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51. 发明公开

EP2373578A1 VORRICHTUNG UND VERFAHREN FÜR KATALYTISCHE GASPHASENREAKTIONEN SOWIE DEREN VERWENDUNG 审中-公开
标题翻译： VORRICHTUNG UND VERFAHRENFÜRKATALYTISCHE GASPHASENREAKINGEN SOWIE DEREN VERWENDUNG
公开(公告)号：EP2373578A1
公开(公告)日：2011-10-12
申请号：EP09767960.9
申请日：2009-12-01
申请人： Uhde GmbH
发明人： SCHWEFER, Meinhard , GROVES, Michael , FUCHS, Jürgen , MAURER, Rainer , SIEFERT, Rolf , HÜNDGEN, Bernhard
IPC分类号： C01B21/20 , B01J8/00 , B01J8/02 , B01J19/00 , B01J12/00 , B01J15/00
CPC分类号： B01J8/0285 , B01J8/008 , B01J8/025 , B01J8/0278 , B01J12/007 , B01J15/005 , B01J19/0013 , B01J19/002 , B01J19/2485 , B01J19/26 , B01J2208/00203 , B01J2208/00212 , B01J2208/00495 , B01J2208/00548 , B01J2208/00716 , B01J2219/00083 , B01J2219/00094 , B01J2219/00119 , B01J2219/00155 , B01J2219/00164 , B01J2219/00245 , B01J2219/32296 , B01J2219/324 , C01B21/26 , C01B21/267 , C01B21/28 , C01C3/022
摘要： The invention relates to improved reactors for catalytic, exothermal gas phase reactions having an entrance zone (1), a reaction zone (2) comprising at least one catalyst (4) and an outlet zone (3) for the product gas, viewed in the flow direction of a reactant gas comprising at least one oxidizing agent and at least one component to be oxidized. The reactors have means, such as insulating jackets (6) and/or devices for transporting coolant, at least in the region of the entrance zone (1), wherein said coolants reduce the transport of heat generated in the reaction zone (2) into the entrance zone (1) and thus reduce the risks of advanced ignition of the reactant gas mixture used or the development of undesired secondary reactions in the entrance zone (1) and/or wherein the inside walls of the reactor are designed from inert material, at least in the region of the entrance zone (1). The reactant gas enters the entrance zone (1) as a homogenous gas mixture, with regard to the material composition thereof, via one or more supply lines (30). The reactors can be used particularly for ammonia oxidation, such as in nitric acid systems, in which preferably honeycombed transition metal catalysts having small cross-sections are used as the platinum nets that are conventionally employed.
摘要翻译：改进的反应器，用于在进料气体的流动方向上看到催化，放热气相反应，其包含至少一种氧化剂和至少一种待氧化的组分，入口区域（1），反应区域（2）描述了至少一种用于产品气体的催化剂（4）和出口区（3）。至少在入口区域（1）的区域中的反应器具有例如绝缘套（6）和/或用于输送冷却剂的装置的装置，其减少反应区（2）中产生的热量的传输）进入入口区（1），从而降低进料区（1）中所采用的进料气体混合物的预点燃或不期望的副反应过程的风险，和/或其中反应器的内壁在至少在进入区域（1）的区域，由惰性材料制成。进料气体通过一个或多个进料管线（30）相对于其物质组合物作为均匀气体混合物进入入口区域（1）。反应器可以特别用于氨氧化，例如在硝酸设备中，其中使用优选以蜂窝形式形成的过渡金属催化剂，其具有比通常使用的铂网格更小的横截面。

52. 发明公开

EP2202201A1 Ammonia oxidation catalysts 有权转让
标题翻译： AMMONIAKOXIDATIONSKATALYSATOREN
公开(公告)号：EP2202201A1
公开(公告)日：2010-06-30
申请号：EP08172820.6
申请日：2008-12-23
申请人： SÜD-CHEMIE CATALYSTS ITALIA S.r.l.
发明人： Estenfelder, Marvin , Cremona, Alberto
IPC分类号： C01B21/26 , C01B21/28 , B01J8/00 , B01J8/04 , B01J19/24
CPC分类号： C01B21/265 , B01J19/2485 , B01J23/8986 , B01J35/04 , B01J37/0205 , B01J37/0207 , B01J37/0248 , C01B21/28 , Y10T428/24149
摘要： Ammonia oxidation catalyst units comprising a pair of honeycomb-type blocks having interplaced between them a layer performing the function of uniformly mixing the gas flow and an ammonia oxidation catalyst, the blocks having height of less than 15 cm.
摘要翻译：氨氧化催化剂单元包括一对蜂窝型块，它们之间插入一层，该层具有均匀混合气流的功能和氨氧化催化剂，其高度小于15cm。

53. 发明公开

EP2160236A1 VORRICHTUNG UND VERFAHREN FÜR KATALYTISCHE GASPHASENREAKTIONEN SOWIE DEREN VERWENDUNG 有权转让
标题翻译： DEVICE AND METHOD FOR气相反应催化氨及其用途
公开(公告)号：EP2160236A1
公开(公告)日：2010-03-10
申请号：EP08758816.6
申请日：2008-05-28
申请人： Uhde GmbH
发明人： SCHWEFER, Meinhard , GROVES, Michael , FUCHS, Jürgen , MAURER, Rainer , SIEFERT, Rolf , HÜNDGEN, Bernhard
IPC分类号： B01J8/00 , B01J8/02 , B01J15/00 , B01J19/00 , C01B21/26 , C01B21/28
CPC分类号： B01J8/008 , B01J8/02 , B01J8/025 , B01J8/0278 , B01J8/0285 , B01J15/005 , B01J19/002 , B01J2208/00176 , B01J2208/00203 , B01J2208/00212 , B01J2208/00495 , B01J2208/0053 , B01J2208/00716 , B01J2219/00006 , B01J2219/00263 , B01J2219/025 , C01B21/265 , C01B21/28
摘要： The invention relates to improved reactors for catalytic, exothermic gas phase reactions having an entry zone (1), a reaction zone (2) comprising at least one catalyst (4), and an exit zone (3) for the product gas, as viewed in the flow direction of a reactant gas. The reactors have means in the region of the entry zone (1), or the entry zone (1) and the reaction zone (2), such as insulating jackets (6) and/or devices for transporting coolant, reducing the transport of heat from the reaction zone (2) into the entry zone (1), and thus the risks of pre-ignition of the reactant gas mixture used or the triggering of undesired secondary reactions in the entry zone (1), and/or the interior walls of the reactor in the area of the entry zone (1), or in the area of the entry zone (1) and the reaction zone (2), being made of an inert material. The reactors can be used in particular for ammonia oxidation, such as in nitric acid production systems, in which preferably honeycomb-shaped transition metal catalysts having smaller cross sections than the typically used platinum meshes are used.

54. 发明公开

EP2121177A1 VERFAHREN UND EINRICHTUNG ZUR VERHINDERUNG DER KORROSION AN EINEM GASEINTRITTSSTUTZEN BEI EINER SALPETERSÄUREKONDENSATION 有权转让
标题翻译：方法和设备，用于硝酸防冷凝腐蚀对进气口配件
公开(公告)号：EP2121177A1
公开(公告)日：2009-11-25
申请号：EP07846701.6
申请日：2007-11-21
申请人： Uhde GmbH
发明人： MAURER, Rainer
IPC分类号： B01J19/26 , C01B21/28
CPC分类号： B01J19/26 , B01J4/001 , B01J4/002 , B01J2219/00119 , C01B21/28 , Y10S423/06 , Y10S423/08 , Y10T137/6525
摘要： According to the invention, the contact of condensing gas with the nozzle and the nozzle surroundings is to be minimized using a method and a device for preventing corrosion on and in the region of a gas inlet nozzle during nitric acid condensation. This is achieved in that the gas inlet nozzle has a sleeve on the inside in the transition region to the inside of the condenser, the sleeve forming a gas inlet opening in the shape of an annular gap, wherein the annular chamber is equipped with at least one feed opening for secondary air such that a peripheral flow of secondary air is formed around the incoming NO gas.

55. 发明公开

EP1483200A1 VERFAHREN ZUR HERSTELLUNG VON SALPETERSÄURE 有权
标题翻译：用于生产硝酸
公开(公告)号：EP1483200A1
公开(公告)日：2004-12-08
申请号：EP03714742.8
申请日：2003-02-15
申请人： Uhde GmbH
发明人： DZIOBEK, Frank , CLAES, Detlev , JOHANNING, Joachim , MAURER, Rainer , SZONN, Erich
IPC分类号： C01B21/40
CPC分类号： C01B21/26 , C01B21/28 , F01K23/064 , Y02P20/129
摘要： The invention relates to a method for the production of nitric acid having a concentration of between 50 and 76 %, from ammonia and gas containing oxygen, under pressure, according to a single pressure method or dual pressure method. The expansion of the residual gas takes place in at least two stages in a work efficient manner. At least one device for heating the previously expanded gas to a temperature of more than 450° is disposed between every other expansion stage, using waste heat from the production process of nitric acid.

56. 发明授权

EP1150765B1 CATALYST SUPPORT 有权
标题翻译：催化剂支持
公开(公告)号：EP1150765B1
公开(公告)日：2003-02-12
申请号：EP99959581.2
申请日：1999-12-10
申请人： Imperial Chemical Industries PLC
发明人： DAVIES, Raymond
IPC分类号： B01J8/02 , B01J8/00 , C01B21/26 , C01B21/28
CPC分类号： B01J8/008 , B01J8/025 , B01J2208/00141 , B01J2208/00884 , C01B21/28
摘要： A catalyst support structure e.g. for use in an ammonia oxidation reactor, comprising a series of primary supports (19) disposed above a catalyst bed, a lattice assembly disposed beneath the catalyst bed and on which the catalyst bed rests, said lattice assembly being suspended from the primary supports (19) by suspending means (27) extending through the catalyst bed. Preferably the support structure includes a static start-up burner arrangement in the form of one or more perforated tubes (24) adjacent the primary supports (19).
摘要翻译：催化剂载体结构例如用于氨氧化反应器中，所述反应器包括设置在催化剂床上方的一系列主要支撑体（19），设置在催化剂床下方并且催化剂床置于其上的网格组件，所述网格组件从主要支撑体（19 ）通过延伸穿过催化剂床的悬浮装置（27）。优选地，支撑结构包括邻近主支撑件（19）的一个或多个穿孔管（24）形式的静态启动燃烧器装置。

57. 发明公开

EP1189838A1 PROCESS FOR THE NONDESTRUCTIVE HEATING AND SUPPLY OF HOT AMMONIA OR HOT AMMONIA CONTAINING FEED GAS 有权
标题翻译：程序销毁免费加热和供应被加热氨水或加热AMMONIAKENTHÄLTENDEM用气
公开(公告)号：EP1189838A1
公开(公告)日：2002-03-27
申请号：EP00928666.7
申请日：2000-05-01
申请人： E.I. DU PONT DE NEMOURS AND COMPANY
发明人： GELBLUM, Peter Gideon , BARNES, John, J. , BLETSOS, Ioannis, V. , HERRON, Norman , KIM, Tae, Hoon
IPC分类号： C01B21/28 , C01C3/02 , B01J19/02
CPC分类号： C01C1/0452 , B01D53/79 , B01J19/02 , B01J2219/0236 , B01J2219/0277 , B01J2219/0286 , C01B21/28 , C01C1/02 , C01C3/0208 , C01C3/022 , Y02P20/52
摘要： A process for nondestructive heating and supplying of ammonia feed gas wherein high quality ammonia (typically greater than 90 % and as high as 99 %) is preserved at temperatures well in excess of the conventional limit of 230 °C (typically from 400 to 700 °C) by controlling the selection of metal surfaces in contact with the hot gas, the bulk temperature of the gas, the wall temperature, the pressure, the contact time, and the spatial surface density. Such hot gases are particularly useful for the manufacture of hydrogen cyanide.

58. 发明公开

EP1034134A1 AMMONIA OXIDATION CATALYSTS 审中-公开
标题翻译：氨氧化催化剂
公开(公告)号：EP1034134A1
公开(公告)日：2000-09-13
申请号：EP98952918.5
申请日：1998-11-06
申请人： IMPERIAL CHEMICAL INDUSTRIES PLC
发明人： CREWDSON, Bernard, John , WARD, Andrew, Mark , DUNNE, Michael, David
IPC分类号： C01B21/26 , C01B21/28 , B01J8/02 , B01J23/83
CPC分类号： B01J8/0242 , B01J8/008 , B01J8/0214 , B01J19/2495 , B01J35/02 , B01J2208/00884 , C01B21/265 , C01B21/28
摘要： An ammonia oxidation catalyst cartridge unit comprises a pair of retaining meshes spaced apart by less than 50 mm defining an enclosure filled with a random packed mass of particles of a composition comprising oxides of at least one metal selected from manganese, iron, nickel and cobalt, especially cobalt and at least one element A selected from rare earths and yttrium in such proportions that the element A to cobalt atomic ratio is in the range of 0.8 to 1.2. The catalyst particles have a minimum dimension of at least 0.5 mm and a maximum dimension of not more than 5 mm, and the spacing between the meshes is at least 4 times, but not more than 50 times, the maximum dimension of the particles. The unit may extend across the ammonia oxidation reactor cross section or a catalyst cartridge may comprise a grid or apertured plate, extending across the cross section of the reactor, with a unit as aforesaid in each aperture.
摘要翻译：一种氨氧化催化剂盒单元包括间隔小于50mm的一对保持网，从而限定了填充有随机填充的颗粒的外壳，所述颗粒包含选自锰，铁，镍和钴中的至少一种金属的氧化物，尤其是钴和至少一种选自稀土和钇的元素A，其比例使得元素A与钴的原子比在0.8至1.2的范围内。催化剂颗粒具有至少0.5mm的最小尺寸和不大于5mm的最大尺寸，并且网眼之间的间距为颗粒的最大尺寸的至少4倍但不超过50倍。该单元可横跨氨氧化反应器横截面延伸，或者催化剂筒可包括横跨反应器的横截面延伸的格栅或多孔板，其中在每个孔中具有前述的单元。

59. 发明公开

EP0641737A1 Packed bed arrangement useful for mixing and/or oxidation 失效
标题翻译： Zusammenstellung einesSchützguttbetteszur Anwendung bei Misch- und Oxidationsverfahren。
公开(公告)号：EP0641737A1
公开(公告)日：1995-03-08
申请号：EP93116997.3
申请日：1993-10-20
申请人： PRAXAIR TECHNOLOGY, INC.
发明人： Drnevich, Raymond Francis , Dreisinger, Douglas Ronald
IPC分类号： C01B21/28 , C01C3/02 , C01B15/029 , C07C253/24 , B01J19/00 , C07C57/04 , B01F3/02
CPC分类号： B01J12/005 , B01J8/008 , B01J8/0453 , B01J19/002 , B01J2219/00263 , C01B21/28 , Y02P20/129
摘要： The present invention relates to processes and apparatus for mixing oxidizable reactants with oxidant and/or oxidizing oxidizable reactants. Through using particular mixing and/or oxidizing arrangements, the risk of flammable or explosive reactions can be significantly reduced or prevented. When ammonia is used as the reactant, nitric acid can be obtained.
摘要翻译：一种或多种反应物（I）通过将它们与填充床中的氧化剂（II）混合而被氧化。惰性包装材料（III）; 然后在氧化条件下进行反应。（I）特别是MeOH，PhH，萘，O-二甲苯，异丙基苯，CH 4，丙烯，丙烯醛，H 2或NH 3。（III）是（a）最大的球形颗粒。直径。尺寸在公式 1; DP = 0.61Dt（VSD / VLB） - 0.727Dt（1）或（b）最大的非球形颗粒。大小由公式定义 DP = 6（VP / SP）（2）。 DP =直径的球形（III）（英寸）; VSD =设计入口条件下的表观速度（ft / sec）; VLB =混合物的层流燃烧速度。（英尺/秒）; Dt = dia 包装管（英寸）; VP = vol。的非球形（III）; SP =非球形（III）（inch2）的表面积。首选（I）是NH 3，加入至少15％在（二）中。（二）有O2浓至少25％。县。在反应过程中，将包含H 2 O的缓和材料加入到填充床中以保持温度。低于自燃温度（特别是0.5-0.9吨/吨NH3）。县。（III）是不可燃和选择。吸热，尤其是陶瓷，砂砾，沙子，玻璃珠，石灰石或混合物。用NH3，mixt。然后是pref。当通过下游废热锅炉系统从氧化物质中除去或回收产生的热量时，通入氧化催化剂的填充床。氧化物质（即N氧化物）是优选的。在H 2 O存在下浓缩，得到HNO 3。

60. 发明公开

EP0044973A1 Vorrichtung zur Verteilung eines aus einem Rohr ankommenden Gases auf den Querschnitt eines Behälters 失效
标题翻译：用于从管分配进入气体到容器的横截面。
公开(公告)号：EP0044973A1
公开(公告)日：1982-02-03
申请号：EP81105206.7
申请日：1981-07-04
申请人： BASF Aktiengesellschaft
发明人： Coulon, Guenter, Dr. Phys. , Leuckel, Wolfgang, Dr. Ing.
IPC分类号： B01J4/00 , C01B21/26 , F15D1/04
CPC分类号： F15D1/08 , B01J8/0278 , B01J2208/00849 , C01B21/28
摘要： Vorrichtung zur Verteilung eines aus einem Rohr ankommenden Gases auf den Querschnitt eines Behälters, dessen Durchmesser ein Vielfaches des Rohrdurchmessers beträgt, insbesondere zur Verteilung des Ammoniak/Luft-Gemisches bei der katalytischen Ammoniakoxidation, wobei das Eintrittsrohr (1) mit einem konzentrisch angeordneten Innenrohr ausgestattet (3) ist und im Kreisring zwischen Eintrittsrohr und Innenrohr Einbauten (4) zur Erzeugung eines Dralles angeordnet sind.
摘要翻译：装置，用于在其直径的容器的横截面从管气体分配呼入是管道直径的倍数，尤其是在氨的催化氧化中的氨/空气混合物的分布，其中所述入口管（1）配备有一个同心设置的内管（3）和在所述入口管和内管的内部（4）之间的环形空间被安排成产生涡流。

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