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51. 发明公开

EP1170389A2 Improved beta-diketones for the extraction of copper from aqueous ammoniacal solutions 失效
标题翻译： Verbesserte Beta-Diketonefürdie Extraktion von Kupfer aus ammoniakalischenLösungen
公开(公告)号：EP1170389A2
公开(公告)日：2002-01-09
申请号：EP01116257.5
申请日：1997-01-30
申请人： HENKEL CORPORATION
发明人： Virnig, Michael J. , Kordosky, Gary A.
IPC分类号： C22B3/26 , C22B15/00 , C07C49/12
CPC分类号： C07C45/455 , C07C45/68 , C07C49/76 , C07C49/782 , C22B3/0021 , C22B15/0078 , Y02P10/234 , Y02P10/236
摘要： A process for recovery of copper from an aqueous ammoniacal solution containing copper values comprising:

(A) contacting a copper pregnant aqueous ammoniacal solution containing copper values with a water insoluble beta-diketone copper extractant dissolved in a water-immiscible organic solvent to extract copper values from said aqueous ammoniacal solution into said organic solution thereby forming a copper pregnant organic phase and a copper depleted aqueous phase;
(B) separating said aqueous phase and said organic phase;
(C) contacting the copper pregnant organic phase with an aqueous acidic stripping solution;
(D) separating said aqueous acidic stripping solution now containing the copper values from the organic phase; and
(E) recovering the copper from said aqueous acidic stripping solution; characterized in that the beta-diketone extractant being a highly sterically hindered beta-diketone selected from beta-diketones of formula II:
where R is phenyl or alkyl substituted phenyl, R' is alkyl having from above 1 to 8 carbon atoms, and R", R"' and R"" are the same or different and are chosen from the group consisting of H, alkyl having from 1 to 8 carbon atoms, and aralkyl having from 7 to 14 carbon atoms, with the proviso that (a) less than two of R", R"' and R"" are H and (b) the total number of carbons in all R groups is at least 13.
摘要翻译：一种从含有铜含量的氨水溶液中回收铜的方法，包括：（A）将含铜铜的怀孕的含水氨水溶液与溶解在与水不混溶的有机溶剂中的水不溶性β-二酮铜提取剂接触以提取铜值从所述氨水溶液中加入所述有机溶液，从而形成铜怀孕的有机相和贫铜的水相; （B）分离所述水相和所述有机相; （C）将铜怀孕的有机相与含水酸性剥离溶液接触; （D）从有机相中分离现在含有铜值的酸性水溶液; 和（E）从所述酸性酸性剥离溶液中回收铜; 其特征在于β-二酮萃取剂是高度位阻的β-二酮，其选自式II的β-二酮：其中R是苯基或烷基取代的苯基，R'是具有1-8个碳原子的烷基，并且R“，R”'和R“”相同或不同，并且选自H，具有1至8个碳原子的烷基和具有7至14个碳原子的芳烷基，条件是（ a）R“，R”'和R“”中的少于两个为H，（b）所有R基团中的碳总数至少为13。

52. 发明授权

EP1012351B1 CHLORIDE ASSISTED HYDROMETALLURGICAL EXTRACTION OF COPPER FROM SULPHIDE ORE MATERIALS 有权
标题翻译：酰氯离子支持HYDRO冶金提取从氯化铜SULFIDERZROHSTOFFEN
公开(公告)号：EP1012351B1
公开(公告)日：2002-01-09
申请号：EP98939458.0
申请日：1998-08-14
申请人： COMINCO ENGINEERING SERVICES LTD.
发明人： JONES, David, L.
IPC分类号： C22B15/00 , C22B3/06 , C22B3/08 , C22B3/10 , C22B3/26
CPC分类号： C22B23/043 , C22B3/0005 , C22B3/06 , C22B3/08 , C22B15/0067 , C22B15/0069 , C22B15/0071 , C22B15/0084 , C22B15/0089 , C22B23/0415 , C22B23/0423 , C22B23/0476 , Y02P10/214 , Y02P10/234 , Y02P10/236
摘要： A process for the extraction of copper from a sulphide ore or concentrate comprises the steps of subjecting the ore or concentrate to pressure oxidation in the presence of oxygen and an acidic solution containing halide and sulphate ions to obtain a resulting pressure oxidation slurry. The slurry is subjected to a liquid/solid separation step to obtain a resulting pressure oxidation filtrate and a solid residue containing an insoluble basic metal sulphate salt. The basic metal sulphate salt is leached in a second leaching with an acidic sulphate solution to dissolve the basic metal salt to produce a leach liquor containing a metal sulphate, e.g. copper sulphate, in solution and a resulting solid residue. The leach liquor is separated from the solid residue and subjected to a solvent extraction process to produce metal concentrate solution and a metal depleted raffinate. At least a portion of the raffinate is recycled to the pressure oxidation.

53. 发明公开

EP1129225A1 SULFATISATION PROCESS FOR METAL EXTRACTION FROM SULFIDE ORES 有权
标题翻译：硫酸用于获得金属不受硫化矿石
公开(公告)号：EP1129225A1
公开(公告)日：2001-09-05
申请号：EP00954878.5
申请日：2000-08-29
申请人： Joma Chemical AS
发明人： FLAX, Solomon
IPC分类号： C22B1/06 , C22B19/02 , C22B15/00 , C22B19/20 , C22B3/08 , C22B23/00
CPC分类号： C22B19/22 , C22B1/06 , C22B15/0071 , C22B19/02 , C22B23/005 , Y02P10/234 , Y02P10/236
摘要： The invention provides a hydrometallurgical process for treating metal-containing sulfide ores and concentrates, comprising reacting said metal-containing sulfide with concentrated sulfuric acid at a temperature of between about 300 °C and 400 °C in the presence of oxygen to produce a solid metal sulfate product and a gaseous product which is primarily SO3, wherein said metal is selected from the group consisting of iron, copper, zinc, nickel, cobalt and manganese. Said metal sulfate product is then leached with dilute sulfuric acid to form a metal-containing solution, from which the metal values are separated by precipitation at raised H2SO4-concentrations obtained by saturating the solution with the gaseous SO3 from the sulfatization reaction step.

54. 发明公开

EP1063307A2 Method for recovering copper by solvent extraction in alternate steps 失效
标题翻译： Verfahren zur Kupfergewinnung durchFlüssig-FlüssigExtraktion in abwechselnden Stufen
公开(公告)号：EP1063307A2
公开(公告)日：2000-12-27
申请号：EP00120604.4
申请日：1996-05-30
申请人： HENKEL CORPORATION
发明人： Virnig, Michael , Mackenzie, J.
IPC分类号： C22B3/30 , C22B15/00 , B01D11/04 , C25C1/12
CPC分类号： C22B15/0084 , C22B3/0012 , C22B3/0017 , C25C1/12 , Y02P10/234 , Y02P10/236
摘要： An improved process is described for the recovery of copper from an aqueous feed solution using solvent extraction and electrowinning in which the electrowinning is conducted in a first step wherein the electrolyte is flowing perpendicular to the cathode surface without auxiliary mixing of the electrolyte between electrodes, and a second step wherein the electrolyte is flowing parallel to the cathode surface. In a second embodiment, solvent extraction of copper and solvent extraction of acid are conducted in alternate steps to allow more complete recovery of copper.
摘要翻译：描述了一种改进的方法，用于使用溶剂萃取和电解提取来从含水进料溶液中回收铜，其中电解提取优选在第一步骤中进行，其中电解液垂直于阴极表面流动，而不在电极之间辅助混合电解质，以及第二步骤，其中电解液平行于阴极表面流动。用第一种有机萃取剂溶液从含水进料溶液中萃取铜，并从贫去铜的水溶液中萃取酸并用第二种有机萃取剂溶液萃取酸，以交替的步骤进行铜的更完全回收。

55. 发明公开

EP1044969A3 Processes and intermediates for preparing anti-cancer compounds 有权
标题翻译：方法和中间体用于制备抗癌药物
公开(公告)号：EP1044969A3
公开(公告)日：2000-11-29
申请号：EP00302256.3
申请日：2000-03-20
申请人： Pfizer Products Inc.
发明人： Lehner, Richard Shelton , Norris, Timothy , Santafianos, Dinos Paul
IPC分类号： C07D239/94 , C07F7/08
CPC分类号： C22B15/0004 , C07D239/94 , C07F7/0812 , C22B15/0071 , Y02P10/236
摘要： The present invention relates to methods and intermediates for preparing compounds of the formula 1 and the pharmaceutically acceptable salts and solvates thereof, as well as structurally related compounds, wherein R 1 , R 2 and R 15 are as defined herein. The foregoing compounds are useful in the treatment of hyperproliferative disorders, such as cancers, in mammals. The present invention also relates to a method of preparing compounds of the formula 9 and the pharmaceutically acceptable salts and solvates thereof, wherein R 6 -R 10 and R 15 are as defined herein.

56. 发明公开

EP0958390A1 IMPROVEMENT IN THE PROCESS OF RECOVERY OF METALS 失效
标题翻译：改进的金属回收过程
公开(公告)号：EP0958390A1
公开(公告)日：1999-11-24
申请号：EP97954561.0
申请日：1997-12-22
申请人： HENKEL CORPORATION
发明人： VIRNIG, Michael, J. , KORDOSKY, Gary, A. , WOLFE, George, A. , MACKENZIE, J., Murdoch
IPC分类号： C01G3 , C01G9 , C01G53 , C22B3 , C22B15
CPC分类号： C01G3/003 , C01G9/003 , C01G53/003 , C22B3/0017 , C22B15/0078 , C22B23/0446 , Y02P10/234 , Y02P10/236
摘要： An improved process for the extraction of a metal from an aqueous ammoniacal solution comprising: (i) contacting the aqueous ammoniacal solution with an extraction reagent comprised of a water insoluble extractant for the metal, to provide an organic phase, now containing metal values, and an aqueous phase from which metal values have been extracted; (ii) contacting the organic phase with an aqueous stripping solution to provide an aqueous strip phase, now containing metal values, and an organic phase from which metal values have been stripped; and (iii) recovering the metal values from the aqueous stripping solution; the improvement wherein (a) the extraction reagent contains an ammonia antagonist having only hydrogen bond acceptor properties; (b) the stripping solution is an aqueous highly acidic solution; and (c) the organic phase is washed with a weakly acidic aqueous solution prior to stripping with the highly acidic aqueous stripping solution. The extractant is preferably an oxime extractant, either a ketoxime or an aldoxime. The preferred hydrocarbon solvent is kerosene and the preferred antagonist is 2,2,4-trimethylpentane-1,3-diol diisobutyrate.

57. 发明公开

EP0924307A1 Solvent extraction of cobalt and nickel values from a magnesium containing solution 失效
标题翻译： Füssig-flüssig-Extraktion von Kobalt und Nickel aus einer magnesiumhaltigenLösung
公开(公告)号：EP0924307A1
公开(公告)日：1999-06-23
申请号：EP98204323.4
申请日：1996-06-07
申请人： COMINCO ENGINEERING SERVICES LTD.
发明人： Jones, David L.
IPC分类号： C22B23/00 , C22B3/26 , C22B3/30 , C22B3/38 , C22B26/22
CPC分类号： C22B3/10 , C22B3/0005 , C22B3/0066 , C22B3/06 , C22B3/08 , C22B3/20 , C22B3/42 , C22B11/00 , C22B15/0067 , C22B15/0069 , C22B15/0071 , C22B15/0084 , C22B15/0089 , C22B19/22 , C22B19/26 , C22B23/0415 , C22B23/0423 , C22B23/043 , C22B23/0453 , Y02P10/234 , Y02P10/236
摘要： A process for the extraction of nickel and/or cobalt values from a solution comprises the steps of effecting a cobalt solvent extraction in the presence of magnesium ions with a cobalt extractant to produce a cobalt extractant loaded with cobalt ions and a first raffinate containing nickel and magnesium ions in solution. The first raffinate is subjected to magnesium solvent extraction with a magnesium extractant to produce a magnesium extractant loaded with magnesium and cobalt ions and a second raffinate. The second raffinate is subjected to nickel solvent extraction with a nickel extractant to produce a nickel loaded extractant and a third raffinate.
摘要翻译：从溶液中提取镍和/或钴值的方法包括以下步骤：在镁离子存在下用钴提取剂进行钴溶剂萃取以产生负载有钴离子的钴提取剂和含镍的第一萃余液和溶液中的镁离子。用镁提取剂对第一残液进行镁溶剂萃取以产生负载有镁和钴离子的镁提取剂和第二残液。将第二萃余液用镍萃取剂进行镍溶剂萃取以产生负载镍的萃取剂和第三萃余液。

58. 发明公开

EP0745439A3 Process for removing heavy metals from soil 失效
标题翻译：一种用于去除从土壤中重金属的方法
公开(公告)号：EP0745439A3
公开(公告)日：1999-02-24
申请号：EP96113210.7
申请日：1992-09-15
申请人： COGNIS, INCORPORATED
发明人： Fristad, William E. , Virnig, Michael J. , Cassel, Jonathan M. , Elliott, Dana K.
IPC分类号： B09C1/02
CPC分类号： C22B43/00 , B03B5/00 , B09B3/0016 , B09C1/02 , B09C1/10 , C22B1/005 , C22B3/06 , C22B3/1616 , C22B3/165 , C22B3/24 , C22B3/42 , C22B3/46 , C22B7/007 , C22B13/04 , C22B13/045 , C22B15/0067 , C22B25/04 , C22B25/06 , Y02P10/228 , Y02P10/234 , Y02P10/236
摘要： Heavy metals are efficiently removed from contaminated soil by a process which comprises leaching or washing the soil with a mild leachant solution comprised of an aqueous solution of an acid and a salt. Heavy metals are also efficiently removed from paint chips by washing with an aqueous acid. The heavy metals are recovered from the leachant be cementation.

59. 发明授权

EP0647721B1 Agent for treating metal ions in an aqueous solution, process for producing the metal ion-treating agent and method for treating metal ions in an aqueous solution 失效
标题翻译：剂用于治疗其制备在水溶液中的金属离子，处理和过程在水溶液中处理的金属离子
公开(公告)号：EP0647721B1
公开(公告)日：1998-12-23
申请号：EP94114056.8
申请日：1994-09-07
申请人： KAWASAKI KASEI CHEMICALS LTD.
发明人： Sakurai, Tatsuya, c/o Kawasaki Kasei Chem. Ltd. , Fujimura, Hiroshi, c/o Kawasaki Kasei Chem. Ltd. , Kusabe, Koji, c/o Kawasaki Kasei Chem. Ltd. , Hata, Keishiro, c/o Kawasaki Kasei Chem. Ltd.
IPC分类号： C22B3/24 , C22B7/00 , G03C5/00 , G03C5/395 , G03C11/24 , C02F1/70
CPC分类号： C22B11/04 , C22B3/44 , C22B15/0084 , C22B43/00 , Y02P10/234 , Y02P10/236 , Y10S423/14 , Y10S526/915

60. 发明公开

EP0871800A1 METHOD FOR RECOVERING COPPER 失效
标题翻译：一种获得铜
公开(公告)号：EP0871800A1
公开(公告)日：1998-10-21
申请号：EP96926958.0
申请日：1996-05-30
申请人： HENKEL CORPORATION
发明人： VIRNIG, Michael, J. , MACKENZIE, J., Murdoch
IPC分类号： C22B3 , C22B15 , C25C1
CPC分类号： C22B15/0084 , C22B3/0012 , C22B3/0017 , C25C1/12 , Y02P10/234 , Y02P10/236
摘要： An improved process is described for the recovery of copper from an aqueous feed solution using solvent extraction and electrowinning in which the electrowinning is conducted in a first step (EW1) wherein the electrolyte is flowing perpendicular to the cathode surface without auxiliary mixing of the electrolyte between electrodes, and a second step (EW2) wherein the electrolyte is flowing parallel to the cathode surface. In a second embodiment, solvent extraction of copper and solvent extraction of acid are conducted in alternate steps to allow more complete recovery of copper.

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