZUR UMSETZUNG VON SILICIUMTETRACHLORID ZU TRICHLORSILAN 审中-公开
标题翻译：使用的压力下操作，硅酸盐EXCHANGER作为四氯化硅的实施，三氯硅烷一项投资的一个组成部分
公开(公告)号：EP2526052A1
公开(公告)日：2012-11-28
申请号：EP10801574.4
申请日：2010-12-16
申请人： Evonik Degussa GmbH
发明人： STOCHNIOL, Guido , ÖNAL, Yücel , BIEKER, Alfons , PAULI, Ingo , LUNT-RIEG, Ingrid
IPC分类号： C01B33/027 , C01B33/107
CPC分类号： C01B33/1071 , C01B33/10731
摘要： The invention relates to the use of a ceramic heat exchanger as an integral component of a method for the catalytic hydrodehalogenation of silicon tetrachloride to trichlorosilane in the presence of hydrogen, wherein the product gas and the reactant gases are conducted through the heat exchanger as pressurized streams and the heat exchanger comprises heat exchanger elements made of ceramic material.

74. 发明公开

EP2465819A1 METHOD FOR PURIFYING CHLOROSILANES 有权
标题翻译： VERFAHREN ZUR REINIGUNG VON CHLORSILANEN
公开(公告)号：EP2465819A1
公开(公告)日：2012-06-20
申请号：EP10808063.1
申请日：2010-07-07
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： NAGAI, Naoki , SHIMIZU, Takaaki , UEHARA, Katsuhiro , KUBOTA, Tohru
IPC分类号： C01B33/107
CPC分类号： C01B33/10778
摘要： The present invention provides a method for obtaining high purity chlorosilanes from chlorosilanes containing boron impurities and phosphorus impurities. On the basis of the finding that solid by-product formation in the purification of chlorosilanes by adding an aromatic aldehyde results from a catalytic reaction by iron ions or rust-like iron, a Lewis base having a masking effect is added to chlorosilanes. Examples of the Lewis base include a divalent sulfur-containing compound and an alkoxysilane. The divalent sulfur-containing compound is preferably a compound represented by the formula: R-S-R' (wherein R is a hydrocarbon group or a carbonyl group; and the sum of the carbon atoms in R and R' is 7 or more), and the alkoxysilane is preferably a compound represented by the formula: R x Si(OR') 4-x (wherein R and R' are each an alkyl group having 1 to 20 carbon atoms).
摘要翻译：本发明提供从含有硼杂质和磷杂质的氯硅烷中获得高纯度氯硅烷的方法。基于通过添加芳族醛的氯硅烷的纯化形成固体副产物的结果是由铁离子或铁锈等的催化反应产生，将具有掩蔽效果的路易斯碱加入到氯硅烷中。路易碱碱的实例包括二价含硫化合物和烷氧基硅烷。二价含硫化合物优选为由下式表示的化合物：RSR'（其中R为烃基或羰基，R和R'中的碳原子总数为7以上），烷氧基硅烷优选为由式：R x Si（OR'）4-x（其中R和R'各自为具有1至20个碳原子的烷基）表示的化合物。

75. 发明公开

EP2462058A1 VERFAHREN UND ANLAGE ZUR HERSTELLUNG VON TRICHLORSILAN 有权
标题翻译：方法和系统的三氯硅烷
公开(公告)号：EP2462058A1
公开(公告)日：2012-06-13
申请号：EP10739921.4
申请日：2010-08-02
申请人： Schmid Silicon Technology GmbH
发明人： PETRIK, Adolf , HAHN, Jochem , SCHMID, Christian
IPC分类号： C01B33/107
CPC分类号： C01B33/1071 , C01B33/10763
摘要： A process is described for producing trichlorosilane, in which silicon particles are reacted with tetrachlorosilane and hydrogen and optionally with hydrogen chloride in a fluidized-bed reactor (101) to form a trichlorosilane-containing product gas stream, wherein the trichlorosilane-containing product gas stream is passed out of the reactor (101) via an outlet (117), upstream of which at least one particle separator (118) is connected, which particle separator selectively only allows silicon particles to pass up to a defined maximum size, and wherein in preferably regular time intervals, or continuously, via at least one further outlet (109; 112) silicon particles are ejected from the reactor (101) without such a particle separator. In addition, a system (100) is described which is suitable for carrying out such a process and which has a first (101) and a second (102) fluidized-bed reactor which are connected in such a manner that silicon ejected from the first reactor (101) can be transferred into the second reactor (102).

76. 发明公开

EP2454016A2 VERFAHREN ZUR BEHANDLUNG VON AMINOFUNKTIONELLEN, POLYMEREN KATALYSATOR-PRÄKURSOREN 有权
标题翻译：高分子化学工业有限公司
公开(公告)号：EP2454016A2
公开(公告)日：2012-05-23
申请号：EP10720757.3
申请日：2010-05-17
申请人： Evonik Degussa GmbH
发明人： RAULEDER, Hartwig , MÜH, Ekkehard , SCHORK, Reinhold , SCHÖN, Uwe
IPC分类号： B01J31/08 , B01J37/08 , C01B33/107 , C07F7/12 , B01J41/04 , B01J41/14
CPC分类号： B01J31/08 , B01J37/08 , B01J41/04 , B01J41/07 , C01B33/107 , C01B33/10773 , C01P2006/80 , C07F7/125
摘要： The invention relates to a method for treating an amino functional, polymeric catalyst precursor having a high water content, its inner porous structure and outer spherical shape being retained, forming a catalyst by treatment of the catalyst precursor at mild temperatures and low pressure and producing a catalyst having a water content of less than 2.5 % by weight. The method is preferably integrated into an industrial-scale process for producing dichlorosilane, monosilane, silane,or solar or semiconductor silicon from silanes.
摘要翻译：本发明涉及一种用于处理基本上含水氨基官能的聚合催化剂前体的方法，同时保持其内部多孔结构和其外部球形形式以形成催化剂，其中催化剂前体在温和的温度下和在减压以制备水含量低于2.5重量％的催化剂。该方法优选整合成从硅烷制备二氯硅烷，硅烷，硅烷或太阳硅或半导体硅的工业规模方法。

77. 发明授权

EP2176169B1 PROCESS FOR PREPARING TITANIUM TETRACHLORIDE USING OFF-GASES FROM A SILICA AND ZIRCON CARBO-CHLORINATION PROCESS 有权转让
标题翻译：用于生产四氯化钛BY利用排气从KIESELERDE- AND ZIRKON-CARBOCHLORIERUNGSVERFAHREN
公开(公告)号：EP2176169B1
公开(公告)日：2012-03-07
申请号：EP08797019.0
申请日：2008-08-01
申请人： E. I. du Pont de Nemours and Company
发明人： BECNEL, Timothy, J. , HSU, Yung-Hsing, Samson , MUSICK, Charles, David , AKSER, Mustafa , ZAHER, Joseph, J.
IPC分类号： C01G23/02 , C01G25/04 , B01D53/68 , C01B33/107
CPC分类号： C01G23/022 , C01B33/10721 , C01G25/04
摘要： This disclosure relates to an improved process for preparing titanium tetrachloride comprising reacting ores comprising metal oxides with chlorine and a carbon compound at a temperature of about 900°C to about 1300°C to form the corresponding chlorides and off gas comprising carbon monoxide, wherein the metal in the metal oxide is selected from the group consisting of silicon, zircon and mixtures thereof, and wherein the carbon compound is selected from the group consisting of coke, charcoal, silicon carbide and mixtures thereof; and reacting titanium dioxide with a stream comprising off gases formed in the previous step to form titanium tetrachloride and carbon dioxide.

78. 发明公开

EP2385017A1 Process for purifying silicon source material by high gravity roating packed beds 有权
标题翻译：通过用高重力旋转固定床为硅源材料的纯化的方法
公开(公告)号：EP2385017A1
公开(公告)日：2011-11-09
申请号：EP10004757.0
申请日：2010-05-05
申请人： Su, Shyang , Su, Yiheng , Vukelic, Michael
发明人： Su, Shyang , Su, Yiheng , Vukelic, Michael
IPC分类号： C01B33/107
CPC分类号： C01B33/10778 , B01J19/0066 , B01J19/1862 , C01B33/10784 , C01B33/10789
摘要： A process is disclosed for purification of silicon source material including trichlorosilane. First, the silicon source material in liquid state with impurities vapor and the other chlorosilane or silane are passing a first high gravity rotating packed bed with spongy metal, at a temperature lower than the boiling point of the silicon source material, the impurities vapor and the other chlorosilane or silane are separated from the liquid silicon source material; second, the silicon source material in liquid state is fed to a second high gravity rotating packed bed, oxygen is also fed to the second high gravity rotating packed bed to form impurity containing siloxane complexes with higher boiling point. Finally distilling to remove the impurity containing siloxane complexes from the silicon source material.
摘要翻译：一种方法是游离缺失盘为包含三氯硅烷的硅源材料的纯化。首先，在液体状态下的硅源材料与杂质的蒸汽和其它氯硅烷或硅烷使第一高重力与海绵状金属旋转床，在比硅源材料的沸点低的温度下，杂质蒸气和其它氯硅烷或硅烷从液体硅源材料分离; 第二，在液态硅源材料被供给到第二高重力旋转填充床，氧气被如此输送到第二高重力旋转填充床，以形成杂质含硅氧烷配合物的更高的沸点。最后蒸除去杂质从硅源材料包含硅氧烷络合物。

79. 发明公开

EP1947057A4 PROCESS FOR PRODUCTION OF SILICON TETRAFLUORIDE, AND APPARATUS FOR THE PROCESS 审中-公开
标题翻译：用于生产四氟化硅及其装置
公开(公告)号：EP1947057A4
公开(公告)日：2011-11-09
申请号：EP06810921
申请日：2006-09-29
申请人： STELLA CHEMIFA CORP
发明人： NAGANO MITSUGU , MORIYA TAKEHIKO , WAKI MASAHIDE , MIYAMOTO KAZUHIRO
IPC分类号： C01B33/107 , B01D3/14
CPC分类号： C01B33/10705 , B01D3/146 , B01D3/148

80. 发明公开

EP2362852A2 METHOD FOR THE PRODUCTION OF POLYCRYSTALLINE SILICON 审中-公开
标题翻译：用于生产多晶硅
公开(公告)号：EP2362852A2
公开(公告)日：2011-09-07
申请号：EP09756564.2
申请日：2009-10-20
申请人： Sunlit S.R.L.
发明人： TOZZOLI, Silvio , PUSHKO, Anatoli, Vasilievich
IPC分类号： C01B33/039 , C01B33/029 , C01B33/107 , C01B33/04 , C01B33/037
CPC分类号： C01B33/037 , C01B33/029 , C01B33/043 , C01B33/10705
摘要： The process for the production of polycrystalline silicon starting from metallurgical silicon, milled up to a predetermined granulometry, implies the reaction of metallurgical silicon with anhydrous hydrogen fluoride (HF), to obtain silicon tetrafluoride (SiF4), and to operate the synthesis of monosilane (SiH4) by a reaction of hydrogenation of the silicon tetrafluoride (SiF4) with alkaline or alkaline earth metals halide in fluid medium of organic solvent or melt salts. Then a thermal decomposition of said monosilane (SiH4) in a boiling-pseudo fluidized bed reactor is carried out, to obtain high purity granulated polycrystalline silicon.

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