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51. 发明公开

EP0296396A2 Mesophase pitch-based carbon fibres 失效
标题翻译： Auf Mesaphasenpech basierende Kohlenstoffasern。
公开(公告)号：EP0296396A2
公开(公告)日：1988-12-28
申请号：EP88108892.6
申请日：1988-06-03
申请人： PETOCA LTD.
发明人： Suto, Yoshinori Kashima Seiyusho of , Ito, Toshiyuki Kashima Seiyusho of , Nakajima, Hideyuki Kashima Seiyusho of , Okamura, Keiichiro Kashima Seiyusho of , Nayuki, Shin-ichi Kashima Seiyusho of , Ogawa, Hiroyasu Kashima Seiyusho of , Enomoto, Harumitsu Kashima Seiyusho of
IPC分类号： D01F9/145
CPC分类号： D01F9/15 , D01F9/155
摘要： A method for producing mesophase pitch based carbon fibers which enables to produce high strength high modulus carbon fibers at a relatively low temperature with stabilized production manner. This method comprises carbonizing infusiblized fibers, in an inert atmosphere under no tension state or a tension of 1 mg/denier or less in the first stage to give a specified interlayer spacing and a crystallite thickness and then carbonizing under a tension of 50 - 300 mg/denier at a temperature of 2600°C or more in the second stage.
摘要翻译：一种生产中间相沥青基碳纤维的方法，其能够以稳定的生产方式在相对低的温度下生产高强度高模量碳纤维。该方法包括在无张力状态的惰性气氛中或在第一阶段中1mg /旦尼尔或更小的张力下碳化不熔化的纤维，得到规定的层间距和微晶厚度，然后在50-300mg的张力下碳化 /旦在第二阶段的2600℃以上的温度。

52. 发明公开

EP0280233A1 Method for producing carbon-carbon composite materials 失效
标题翻译： Verfahren zur Herstellung von Kohlenstoff-Kohlenstoff-Verbundmaterialien。
公开(公告)号：EP0280233A1
公开(公告)日：1988-08-31
申请号：EP88102568.8
申请日：1988-02-22
申请人： PETOCA LTD.
发明人： Takabatake, Minoru Kashima Seiyusho
IPC分类号： C04B35/52 , D01F11/10 , D01F9/14
CPC分类号： C04B35/83 , D01F11/10
摘要： A method for producing high density, high strength carbon-carbon composite material, is provided by using

(i) pitch-based infusible fibers,
(ii) pitch-based carbon fibers having been carbonized at a temperature lower than 2200°C or
(iii) structures, containing as a principal constituent, said fibers (i) or (ii) as a reinforcement material,
impregnating said reinforcement material with a liquid carbonaceous material such as pitch or the like and then carbonizing said impregnated material and if necessary graphitizing said carbonized product.
摘要翻译：通过使用（i）基于沥青的可熔纤维，（ii）在低于2200℃的碳化处理的沥青类碳纤维或（iii）的高分子量的碳 - 碳复合材料的制造方法，）作为主要成分的所述纤维（i）或（ii）作为增强材料，用液体碳质材料如沥青等浸渍所述增强材料，然后碳化所述浸渍的材料，并且如果需要，石墨化所述碳化的产品。

53. 发明公开

EP1033423A1 METHOD FOR PRODUCING MESOPHASE PITCH ACTIVE CARBON FIBER, MESOPHASE PITCH ACTIVE CARBON FIBER, ELECTRIC DOUBLE-LAYER CAPACITOR 有权
标题翻译：用于生产中间相沥青基活性炭纤维，中间相沥青基活性炭纤维，双电层电容器
公开(公告)号：EP1033423A1
公开(公告)日：2000-09-06
申请号：EP99943442.6
申请日：1999-09-21
申请人： PETOCA, Ltd
发明人： MAEDA, Takashi, Petoca, Ltd. , KAWABUCHI, Yuji , HAGA, Takahiro , HOSOTSUBO, Tomiji
IPC分类号： D01F9/14
CPC分类号： D01F9/145 , H01G11/34 , Y02E60/13
摘要： A process for producing a mesophase pitch based active carbon fiber, comprising the steps of carbonizing a mesophase pitch based infusibilized fiber at 600 to 900°C, activating the thus obtained carbon fiber with alkali, and immersing the thus obtained mesophase pitch based active carbon fiber in an electrolyte and subjecting the immersed mesophase pitch based active carbon fiber to such a charge and discharge treatment that a voltage, gradually increased until exceeding 2.5 V is applied at a constant current density to the mesophase pitch based active carbon fiber so that an electric double layer is formed at an interface of the mesophase pitch based active carbon fiber and the electrolyte to thereby effect a charging and thereafter a discharging is effected at a constant current density. There are further provided an active carbon fiber produced by the above process and an electric double layer capacitor including an electrode comprising this active carbon fiber.
摘要翻译：一种生产中间相沥青基活性炭纤维，包括碳化的中间相沥青的步骤过程基于在600熔化纤维至900℃，激活与碱将这样得到的碳纤维，并始终唱如此获得的中间相沥青基活性炭纤维在电解质和使所浸入的中间相沥青基活性炭纤维寻求一个充电和放电处理没有电压时，逐渐增加，直到超过2.5 V在基于活性的碳纤维作为双电做的恒定电流密度的中间相沥青中的应用层在形成于中间相沥青基活性炭纤维与电解质的界面，从而实现充放电之后是一个实现以恒定的电流密度。这里还提供了对用上述方法和包含这个活性炭纤维包括双电层电容器电极产生的活性的碳纤维。

54. 发明公开

EP1011161A2 Graphite Materials for negative electrode used in lithium secondary battery 有权
标题翻译： Graphite-MaterialenfürNegativelektrode eines锂 - Akkumulators
公开(公告)号：EP1011161A2
公开(公告)日：2000-06-21
申请号：EP99123067.3
申请日：1999-11-20
申请人： PETOCA Ltd.
发明人： Tamaki, Toshio, c/o Petoca Ltd. , Ishigami, Kazunori, c/o Petoca Ltd.
IPC分类号： H01M4/58 , C01B31/04
CPC分类号： H01M4/587 , H01M4/362 , H01M2004/021
摘要： There are disclosed graphite materials for a negative electrode used in a lithium secondary battery which graphite materials have an average specific surface area of 1.5 m 2 /gram to 5 m 2 /gram and comprise (A) milled graphite fibers which are produced by milling and graphitizing mesophase pitch-based carbon fibers, and which have an interplanar spacing of the graphite layer (d 002 ) of at most 0.337nm and a specific surface area of 0.8m 2 /gram to 1.3m 2 /gram; and (B) graphite materials which have an interplanar spacing of the graphite layer (d 002 ) of at most 0.336nm, a degree of graphitization (P 101 /P 100 ) of at least 2.0 and a specific surface area of 2m 2 /gram to 15m 2 /gram, wherein the components (A) and (B) are mixed at a ratio (A)/(B) by weight of 90/10 to 50/50. The above graphite materials comprising the components (A) and (B), when used for a negative electrode in a lithium secondary battery, can enhance the performance of the battery and charge/discharge capacity thereof especially in a high load discharge.
摘要翻译：公开了用于锂二次电池的负极用石墨材料，其中石墨材料的平均比表面积为1.5m 2 / g〜5m 2 / g，并且包含（A）研磨的石墨纤维，通过研磨和石墨化中间相沥青基碳纤维制成，并且石墨层（d002）的面间距至多为0.337nm，比表面积为0.8m 2 / g至1.3m 2 / 公克; 和（B）具有至多0.336nm的石墨层的面间距（d002），石墨化度（P101 / P100）为2.0以上，比表面积为2m 2 / g的石墨材料， 15m 2 / g，其中组分（A）和（B）以90/10至50/50的重量比（A）/（B））混合。包含组分（A）和（B）的上述石墨材料当用于锂二次电池中的负极时，可以提高电池的性能和充电/放电容量，特别是在高负载放电中。

55. 发明授权

EP0701011B1 "NITROGEN-CONTAINING ISOTROPIC PITCH AND PROCESS FOR ITS PREPARATION" 失效
标题翻译： “含氮MAKING OF各向同性沥青与方法”
公开(公告)号：EP0701011B1
公开(公告)日：1999-12-01
申请号：EP95114130.8
申请日：1995-09-08
申请人： PETOCA, Ltd
发明人： Maeda, Takashi, c/o Petoca Ltd, , Hosotsubo, Tomiji, c/o Petoca Ltd,
IPC分类号： C10C3/02 , D01F9/155 , C04B35/83
CPC分类号： C10C3/023 , D01F9/155

56. 发明授权

EP0644603B1 Negative electrode for use in a secondary battery 失效
标题翻译：用于负极的二次电池
公开(公告)号：EP0644603B1
公开(公告)日：1999-03-17
申请号：EP94114559.1
申请日：1994-09-15
申请人： Kabushiki Kaisha Toshiba , PETOCA, Ltd
发明人： Ohsaki, Takahisa , Takami, Norio , Nishimura, Yoshiyuki , Tamaki, Toshio
IPC分类号： H01M4/58 , H01M10/40
CPC分类号： H01M10/05 , H01M4/0404 , H01M4/0459 , H01M4/382 , H01M4/405 , H01M4/583 , H01M4/587 , H01M4/622 , H01M4/661 , H01M2004/027 , H01M2300/0025

57. 发明授权

EP0644280B1 Milled carbon fiber and process for producing the same 失效
标题翻译：磨碎碳纤维和它们的制备方法
公开(公告)号：EP0644280B1
公开(公告)日：1998-12-23
申请号：EP94114568.2
申请日：1994-09-15
申请人： PETOCA, Ltd
发明人： Nishimura, Yoshiyuki, c/o Petoca, Ltd. , Ejiri, Hiroshi, c/o Petoca, Ltd.
IPC分类号： D01F9/145 , D01F9/32
CPC分类号： D01F9/322 , D01F9/145 , Y10T428/2918

58. 发明公开

EP0792958A2 Activated carbon fiber molding and process for producing the same 失效
标题翻译：活性炭纤维的模塑材料和制备方法
公开(公告)号：EP0792958A2
公开(公告)日：1997-09-03
申请号：EP97103350.1
申请日：1997-02-28
申请人： PETOCA LTD.
发明人： Hosotsubo, Tomiji , Kawamura, Toshifumi , Miura, Kouichi , Nakagawa, Hiroyuki
IPC分类号： D01F9/145 , C04B35/83
CPC分类号： C04B35/62272 , D01F9/145
摘要： A process for producing an activated carbon fiber molding is disclosed which comprises spinning an isotropic pitch to thereby obtain pitch fibers, infusibilizing the pitch fibers to thereby obtain infusibilized fibers, heating the infusibilized fibers under a mechanical load to thereby obtain a molding and activating the molding. In this process, the infusibilized fibers and/or infusibilized fibers molding may be heated in an inert atmosphere so as to effect a light carbonization thereof and thereafter subjected to the subsequent step of the process. The pitch-based porous activated carbon fiber molding obtained by this process has a strikingly high bulk density and can sufficiently exhibit the specific properties of the activated carbon fiber, e.g. a large specific surface area, to thereby have a high adsorption efficiency.
摘要翻译：一种用于在活性碳纤维成型制造方法是圆盘游离缺失，其包括旋涂各向同性沥青从而获得沥青纤维;难熔化处理沥青纤维，从而得到难熔化的纤维，机械负载条件下加热该难熔化处理的纤维，从而得到模制和激活所述成型，在此过程中，不熔化纤维和/或难熔纤维成型可以以惰性气氛中，在这样进行加热以影响一个轻碳化物，然后进行该过程的后续步骤。通过这种方法得到的沥青系多孔活性碳纤维成型体具有显着高的堆积密度，并且可以充分发挥活性碳纤维的具体性质，例如大的比表面积，从而具有高的吸附效率。

59. 发明授权

EP0604768B1 Carbon fiber rovings for reinforcement of concrete 失效
标题翻译：为混凝土的增强碳纤维
公开(公告)号：EP0604768B1
公开(公告)日：1997-06-11
申请号：EP93119109.2
申请日：1993-11-26
申请人： PETOCA Ltd. , TAKENAKA CORPORATION
发明人： Nagata, Yoshikazu, c/o Petoca, Ltd. , Takano, Katsumi, c/o Petoca, Ltd. , Ohno, Sadatoshi, c/o Takenaka Corp. Plannners , Yonezawa, Toshio, c/o Takenaka Corp. Plannners , Ida, Junichi Hirabari-Jutaku 4-306 , Iwata, Masaki
IPC分类号： C04B20/10 , D01F11/14
CPC分类号： C04B14/386 , C04B20/1037 , C04B2111/00155 , C04B2201/50 , D01F11/14 , Y10T428/2913 , Y10T428/292 , Y10T428/2938 , Y10T428/30 , C04B20/1022 , C04B20/1025

60. 发明公开

EP0707098A3 Process for preparing milled graphite fibers 失效
标题翻译：磨碎的石墨纤维的制备方法
公开(公告)号：EP0707098A3
公开(公告)日：1996-05-01
申请号：EP95115326.1
申请日：1995-09-28
申请人： PETOCA Ltd.
发明人： Tamaki, Toshio, c/o Petoca Ltd. , Tamaki, Minoru, c/o Petoca Ltd. , Katsuta, Yasushi, c/o Petoca Ltd.
IPC分类号： D01F9/145
CPC分类号： D01F9/145
摘要： Disclosed is a process for preparing milled graphite fibers in which the amount of metallic components contained in the milled carbon fibers before graphitizing is limited to not more than 100/1 000 000 in terms of weight ratio. Also disclosed is a process for preparing milled graphite fibers in which the amount of metallic components contained in the milled carbon fibers before graphitizing except metallic components originally contained in the fibers themselves is limited to not more than 50/1 000 000 in terms of weight ratio. According to these processes, there can be obtained milled graphite fibers whose surfaces are inert, which suffer few longitudinal crackings and which are almost free from occurrence of particulate substances comprising agglomerated or bonded fibers.
摘要翻译：公开了一种制备磨碎石墨纤维的方法，其中石墨化之前磨碎的碳纤维中所含金属成分的量按重量比限制在不超过100/1000000。还公开了一种制备磨碎的石墨纤维的方法，其中，除了初始包含在纤维中的金属成分本身之外，石墨化之前磨碎的碳纤维中所含的金属成分的量按重量比限制在不超过50/1000000 。根据这些方法，可以获得表面惰性的磨碎石墨纤维，其纵向裂纹很少，几乎不会发生包含附聚或粘合纤维的颗粒状物质。

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