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51. 发明公开

EP3357900A1 1,3,3,3-TETRAFLURORPROPENE PROCESS AZEOTROPES WITH HF 审中-公开
公开(公告)号：EP3357900A1
公开(公告)日：2018-08-08
申请号：EP17204184.0
申请日：2011-08-25
申请人： Honeywell International Inc.
发明人： HULSE, Ryan , PHAM, Hang T. , SINGH, Rajiv Ratna , MERKEL, Daniel C. , POKROVSKI, Konstantin A. , TUNG, Hsueh Sung
IPC分类号： C07C21/18 , C07C17/25 , C07C17/38 , C01B7/19
CPC分类号： C07C21/18 , C01B7/191 , C07C17/38 , C07C19/08
摘要： The present invention pertains to azeotropic and azeotrope-like compositions of the following three blends:
1. Trans-1,3,3,3-tetrafluoropropene (HFO-1234ze(E)), cis-1,3,3,3-tetrafluoropropene (HFO-1234ze(Z)) and hydrogen fluoride (HF);
2. HFO-1234ze(E), 1,1,1,3,3-pentafluoropropane (HFC-245fa) and HF; and
3. HFO-1234ze(Z), HFC-245fa and HF.
These azeotropic and azeotrope-like compositions are useful as intermediates in the production of HFO-1234ze(E).

52. 发明公开

EP3352740A1 LIQUID NICOTINE FORMULATION 审中-公开
公开(公告)号：EP3352740A1
公开(公告)日：2018-08-01
申请号：EP16778094.9
申请日：2016-09-22
申请人： TTP PLC
发明人： HOPPE, Hans-Jürgen , MCDERMENT, Iain
IPC分类号： A61K9/72 , A61K9/00 , A61K31/465
CPC分类号： A61K31/465 , A61K9/007 , A61K9/0078 , A61K9/12 , A61K47/10 , A61M15/009
摘要： There is disclosed a liquid formulation for inhalation into the lungs, comprising an aqueous solution of nicotine or a nicotine analogous molecule, at least one organic and/or inorganic salt, an organic liquid having a viscosity higher than water, and optionally an organic alcohol, wherein the pH of the formulation is greater than pH 7 and the formulation does not include a propellant. There is further disclosed a corresponding method of aerosolising the liquid formulation, a method for delivering nicotine to the user, and an aerosol-generating device.

53. 发明公开

EP3269698A1 PROCESS FOR THE MANUFACTURE OF FLUORINATED OLEFINS 有权
标题翻译：制造氟化烯烃的方法
公开(公告)号：EP3269698A1
公开(公告)日：2018-01-17
申请号：EP17170975.1
申请日：2011-06-22
申请人： Honeywell International Inc.
发明人： WANG, Haiyou , TUNG, Hsueh Sung
IPC分类号： C07C17/357 , C07C21/18 , C07C17/354 , C07C19/08
CPC分类号： C07C17/04 , C07C17/354 , C07C17/357 , C07C21/18 , C07C19/08
摘要： Provided are methods for producing fluorinated organic compounds, which preferably comprises converting at least one compound of formula (I) CH 2 XCHZCF 3 to at least one compound of formula (II) CHX=CZCF 3 where X and Z are independently H or F, with the proviso that X and Z are not the same. The converting step comprises catalytically reacting at least one compound of formula (I), preferably via dehydrogenation or oxidative dehydrogenation. In another aspect, the inventive method of preparing fluorinated organic compounds comprises converting a reaction stream comprising at least one pentafluoropropene to a product stream comprising at least one pentafluoropropane and at least one compound of formula (I), separating out the compound of formula (I) from the product stream, and converting the compound of formula (I) separated from the product stream to at least one compound of formula (II), wherein the conversion the compound of formula (I) to 3,3,3-trifluoropropene is substantially limited.
摘要翻译：提供了用于生产氟化有机化合物的方法，其优选包括将至少一种式（I）CH 2 XCHZCF 3化合物转化为至少一种式（II）化合物CHX = CZCF 3，其中X和Z独立地为H或F，条件是 X和Z不一样。转化步骤包括催化反应至少一种式（I）化合物，优选通过脱氢或氧化脱氢。另一方面，制备氟化有机化合物的本发明方法包括将包含至少一种五氟丙烯的反应物流转化为包含至少一种五氟丙烷和至少一种式（I）化合物的产物物流，从而分离出式（I）化合物）从产物流中分离出来，并将从产物流分离的式（I）化合物转化为至少一种式（II）化合物，其中式（I）化合物转化为3,3,3-三氟丙烯的转化率为充分受限。

54. 发明公开

EP3263543A1 INTEGRATED PROCESS FOR THE MANUFACTURE OF FLUORINATED OLEFINS 审中-实审
标题翻译：氟化烯烃制造的综合方法
公开(公告)号：EP3263543A1
公开(公告)日：2018-01-03
申请号：EP17180528.6
申请日：2011-10-07
申请人： Honeywell International Inc.
发明人： BEKTESEVIC, Selma , TUNG, Hsueh Sung , KOPKALLI, Haluk
IPC分类号： C07C17/23 , C07C21/18 , C07C19/08 , C07C17/38
CPC分类号： C07C17/25 , C07C17/354 , C07C17/38 , Y02P20/125 , Y02P20/582 , C07C21/18 , C07C19/08
摘要： The instant invention relates, at least in part, to a method increasing the cost efficiency for dehydrohalogenation production of a fluorinated olefin by recovering and recycling spent dehydrohalogenation agent. In one aspect, the present invention relates to dehydrohalogenating a fluorinated alkane (e.g. pentafluoropropane and/or hexafluoropropane) in the presence of a dehydrohalogenating agent to produce a fluorinated olefin (e.g. tetrafluoropropenes and/or pentafluoropropenes). Removal of spent dehydrohalogenating agent from the reactor allows for facile separation of organic and dehydrohalogenating agent, the latter of which is recycled.
摘要翻译：本发明至少部分涉及通过回收和再循环用过的脱卤化氢剂来提高氟化烯烃的脱卤化氢生产的成本效率的方法。一方面，本发明涉及在脱卤化氢剂存在下使氟化烷烃（例如五氟丙烷和/或六氟丙烷）脱卤化氢以产生氟化烯烃（例如四氟丙烯和/或五氟丙烯）。从反应器中除去用过的脱卤化氢剂可以使有机和脱卤化氢剂容易分离，后者可循环使用。

55. 发明公开

EP3239122A1 A PROCESS FOR DEHYDROCHLORINATING 1,1,1,2-TETRAFLUORO-2-CHLOROPROPANE TO 2,3,3,3-TETRAFLUOROPROPENE IN THE PRESENCE OF AN ALKALI METAL-DOPED MAGNESIUM OXYFLUORIDE CATALYST AND METHODS FOR MAKING THE CATALYST 审中-公开
标题翻译：在碱金属掺杂的氟氧化镁催化剂存在下将1,1,1,2-四氟-2-氯丙烷脱氢氯代为2,3,3,3-四氟丙烯的方法和制备催化剂的方法
公开(公告)号：EP3239122A1
公开(公告)日：2017-11-01
申请号：EP17176693.4
申请日：2009-05-28
申请人： Honeywell International Inc.
发明人： WANG, Haiyou , TUNG, Hsueh Sung
IPC分类号： C07C17/23 , C07C21/18 , B01J27/138 , B01J23/04 , C07C17/25 , B01J37/02 , B01J27/128 , B01J37/00
CPC分类号： B01J27/128 , B01J27/138 , B01J37/0009 , B01J37/0036 , B01J37/0236 , C07C17/25 , C07C21/18
摘要： A process for making a fluorinated olefin. The process has the step of dehydrochlorinating a hydrochlorofluorocarbon having at least one hydrogen atom and at least one chlorine atom on adjacent carbon atoms in the presence of a catalytically effective amount of a catalyst composition. The catalyst composition is represented by the following: n wt.% MX/M'O y F z , wherein 0 + , Na + , K + , Rb + , and Cs + ; X is a halogen ion selected from the group consisting of F - , Cl - , Br - , and I - , M' is a bivalent metal ion; wherein n is a weight percentage of about 0.05% to about 50% MX based on the total weight of the MX and M'O y F z , and wherein y and z are the mole fractions of oxygen and fluorine in M'O y F z , respectively. There are also methods for making catalyst compositions.
摘要翻译：一种制备氟化烯烃的方法。该方法具有在催化有效量的催化剂组合物存在下使在相邻碳原子上具有至少一个氢原子和至少一个氯原子的氢氯氟烃脱氯化氢的步骤。所述催化剂组合物由以下表示：其中0

56. 发明公开

EP3207013A1 METHOD FOR SEPARATING HF FROM HF/HALOGENATED HYDROCARBON MIXTURES USING IONIC LIQUIDS 审中-公开
标题翻译：使用离子液体分离HF /卤代烃混合物中HF的方法
公开(公告)号：EP3207013A1
公开(公告)日：2017-08-23
申请号：EP15850637.8
申请日：2015-10-15
申请人： Honeywell International Inc.
发明人： WANG, Haiyou , TUNG, Hsueh Sung
IPC分类号： C07C17/25 , C07C17/093 , C07C17/10 , C07C19/08
CPC分类号： C01B7/195
摘要： The present invention relates to an ionic liquid comprised of a salt, the anion of which is Cl−, F−, and (HF)nF−(n=1.0−4.0), or combination thereof. In another embodiment, the present invention relates to a process of separating HF from a first mixture comprised of at least one halogenated hydrocarbon and HF which comprises contacting the mixture with an ionic liquid comprised of a salt, the anion of which is Cl−, F−, and (HF)nF− where n is a positive number ranging from 1 to 4, inclusive 4.0), to form a second mixture comprised of HF, halogenated hydrocarbon and said ionic liquid, extracting a solution comprising HF therefrom, and recovering HF therefrom.
摘要翻译：本发明涉及由阴离子为Cl-，F-和（HF）nF-（n = 1.0-4.0）的盐或其组合组成的离子液体。在另一个实施方案中，本发明涉及从包含至少一种卤代烃和HF的第一混合物中分离HF的方法，该方法包括使该混合物与由盐组成的离子液体接触，所述盐的阴离子为Cl - ，F - 和（HF）nF-，其中n是1-4的正数，包括4.0），以形成由HF，卤代烃和所述离子液体组成的第二混合物，从其中提取包含HF的溶液，并回收HF 由此。

57. 发明公开

EP3176147A1 PROCESS FOR THE PRODUCTON OF HFO TRANS-1234ZE FROM HFC-245FA 有权
标题翻译：从HFC-245FA生产HFO TRANS-1234ZE的方法
公开(公告)号：EP3176147A1
公开(公告)日：2017-06-07
申请号：EP17152564.5
申请日：2007-08-24
申请人： Honeywell International Inc.
发明人： WANG, Haiyou , TUNG, Hsueh Sung
IPC分类号： C07C17/25 , C07C17/38 , C07C21/18
CPC分类号： C07C17/087 , C07C17/25 , C07C17/38 , C07C17/383 , C07C19/08 , C07C21/18
摘要： A process for the production of trans-1,3,3,3-tetrafluoropropene which comprises:
(a) dehydrofluorinating 1,1,1,3,3-pentafluoropropane to thereby produce a result comprising cis-1,3,3,3-tetrafluoropropene, trans-1,3,3,3-tetrafluoropropene and hydrogen fluoride;
(b) optionally recovering hydrogen fluoride from the result of step (a); and
(c) recovering trans- 1,3,3,3-tetrafluoropropene.
摘要翻译：一种生产反式-1,3,3,3-四氟丙烯的方法，该方法包括：（a）将1,1,1,3,3-五氟丙烷脱氟化氢，从而得到包含顺式-1,3,3,3 - 四氟丙烯，反式-1,3,3,3-四氟丙烯和氟化氢; （b）任选地从步骤（a）的结果回收氟化氢; 和（c）回收反式-1,3,3,3-四氟丙烯。

58. 发明公开

EP3173397A1 METHOD FOR PRODUCING FLUORINATED ORGANIC COMPOUNDS 审中-公开
标题翻译：生产氟化有机化合物的方法
公开(公告)号：EP3173397A1
公开(公告)日：2017-05-31
申请号：EP16188659.3
申请日：2008-08-04
申请人： Honeywell International Inc.
发明人： JOHNSON, Robert C. , TUNG, Hsueh Sung , MERKEL, Daniel C.
IPC分类号： C07C17/20 , C07C17/21 , C07C19/10
CPC分类号： C07C17/25 , C07C17/04 , C07C17/087 , C07C17/204 , C07C17/206 , C07C17/21 , C07C17/23 , C07C21/18 , C07C19/01 , C07C19/10 , C07C19/08 , C07C21/073
摘要： Disclosed are processes for the production of fluorinated olefins, preferably adapted to commercialization of CF 3 CF=CH 2 (1234yf). In certain preferred embodiments the processes comprise first exposing a compound of Formula (IA) C(X) 2 =CClC(X) 3 (IA) where each X is independently F, Cl or H, preferably CCl 2 =CClCH 2 Cl, to one or more sets of reaction conditions, but preferably a substantially single set of reaction conditions, effective to produce at least one chlorofluoropropane, preferably in accordance with Formula (IB): CF 3 CClX'C(X') 3 Formula (IB) where each X' is independently F, C1 or H, and then exposing the compound of Formula (IB) to one or more sets of reaction conditions, but preferably a substantially single set of reaction conditions, effective to produce a compound of Formula (II) CF 3 CF=CHZ (II) where Z is H, F, C1, I or Br.
摘要翻译：公开了生产氟化烯烃的方法，优选适用于CF 3 CF = CH 2（1234yf）的商业化。在某些优选的实施方案中，所述方法包括首先将其中每个X独立地为F，Cl或H，优选CCl 2 = CClCH 2 Cl的式（IA）C（X）2 = CClC（X）3（IA）（IB）化合物有效产生至少一种氯氟丙烷的反应条件组，但优选基本上单组的反应条件，其中每个X'独立地为（CF 2 CClX'C（X'）3） F，C 1或H，然后将式（IB）化合物暴露于一组或多组反应条件，但优选基本上单组反应条件，有效地制备式（II）化合物CF 3 CF = CHZ（II ）其中Z是H，F，C1，I或Br。

59. 发明公开

EP3138831A1 SYNTHESIS OF TETRACYCLINES AND ANALOGUES THEREOF 有权
标题翻译： ANALOGA DARAUS的TETRACYCLINSYNTHESE
公开(公告)号：EP3138831A1
公开(公告)日：2017-03-08
申请号：EP16180780.5
申请日：2005-05-20
申请人： President and Fellows of Harvard College
发明人： MYERS, Andrew G. , CHAREST, Mark G. , LERNER, Christian D. , BRUBACKER, Jason D. , SIEGEL, Dionicio R.
IPC分类号： C07C233/26 , A61K31/65 , A61P31/04
摘要： The tetracycline class of antibiotics has played a major role in the treatment of infectious diseases for the past 50 years. However, the increased use of the tetracyclines in human and veterinary medicine has led to resistance among many organisms previously susceptible to tetracycline antibiotics. The modular synthesis of tetracyclines and tetracycline analogs described provides an efficient and enantioselective route to a variety of tetracycline analogs and polycyclines previously inaccessible via earlier tetracycline syntheses and semi-synthetic methods. These analogs may be used as anti-microbial agents or anti-proliferative agents in the treatment of diseases of humans or other animals.
摘要翻译：四环素类抗生素在过去50年的传染病治疗中发挥了重要作用。然而，四环素在人和兽医学中的增加使用导致许多以前易受四环素抗生素敏感的生物体之间的抵抗。所描述的四环素和四环素类似物的模块合成为通过先前的四环素合成和半合成方法先前不能接近的各种四环素类似物和聚环状体提供了有效和对映选择性的途径。这些类似物可以用作抗微生物剂或抗增殖剂来治疗人类或其他动物的疾病。

60. 发明公开

EP3112024A1 PROCESS FOR MAKING FLUORINATED OLEFINS 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLOW FLUORIERTER OLEFINE
公开(公告)号：EP3112024A1
公开(公告)日：2017-01-04
申请号：EP16184365.1
申请日：2008-12-05
申请人： Honeywell International Inc.
发明人： WANG, Haiyou , TUNG, Hsueh Sung
IPC分类号： B01J27/08 , B01J27/128 , B01J35/00 , B01J37/02 , B01J37/04 , C07C17/25 , C07C21/18
CPC分类号： B01J27/138 , B01J27/08 , B01J27/128 , B01J35/0006 , B01J37/0236 , B01J37/04 , C07C17/25 , C07C21/18
摘要： A process for making a fluorinated olefin, comprising dehydrochlorinating a hydrochlorofluorocarbon having at least one hydrogen and at least one chlorine on adjacent carbons in the presence of a catalytically effective amount of a catalyst composition represented by the following:

MX/M'F 2

wherein MX is an alkali metal halide;
M is an alkali metal ion selected from the group consisting of Li + , Na + , K + , Rb + , and Cs + ;
X is a halogen ion selected from the group consisting of F - , Cl - , Br - , and I - ; M'F 2 is a bivalent metal fluoride; and
M' is a bivalent metal ion.
摘要翻译：一种制备氟化烯烃的方法，包括在催化有效量的催化剂组合物存在下，将相邻碳上具有至少一个氢和至少一个氯的氢氯氟烃脱氯化氢：€ƒ€ƒ€ƒ €ƒ€ƒ€ƒMX / M'F 2其中MX是碱金属卤化物; M是选自Li +，Na +，K +，Rb +和Cs +的碱金属离子; X是选自F - ，Cl - ，Br - 和I - 的卤素离子; M'F 2是二价金属氟化物; M'是二价金属离子。

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