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51. 发明公开

EP0367104A3 Organopolysiloxan-Thioharnstoff-Derivate, Verfahren zu ihrer Herstellung und Verwendung 失效
标题翻译：有机聚硅氧烷尿素或有机聚硅氧烷三氧化物衍生物，制备它们的方法及其用途
公开(公告)号：EP0367104A3
公开(公告)日：1991-02-06
申请号：EP89119892.1
申请日：1989-10-26
申请人： Degussa Aktiengesellschaft
发明人： Panster, Peter, Dr. , Deschler, Ulrich, Dr.
IPC分类号： C08G77/48 , C08G77/54 , C08G77/58
CPC分类号： B01J20/22 , C08G77/54 , C08G77/58
摘要： Die Erfindung betrifft gegebenenfalls vernetzte Organopolysiloxan-Harnstoff- und Thioharnstoff-Derivate aus
wobei
x = 0 oder S und R 1 ist
Darin ist R 5 eine Alkylengruppe, Cycloalkylengruppe oder
R 2 hat dieselbe Bedeutung wie R 1 oder ist H. R 3 und R haben ebenfalls dieselbe Bedeutung wie R' oder sind H oder eine Alkylgruppe. Mindestens zwei, aber höchstens drei Gruppen nach Formel (2) sind an die Einheiten nach Formel (1) gebunden. Die freien Valenzen der an das Siliciumatom gebundenen Sauerstoffatome sind durch Siliciumatome weiterer Gruppen der Formel (2), gegebenenfalls unter Einbau von Vernetzern, abgesättigt. Ferner werden Herstellungsverfahren für die Produkte und Verwendung zur Entfernung von gelösten Metallen aus flüssigen Phasen angegeben.

52. 发明公开

EP0367222A2 Durch Organooligosilsesquioxane vernetzte Silicone 失效
标题翻译：由有机低聚硅倍半氧烷交联的有机硅
公开(公告)号：EP0367222A2
公开(公告)日：1990-05-09
申请号：EP89120188.1
申请日：1989-10-31
申请人： WACKER-CHEMIE GMBH
发明人： Weidner, Richard, Dr. Dipl.-Chem. , Zeller, Norbert, Dr. Dipl.-Chem. , Deubzer, Bernward, Dr. Dipl.-Chem. , Frey, Volker, Dr. Dipl.-Chem.
IPC分类号： C08G77/06 , C08G77/22 , C08G77/48 , C08G77/38
CPC分类号： C08G77/22 , C08G77/045 , C08G77/485
摘要： Die Erfindung betrifft Verbindungen der Formel
worin

z die Zahl 6, 8 oder 10 ;
R gleiche oder verschiedene Reste der Formeln
sind, mit der Maßgabe, daß bis zu z-1 der Reste R auch Reste der Formel -O-SiR' 3 sein können, wobei X jeweils einen einwertigen bzw. einen halben zweiwertigen Rest der Formeln

bedeuten, und R', R", R'", Z, Y und n die in der Beschreibung angegebenen Bedeutungen haben, Verfahren zur Herstellung dieser Verbindungen sowie deren Verwendung.
摘要翻译：本发明涉及下式的化合物：其中z是数字6,8或10; [R相同或不同，条件是最多的基团R的Z-1和下式的基团可以是下式的基团-O-SIR“3，其中每个X为一价或平均半二价基团式和R'，R“，R”'，Z，Y和n具有说明书中给出的含义，制备这些化合物的方法及其用途。

53. 发明公开

EP0367105A2 Organosiloxanamin-Copolykondensate, Verfahren zu ihrer Herstellung und Verwendung (II) 失效
标题翻译：有机硅氧烷 - 共聚降解物，Verfahren zu ihrer Herstellung und Verwendung（II）。
公开(公告)号：EP0367105A2
公开(公告)日：1990-05-09
申请号：EP89119893.9
申请日：1989-10-26
申请人： Degussa Aktiengesellschaft
发明人： Panster, Peter, Dr. , Grethe, Horst , Kleinschmit, Peter, Dr.
IPC分类号： C08G77/48 , C08G77/26 , C08G77/54
CPC分类号： C08G77/26 , B01J20/22 , C08G77/54 , C08G77/58
摘要： Die Erfindung betrifft Organosiloxanamin-Copolykondensate als statistische- oder Block-Copolykondensate oder Gemische davon aus
und X - R 4 (II) R 1 bis R 4 ist
R 5 ist direkt an das Stickstoffatom bzw. den einbindigen Rest X gebunden und ist eine Alkylengruppe, Cycloalkylengruppe oder

Darin ist n 1 bis 6 und m 0 bis 6. Die freien Valenzen der an das Siliciumatom gebundenen Sauerstoffatome sind durch Siliciumatome weiterer Gruppen der Formel (III), gegebenenfalls unter Einbau von Vernetzern. abgesättigt, X steht für

-NH 2 , -NH-(CH 2 ) 2 -NH 2 ,
-NH-(CH 2 ) 2 -NH-(CH 2 ) 2 -NH 2 ,
-Cl, -Br, -J, -SH, -P(C 6 H 5 ) 2 ,

wobei R" H oder eine Alkylgruppe ist. Ferner werden Herstellungsverfahren und Verwendung der Verfahrensprodukte zur Entfernung gelöster Metalle aus Lösungen oder zur Adsorption von organischen Lösungsmitteln angegeben.
摘要翻译：本发明涉及有机硅氧烷 - 胺共聚缩合物作为无规或嵌段共聚缩合物或其混合物与...（X-R 4）（II）。 ... <？> R 1至R 4是... ...。 ... R 5直接键合到氮原子或单键连接的基团X上，并且是亚烷基，亚环烷基或... ...或... ...。在这些式中，n为1〜6，m为0〜6。如果合适，则与硅原子键合的氧原子的自由价饱和为式（III）的其它基团的硅原子并入交叉连接器。 X代表-NH2，-NH-（CH2）2-NH2，-NH-（CH2）2-NH-（CH2）2-NH2，-Cl，-Br，-I，-SH，-P（C6H5） 2，... ...其中R“是H或烷基。还给出了制备方法以及用于从溶液中除去溶解的金属或吸附有机溶剂的方法产物的用途。

54. 发明公开

EP0307098A2 Polyalkoxysilylalkylenedisilazanes and silylamines 失效
标题翻译：聚烷氧基甲硅烷基烷基二硅氮烷和硅烷胺。
公开(公告)号：EP0307098A2
公开(公告)日：1989-03-15
申请号：EP88307612.7
申请日：1988-08-17
申请人： DOW CORNING CORPORATION
发明人： Krahnke, Robert Harold , Saam, John Carlton
IPC分类号： C07F7/18 , C08G77/48
CPC分类号： C07F7/1836 , C08G77/50 , C08L83/14
摘要： A polyalkoxysilylalkylenedisilazane of the formula
and a polyalkoxysilylalkylenesilylamine of the formula
where x is 0 or 1; R is a saturated alkyl or aryl radical or mixture of radicals; R′ is alkyl, aryl, or cellosolve radical, or mixture of radicals; R˝ is hydrogen, alkyl, aryl, or arylalkyl radical or mixture of radicals; and A is a divalent hydrocarbon radical having 2 to 20 carbon atoms; and a method for their manufacture by the platinum catalyzed addition of an alkenyl-functional disilazane or silylamine with an alkoxy-functional silicon hydride is disclosed. The silylamine can also be produced by the platinum catalyzed addition of a SiH functional silazane or silylamine and an alkenyltrialkoxysilane. The polyalkoxysilylalkylenedisilazane and the polyalkoxysilylalkylenesilylamine can be reacted with a silanol containing polyorganosiloxane such as a hydroxyl endblocked polydiorganosiloxane in the presence of an acidic catalyst to give a polyalkoxysilyl terminated polydiorganosiloxane in which the terminal groups are bonded to the polymer through an alkylene linkage.
摘要翻译：式CHEM的聚烷氧基甲硅烷基亚烷基二硅氮烷和式CHEM的聚烷氧基甲硅烷基亚烷基二胺其中x为0或1; R是饱和的烷基或芳基或基团的混合物; R min是烷基，芳基或溶纤剂基团，或自由基的混合物; R sec是氢，烷基，芳基或芳基烷基或基团的混合物; A为碳原子数2〜20的二价烃基，并且公开了通过铂催化加成烯基官能的二硅氮烷或甲硅烷基胺与烷氧基官能的氢化硅来制造的方法。甲硅烷胺也可以通过铂催化加成SiH官能硅氮烷或甲硅烷基胺和烯基三烷氧基硅烷来制备。聚烷氧基甲硅烷基亚烷基二硅氮烷和聚烷氧基甲硅烷基亚烷基二甲胺可以在酸性催化剂存在下与含硅烷醇的聚有机硅氧烷如羟基封端的聚二有机硅氧烷反应，得到其中端基通过亚烷基键与聚合物结合的聚烷氧基甲硅烷基封端的聚二有机硅氧烷。

55. 发明公开

EP0303616A4 METHODS FOR THE SYNTHESIS OF POLYSILANES. 失效
标题翻译：用于生产聚硅烷。
公开(公告)号：EP0303616A4
公开(公告)日：1989-01-26
申请号：EP87903115
申请日：1987-04-14
申请人： ZEIGLER JOHN M
发明人： ZEIGLER JOHN M
IPC分类号： C07F7/08 , C08G77/48 , C08G77/60 , C07F7/04
CPC分类号： C08G77/60
摘要： A method of controlling the yield of polysilane of a desired molecular weight and/or polydispersity prepared in a reductive condensation of corresponding silane monomers on a solid catalyst dispersed in an inert solvent for both the monomers and the growing polymer chains, comprises determining the variation of molecular weight and/or polydispersity of the polysilane as a function of the solubility of the polysilane in reaction solvent, determining thereby a chosen optimum solubility of the polysilane in solvent for obtaining a desired yield of polysilane of said desired molecular weight and/or polydispersity, and thereafter carrying out the preparation of the polysilane in a solvent in which the polysiland has said chosen optimum solubility.

56. 发明公开

EP0202108A3 Phospho-boro-silanol interlayer dielectric films and preparations 失效
标题翻译：磷光体 - 硅铝酸盐介质膜和制备
公开(公告)号：EP0202108A3
公开(公告)日：1988-06-15
申请号：EP86303627
申请日：1986-05-13
申请人： STAUFFER CHEMICAL COMPANY
发明人： Estes, William Edward , Marsh, Wayne Edward
IPC分类号： C08G77/56 , C08G77/48 , H01B03/00 , C09D03/82 , C08G77/00 , C08G77/30 , H01B03/46 , B32B27/28
CPC分类号： C08G77/56 , C08G77/48 , H01B3/46 , Y10T428/31663
摘要： There are disclosed certain categories of novel spin-coating compositions comprising phosphorus-doped and/or boron-doped silsesquioxane oligomers. Cured interlayer dielectric films prepared therefrom have a superior combination of defined properties, particularly including adhesion (of single-coat and multiple coats) and/or resistance against degradation at temperatures above 500°C. The spin-coating compositions are prepared in a critical manner from critical raw materials.

57. 发明公开

EP0231497A1 Silicone resist materials containing polysiloxanes 失效
标题翻译： “抗性硅”的材料，聚硅氧烷化合物。
公开(公告)号：EP0231497A1
公开(公告)日：1987-08-12
申请号：EP86117468.8
申请日：1986-12-16
申请人： KABUSHIKI KAISHA TOSHIBA
发明人： Onishi, Yasuobu , Hayase, Shuji , Hayase, Rumiko , Hirata, Akiko
IPC分类号： C08G77/60 , C08G77/14 , C08G77/48 , C08G77/26 , C08L83/06 , C08L83/16 , G03F7/26 , G03F7/075
CPC分类号： C08L83/16 , C08G77/14 , C08G77/26 , C08G77/48 , C08G77/60 , G03F7/0754 , G03F7/0757
摘要： The polysilanes and polysiloxanes of the present invention are polymers that contain silicon in the principal chain, and contain the side chains alkaline soluble groups such as phenol-based hydroxy group and carboxyl group.
One silicone resist material of the present invention comprises the polysilane or the polysiloxane in the above.
Another silicone resist material of the present invention contains the above polysilane or polysiloxane, and an appropriate photosensitive agent.
Still another silicone resist material of the present invention does not contain the above photosensitive agent, and in its stead, it contains a group that possesses photosensitive to ultraviolet rays or the like, via a siloxane bonding in the principal chain. As a substance with such photosensitivity, one may mention, for example, o-nitrobenzylsilyl groups that presents alkaline solubility when it is irradiated by ultraviolet rays.
Accordingly, the silicone resist materials of the present invention, especially the second and third silicone resist materials, are alkaline developable, and also possess a superior resistance to oxygen plasma. Therefore, they can be used as a top layer film in the two-layered resist system, making it possible to form very fine resist patterns, fast and with a minimum number of processing steps. Methods of manufacturing the polysilanes and polysiloxanes as well as of the resist materials are also disclosed.

58. 发明公开

EP0202108A2 Phospho-boro-silanol interlayer dielectric films and preparations 失效
标题翻译：在介电膜的磷和含硼硅烷醇的中间层中的应用。
公开(公告)号：EP0202108A2
公开(公告)日：1986-11-20
申请号：EP86303627.3
申请日：1986-05-13
申请人： National Starch and Chemical Investment Holding Corporation
发明人： Estes, William Edward , Marsh, Wayne Edward
IPC分类号： C08G77/56 , C08G77/48 , H01B3/00 , C09D3/82 , C08G77/00 , C08G77/30 , H01B3/46 , B32B27/28
CPC分类号： C08G77/56 , C08G77/48 , H01B3/46 , Y10T428/31663
摘要： There are disclosed certain categories of novel spin-coating compositions comprising phosphorus-doped and/or boron-doped silsesquioxane oligomers. Cured interlayer dielectric films prepared therefrom have a superior combination of defined properties, particularly including adhesion (of single-coat and multiple coats) and/or resistance against degradation at temperatures above 500°C. The spin-coating compositions are prepared in a critical manner from critical raw materials.

59. 发明公开

EP0041541A4 MERCAPTOORGANOPOLYSILOXANES. 失效
标题翻译： MERCAPTOORGANOPOLYSILOXANE。
公开(公告)号：EP0041541A4
公开(公告)日：1982-05-10
申请号：EP81900106
申请日：1980-11-10
申请人： DOW CORNING
发明人： HOMAN GARY REX , BLEVINS JAN MARGARET
IPC分类号： C08L83/04 , C08G77/00 , C08G77/04 , C08G77/22 , C08G77/28 , C08G77/38 , C08G77/48
CPC分类号： C08G77/28 , C08G77/045

60. 发明公开

EP0031994A2 Organopolysiloxanes that contain sulfur and curable compositions including the same 失效
标题翻译：有机聚硅氧烷和含有这些可固化组合物的含硫。
公开(公告)号：EP0031994A2
公开(公告)日：1981-07-15
申请号：EP80304154.0
申请日：1980-11-20
申请人： DOW CORNING CORPORATION
发明人： Homan, Gary Rex , Lee, Chi-Long
IPC分类号： C08G77/48 , C08L83/14 , C08K5/00 , C08J3/24
CPC分类号： C08G77/50 , C08G77/392 , C08L83/14
摘要： Novel sulfur-containing organopolysiloxanes consisting essentially of a combination of units selected from dimethyl- siloxane units, trimethylsiloxane units, sulfur-containing siloxane units of the formula
and pendent sulfur-containing siloxane units of the formula

wherein: Rand R 1 are the same of different and selected from the group consisting of methyl and ethyl;

x has a value of 2 or 3;
a has a value of 0 or 1;

A and B are the same or different and selected from among the group consisting of divalent radicals of the formulas
and wherein: m and n are the same or different and have a value of from 2 to 4 inclusive, and trivalent radicals having the formula
forming a silacyclopentamer by attachment ofthe(+) bond to a sulfur atom and the other two bonds to the same silicon atom;

R 2 is a monovalent radical selected from the group consisting of alkyl and alkoxy radicals having from 1 to 3 carbon atoms inclusive and phenyl radical;

b has a value of 1 or 2;
R' is a methyl or ethyl;
c has a value of 0 or 1;

provided that (1) in the divalent radical, no carbon atom is attached to both a silicon atom and a sulfur atom; (2) when A is a trivalent radical, x is 2 and a is 0; (3) when B is a trivalent radical,b is 1 and is 0; and (4) when B is a divalent radical is 2 and c is 1; said organopolysiloxane containing an average of at least two sulfur-containing siloxane units per molecule and no more than 10 mole percent pendent sulfur-containing siloxane units based on the total number of siloxane units in the organopolysiloxane. Mixtures of such sulfur-containing organopolysiloxanes with a suitable catalyst provide useful compositions curable to elastomers at room temperature.

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