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61. 发明公开

EP3199514A1 METHOD FOR PRODUCING CYCLIC DIKETONE COMPOUND 有权
标题翻译：生产环状二酮化合物的方法
公开(公告)号：EP3199514A1
公开(公告)日：2017-08-02
申请号：EP15873042.4
申请日：2015-12-22
申请人： Kao Corporation
发明人： TANINO, Kenji , SAKODA, Daichi , SAKAMOTO, Shu
IPC分类号： C07C45/28 , C07C45/57 , C07C49/385 , C07C49/587 , C07B61/00
CPC分类号： C07C45/28 , B01J31/0239 , C01B15/01 , C01G41/02 , C07B61/00 , C07C45/57 , C07C45/64 , C07C45/66 , C07C49/385 , C07C49/587 , C07C49/487
摘要： Provided is a method for producing a compound represented by general formula (I) by oxidative cleavage of a compound of formula (II), which is a bicyclic tetrasubstituted olefin compound, using hydrogen peroxide. The method for producing a compound represented by general formula (I) includes a step of subjecting a compound represented by general formula (II) to oxidative cleavage using hydrogen peroxide in the presence of an acid catalyst or in the presence of a tungstic acid compound to obtain the compound represented by general formula (I):

[In the formulae, formula -A 1- (where the front bond denotes a bond that bonds with a carbon atom C 1 while the back bond denotes a bond that bonds with a carbon atom C 2 ) is an alkylene group having 2 to 6 carbon atoms that may have been substituted and that may further include an ether bond, an ester bond, a secondary amino group, a thioether group, or these, and formula -A 2 - (where the front bond denotes a bond that bonds with a carbon atom C 1 while the back bond denotes a bond that bonds with a carbon atom C 2 ) is an alkylene group having 4 to 10 carbon atoms that may have been substituted and that may further include an ether bond, an ester bond, a secondary amino group, a thioether group, or these.]
摘要翻译：本发明提供一种通过使用过氧化氢使作为二环式四取代烯烃化合物的式（II）的化合物氧化断裂来制造通式（I）所示的化合物的方法。通式（I）表示的化合物的制造方法包括在酸催化剂的存在下或在钨酸化合物的存在下，使用过氧化氢使通式（II）表示的化合物氧化分解的步骤，得到通式（I）所示的化合物：[式中，-A1-（前键表示与碳原子C1键合的键，后键表示与碳原子C2键合的键）是可以被取代的碳原子数2〜6的亚烷基，还可以进一步具有醚键，酯键，仲氨基，硫醚基或它们，式-A2-（前键表示与碳原子C1键合的键，而背键表示与碳原子C2键合的键）是可以被取代的具有4至10个碳原子的亚烷基，并且还可以包括醚键，酯键，一个secon 二芳基氨基，硫醚基或这些。]

62. 发明授权

EP2625158B1 VERFAHREN ZUR HERSTELLUNG VON KETONEN, INSBESONDERE MAKROCYCLISCHER KETONE 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VON KETONEN，INSBESONDERE MAKROCYCLISCHER KETONE
公开(公告)号：EP2625158B1
公开(公告)日：2014-08-13
申请号：EP11767683.3
申请日：2011-10-05
申请人： BASF SE
发明人： SCHELPER, Michael , STOCK, Christoph , EBEL, Klaus , TELES, Joaquim Henrique , PELZER, Ralf
IPC分类号： C07C45/28 , C07C45/62 , C07C49/385 , C07C49/587
CPC分类号： C07C45/28 , C07C45/62 , C07C2601/18 , C07C49/587 , C07C49/385

63. 发明授权

EP1697293B1 (Z)-7-CYCLOHEXADECEN-1-ON ALS RIECHSTOFF 有权转让
标题翻译：（Z）-7 - 环十六碳烯-1-酮，为加香
公开(公告)号：EP1697293B1
公开(公告)日：2008-08-13
申请号：EP04804574.4
申请日：2004-11-25
申请人： Symrise GmbH & Co. KG
发明人： RECKZIEGEL, Aurelia , WÖHRLE, Ingo , SONNENBERG, Steffen
IPC分类号： C07C49/587 , C07C45/66 , C07C45/64 , C07C49/487 , A61K8/18 , C11B9/00
CPC分类号： C11B9/0038 , C07C17/16 , C07C21/14 , C07C45/004 , C07C45/64 , C07C45/66 , C07C49/487 , C07C49/587 , C07C49/203
摘要： The invention relates to the use of compound (Z)-7-cyclohexadecene-1-one as a musk perfume. The invention also relates to mixtures of perfumes or aromatic agents comprising (Z)-7-cyclohexadecene-1-one and to one or more additional perfumes or aromatic agents.

64. 发明公开

EP1947078A1 Novel macrocyclic musk 有权
标题翻译： Neuartiger makrozyklischer Bisam
公开(公告)号：EP1947078A1
公开(公告)日：2008-07-23
申请号：EP08250151.1
申请日：2008-01-11
申请人： International Flavors & Fragrances, Inc.
发明人： Levorse Jr., Anthony T. , Newirth, Brett D
IPC分类号： C07C49/587 , A61K8/35
CPC分类号： C07C49/587 , C07C45/63 , C07C45/65 , C07C49/457 , C07C49/687 , C11B9/0038
摘要： The present invention is directed to novel compounds of the structure

and a method for enhancing a perfume composition by incorporating an olfactory acceptable amount of the compounds provided above.
摘要翻译：本发明涉及新颖的结构化合物和通过掺入嗅觉可接受量的上述提供的化合物来增强香料组合物的方法。

65. 发明授权

EP1270538B1 PROCESSES FOR THE PREPARATION OF MACROCYCLIC KETONES 有权
标题翻译：用于生产环酮MACRO
公开(公告)号：EP1270538B1
公开(公告)日：2005-08-24
申请号：EP01917557.9
申请日：2001-03-28
申请人： JAPAN ENERGY CORPORATION
发明人： TANABE, Yoo , MAKITA, Atsushi, Japan Energy Corporation
IPC分类号： C07C49/587 , C07C49/385 , C07C45/65 , C07C69/757 , C07C67/327
CPC分类号： C07C69/757 , C07C45/673 , C07C45/676 , C07C67/313 , C07C2601/18 , C07C49/587 , C07C49/385

66. 发明公开

EP1270538A1 PROCESSES FOR THE PREPARATION OF MACROCYCLIC KETONES 有权
标题翻译：用于生产环酮MACRO
公开(公告)号：EP1270538A1
公开(公告)日：2003-01-02
申请号：EP01917557.9
申请日：2001-03-28
申请人： Japan Energy Corporation
发明人： TANABE, Yoo , MAKITA, Atsushi, Japan Energy Corporation
IPC分类号： C07C49/587 , C07C49/385 , C07C45/65 , C07C69/757 , C07C67/327
CPC分类号： C07C69/757 , C07C45/673 , C07C45/676 , C07C67/313 , C07C2601/18 , C07C49/587 , C07C49/385
摘要： Disclosed are a process of subjecting a diester of a long-chain dicarboxylic acid having 18 to 21 carbon atoms to intramolecular condensation in the presence of titanium tetrachloride or zirconium tetrachloride and a trialkylamine to form an α-alkoxycarbonylated macrocyclic ketone, and a process for producing a macrocyclic ketone by hydrolyzing an α-alkoxycarbonylated macrocyclic ketone obtained by the process and then subjecting the hydrolyzate to decarboxylation. The invention provides a process for producing a macrocyclic ketone efficiently, which permits high concentration synthesis.

67. 发明授权

EP0955285B1 Process and apparatus for production of 5-cyclohexadecen-1-one 有权
标题翻译：用于制备5-环十六碳烯-1-酮的方法和装置
公开(公告)号：EP0955285B1
公开(公告)日：2001-11-14
申请号：EP99401101.3
申请日：1999-05-05
申请人： Takasago International Corporation
发明人： Itakura, Keisuke, Takasago International Corp. , Yamamoto, Kenichi, Takasago International Corp. , Yagi, Misao, Takasago International Corp. , Amano, Akira, Takasago International Corp.
IPC分类号： C07C45/51 , C07C49/587
CPC分类号： C07C49/587 , C07C45/512 , Y02P20/582

68. 发明公开

EP0742196A1 CYCLOOCTADIENE DERIVATIVE 失效
标题翻译：环辛二烯衍生物
公开(公告)号：EP0742196A1
公开(公告)日：1996-11-13
申请号：EP95907819.7
申请日：1995-02-01
申请人： NISSAN CHEMICAL INDUSTRIES LTD.
发明人： NAKAJIMA, Yasuyuki, Nissan Chemical Industries, , WATANABE, Hisayuki, Nissan Chemical Industries, , ADACHI, Michiaki, Nissan Chemical Industries, Ltd. , TAGAWA, Michito, Nissan Chemical Industries, Ltd. , FUTAGAWA, Mitsugu, Nissan Chemical Industries, Ltd , FURUSATO, Takashi, Nissan Chemical Industries, Ltd , OHYA, Hiroshi, Nissan Chemical Industries, Ltd. , NISHIOKA, Masanori, Nissan Chemical Industries Ltd
IPC分类号： C07C43/215 , C07C43/225 , C07C43/23 , C07C49/587 , C07C61/00 , C07C62/00 , C07C233/57 , C07C235/40 , C07D209/52 , C07D209/56 , C07D307/20
CPC分类号： C07D487/04 , C07C43/21 , C07C43/225 , C07C43/23 , C07C43/315 , C07C49/753 , C07C49/755 , C07C61/26 , C07C61/35 , C07C62/32 , C07C62/34 , C07C205/43 , C07C233/58 , C07C235/40 , C07C251/42 , C07C2601/18 , C07C2603/36 , C07D209/52 , C07D311/94 , C07D493/04 , C07F7/1856 , C07F9/6561
摘要： Cyclooctadiene derivative of the following formula (1):
wherein A 1 , A 2 , A 3 and A 4 each independently represent COOR 5 (where R 5 represents a hydrogen atom, a C 1 -C 10 alkyl group, a phenyl group, a C 7 -C 12 aralkyl group or CONR 6 R 7 (where R 6 and R 7 each independently represent a hydrogen atom, a C 1 -C 10 alkyl group or a phenyl group), or A 1 and A 2 , and/or A 3 and A 4 may be combined together to represent group(s) of:
in which X represents an oxygen atom or NR 8 {where R 8 represents a hydrogen atom, a C 1 -C 10 alkyl group or a phenyl group),
R 0 , R 1 , R 2 , R 3 and R 4 each independently represent a hydrogen atom, a halogen atom, a hydroxyl group and an C 1 -C 10 alkyl group,
the symbol --- represents a single or double bond, and when it is a double bond, then R 1 and R 3 each independently may represent an oxygen atom;
provided that the case where all of R 0 , R 1 , R 2 , R 3 and R 4 represent hydrogen atoms at the same time is excluded, and agrohorticultural fungicides, antimold agents and antithrombocytic agents containing said derivatives.
The compounds have superior fungicidal activity, antimold activity and activity for preventing platelet aggregation, and are useful as an agrohorticultural fungicide, an antimold agent and an antithrombocytic agent.

69. 发明公开

EP0455826A4 SUBSTITUTED OPEN-CHAIN TERPENE COMPOUND 失效
标题翻译：取代的开链化合物
公开(公告)号：EP0455826A4
公开(公告)日：1993-10-06
申请号：EP90917539
申请日：1990-11-29
申请人： MITSUBISHI KASEI CORPORATION
发明人： TAKAYANAGI, HISAO , KITANO, YASUNORI , MORINAKA, YASUHIRO
IPC分类号： C07C33/02 , C07C43/178 , C07C43/315 , C07C45/44 , C07C45/51 , C07C45/63 , C07C45/67 , C07C47/21 , C07C47/24 , C07C47/263 , C07C47/277 , C07C49/203 , C07C49/227 , C07C49/24 , C07C49/255 , C07C49/587 , C07C69/007 , C07C69/738 , C07C255/07 , C07C255/10 , C07C255/15 , C07C255/46 , C07C309/65 , C07D309/06 , C07D309/12 , C07F7/18 , C07C33/048 , C07C43/02 , C07C47/20 , C07C69/78 , C07C255/01 , C07C309/66 , C07C309/73
CPC分类号： C07F7/1856 , C07C33/02 , C07C43/178 , C07C43/315 , C07C45/44 , C07C45/512 , C07C45/516 , C07C45/63 , C07C45/673 , C07C45/676 , C07C47/21 , C07C47/24 , C07C47/263 , C07C47/277 , C07C49/203 , C07C49/227 , C07C49/24 , C07C49/255 , C07C49/587 , C07C69/007 , C07C69/738 , C07C255/07 , C07C255/10 , C07C255/15 , C07C255/46 , C07C309/65 , C07C2601/18 , C07D309/06 , C07D309/12 , C07F7/1852
摘要： A novel substituted open-chain terpene compound of general formula (I) which is useful as an intermediate for the synthesis of sarcophytol A, wherein R is (α), (β), or (γ) (wherein R1 is cyano or formyl R2 is hydrogen or CO¿2?R?3, R3 is C¿1 to C4 alkyl, and R4 is -C=CH or -CH=CH¿2?); X is hydrogen, hydroxyl, halogen, OR?5¿ or OSO¿2R?6 (wherein R5 is hydrogen, 1-alkoxyalkyl, tetrahydrofuryl, tetrahydropyranyl, acyl, or silyl substituted by C¿1? to C5 alkyl or phenyl, and R?6 is C¿1 to C4 alkyl which may be substituted by halogen or phenyl which may be substituted by C1 to C4 alkyl); and n is an integer of 0 to 2, provided that X is OR5 and n is O when R is (β) or (γ); X is neither halogen nor OSO¿2?R?6 when R1¿ is formyl; R2 is not hydrogen when R5 is hydrogen; and R3 is not methyl when R5 is 1-ethoxyethyl.
摘要翻译： Substd。式（I）的萜烯是新的。在（I）中R = CH = CHCHR1CH（CH3）2（gp.a），CH2CHR2COR3（gp.B）或CH2CH2C（OH）（R4）CH3（gp.c）; R1 = CN或CHO; R2 = H或CO2R3; R3 = 1-4C烷基; R4 = C = CH或CH = CH2; X = H，OH，卤素，OR 5或OSO 2 R 6; R5 = H，1-烷氧基烷基，四氢呋喃基，四氢吡喃基，酰基或甲硅烷基。 1-5C烷基或苯基; R6 = 1-4C烷基选择。 substd。通过卤素或苯基取代。 substd。通过1-4C烷基; n = 0-2; 条件是（i）当R = gp时。（b）或（c）X = OR5和n = O; （ii）当R1 = CHO时，X不为卤素或OSO2R6; （iii）当R5 = H时，R2不为H; （iv）当R5 = 1-乙氧基乙基时，则R3不是Me。

70. 发明公开

EP0322537A2 Verfahren zur Herstellung von cyclischen Ketonen durch Isomerisierung von Epoxiden 失效
标题翻译：一种用于通过环氧化物的异构化制备环酮的方法。
公开(公告)号：EP0322537A2
公开(公告)日：1989-07-05
申请号：EP88117877.6
申请日：1988-10-27
申请人： HÜLS AKTIENGESELLSCHAFT
发明人： Büschken, Wilfried, Dr.
IPC分类号： C07C45/58 , C07C49/385 , C07C49/413 , C07C49/587 , C07C49/607
CPC分类号： C07C45/58
摘要： Es war Aufgabe der Erfindung, ausgehend von Epoxiden, ein gegenüber dem Stand der Technik wenig aufwendiges, nur kurze Reaktionszeiten benötigendes und in bezug auf Peroxidbildung risikoloses Verfahren zu finden. Gemäß dem Stand der Technik wird insbesondere mit Diethylether als Lösungsmittel und Magnesiumverbindungen als Katalysator gearbeitet.
Die Lösung des Problems bestand in dem Einsatz polarer Lösungsmittel, wie z. B. N,N′-disubstituierten cyclischen Harnstoffen, in Gegenwart von Alkali- oder Erdalkalihalogeniden.
Die cyclischen Ketone insbesondere mit 15 bis 17 Kohlenstoffatomen werden als Riechstoffe eingesetzt.
摘要翻译：相比于现有技术，本发明的目的，由环氧化物开始，一个，相对不复杂的，只有短的反应时间需要它们，并找到与过氧化物形成无风险的程序。根据现有技术中特别是作为溶剂和镁的化合物作催化剂进行，用二乙醚。该问题的解决方案是使用极性溶剂，如，例如，N，N'-二取代的环状脲，在碱金属或碱土金属卤化物的存在下进行。环酮，特别是具有15至17个碳原子的被用作香料。

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