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31. 发明公开

EP2897903A1 PROCESS FOR PREPARING CRYSTALLINE AMMONIUM SULFATE PRODUCT 有权转让
标题翻译： VERFAHREN UND VORRICHTUNG ZUR HERSTELLUNG EINES KRISTALLINEN AMMONIUMSULFATPRODUKTES
公开(公告)号：EP2897903A1
公开(公告)日：2015-07-29
申请号：EP13762810.3
申请日：2013-09-12
申请人： DSM IP Assets B.V.
发明人： TINGE, Johan Thomas , EKKELENKAMP, Geert , VONK, Pieter
IPC分类号： C01C1/248 , B01D9/00 , C05C3/00
CPC分类号： C01C1/248 , B01D9/0031 , B01D9/0036 , B01D9/0063 , C01C1/24 , C05C3/005
摘要： The invention relates to a process for preparing a crystalline ammonium sulfate product, which process comprises: a) subjecting in a crystallizer a feed solution of ammonium sulfate to crystallization to form a first slurry of ammonium sulfate crystals; b) subjecting the first slurry of ammonium sulfate crystals to a first size classification to yield a first coarse ammonium sulfate crystal fraction and a first fine ammonium sulfate crystal fraction; c) recycling at least part of the first fine ammonium sulfate crystal fraction to the feed solution of ammonium sulfate; and d) recovering a crystalline ammonium sulfate product from the first coarse ammonium sulfate crystal fraction, characterized in that: e) a second size classification is carried out on a second slurry of ammonium sulfate crystals to yield a second coarse ammonium sulfate crystal fraction and a second fine ammonium sulfate crystal fraction.
摘要翻译：本发明涉及一种制备结晶硫酸铵产物的方法，该方法包括：a）在结晶器中使硫酸铵的进料溶液结晶以形成硫酸铵晶体的第一浆料; b）使硫酸铵晶体的第一浆料进行第一粒度分级以产生第一粗硫酸铵晶体级分和第一细小硫酸铵晶体级分; c）将至少部分第一细小硫酸铵结晶部分再循环到硫酸铵的进料溶液中; 和d）从所述第一粗硫酸铵晶体级分回收结晶硫酸铵产物，其特征在于：e）在硫酸铵晶体的第二浆料上进行二次分级，得到第二粗硫酸铵晶体级分和第二细小的硫酸铵结晶部分。

32. 发明公开

EP2578558A1 Process for the recycling of the nutrient elements used by crops 审中-公开
标题翻译： Verfahren zurRückgewinnungvonPflanzenernährungselementen
公开(公告)号：EP2578558A1
公开(公告)日：2013-04-10
申请号：EP12186633.9
申请日：2012-09-28
申请人： Agroittica Acqua e Sole S.p.A.
发明人： Natta, Giuseppe , Donati, Gianni
IPC分类号： C05F17/00 , B01D53/58 , C05C3/00
CPC分类号： C05C3/00 , C05F17/0018 , C05F17/0027 , C12M21/04 , C12M29/18 , C12M29/24 , C12M29/26 , C12M41/18 , C12M47/18 , Y02E50/343 , Y02P20/145 , Y02W30/43 , Y02W30/47
摘要： Process for the recycling of nutrient elements and for the preparation of fertilisers from organic waste coming from the cycle of production and consumption of foods by subjecting the wastes to an anaerobic fermentation in order to obtain a digestate and biogas; extracting ammonia from the digestate with a gas; absorbing the ammonia with a fluid containing sulphuric or phosphoric acid for the production of ammonium sulphate / phosphate. The remaining digestate can also be used as a fertiliser.
摘要翻译：通过对废物进行厌氧发酵以获得消化和生物气体来回收营养元素和从生产和消费食品循环的有机废物中制备化肥的过程; 用气体从消化液中提取氨; 用含有硫酸或磷酸的流体吸收氨以生产硫酸铵/磷酸盐。剩余的消化物也可以用作肥料。

33. 发明公开

EP2149542A3 Verfahren zur Gewinnung von Calciumcarbonat- und Ammoniumsulfatdünger aus organischem Abfall und Anlage zur Durchführung des Verfahrens 审中-公开
标题翻译：一种用于从有机废物和植物中回收碳酸钙和硫酸铵化肥用于实施该方法的工序
公开(公告)号：EP2149542A3
公开(公告)日：2012-08-08
申请号：EP09008479.9
申请日：2009-06-29
申请人： Hansen, Petra
发明人： Hansen, Petra
IPC分类号： C05D3/02 , C05C3/00 , C01C1/244 , C01D7/02 , C05F3/00 , C05F17/00
CPC分类号： C05C3/00 , C01C1/244 , C01F11/18 , C05D3/02 , C05F3/00 , C05F17/0054 , Y02A40/205 , Y02P20/129 , Y02P20/145 , Y02W30/43
摘要： Verfahren zur Gewinnung von Calciumcarbonat- und Ammoniumsulfatdünger aus organischen Stoffen mit den Schritten: Erwärmen der organischen Stoffe auf eine Temperatur bei der Ammoniak und Kohlendioxid aus dem organischen Stoffe ausgasen, und Einleiten der Gase in eine wässrige Gips-Suspension zur Bildung einer wässrigen, Calciumcarbonat enthaltenden Ammoniumsulfatlösung, gekennzeichnet durch die Schritte Abscheiden und Entfernen des unlöslichen Calciumcarbonats, Aufkonzentrieren der Ammoniumsulfatlösung bis zur Sättigungsgrenze Sättigungsgrenze durch Erwärmen und/oder Erzeugen eines Vakuums, Abkühlen der Ammoniumsulfatlösung auf eine Temperatur bei der die Löslichkeitsgrenze des Ammoniumsulfats unterschritten wird und Abscheiden und Entfernen des unlöslichen Ammoniumsulfats und Trocknen des abgeschiedenen unlöslichen Calciumcarbonat und/oder des unlöslichen Ammoniumsulfats.

34. 发明公开

EP2477961A1 REMOVAL OF UREA AND AMMONIA FROM EXHAUST GASES 有权转让
标题翻译：尿素和氨的废气中去除
公开(公告)号：EP2477961A1
公开(公告)日：2012-07-25
申请号：EP10740669.6
申请日：2010-08-10
申请人： Stamicarbon B.V.
发明人： MEESSEN, Jozef Hubert , ORFANIDIS, Pantelis
IPC分类号： C07C273/16 , C01C1/12 , C05C3/00 , C05C9/00 , C05G3/00
CPC分类号： C05C3/00 , B01D53/54 , B01D53/58 , B01D53/80 , B01D2251/506 , B01D2257/406 , B01D2257/70 , C01C1/12 , C01C1/22 , C05C3/005 , C05C9/00 , C07C273/16
摘要： The invention relates to a method for recovery of urea dust and ammonia from a gas stream by contacting said gas stream with an aqueous sulphuric acid solution, thus forming an acid solution of ammonium sulphate and urea, characterized in that the acid solution is concentrated to a melt comprising less than 5 wt% of water, which melt is subsequently transferred into solid particles comprising urea and ammonium sulphate

35. 发明公开

EP1945596A4 ORGANIC CONTAINING SLUDGE TO FERTILIZER ALKALINE CONVERSION PROCESS 失效转让
标题翻译：碱法转换有机物含污泥肥料的
公开(公告)号：EP1945596A4
公开(公告)日：2012-07-18
申请号：EP06814769
申请日：2006-09-15
申请人： VITAG CORP
发明人： BURNHAM JEFFREY C
IPC分类号： C05F7/00 , C02F11/14 , C05C3/00 , C05F17/00 , C05F17/02
CPC分类号： C05B17/00 , A45D20/18 , C02F11/06 , C02F11/14 , C05C3/00 , C05C7/00 , C05C11/00 , C05F3/00 , C05F5/008 , C05F7/00 , C05F9/00 , C05F11/00 , C05G3/0088 , Y02A40/205 , Y02A40/212 , Y02A40/213 , Y02A40/214 , Y02P20/145 , Y02W30/43 , C05D3/02
摘要： This invention is directed to systems, devices and methods for treating organic-containing sludges and converting such sludges to high value fertilizers containing both inorganic and organic fertilizer components, which creates an inorganically-augmented bioorganic fertilizer. The invention describes methods to create a thixotrophic or paste-like material via the application of mixing energy to the organic sludge followed by an alkaline treatment and a subsequent ammoniation. The invention further describes a method to increase the plant nutrient content in the organic containing product to a level which permits the finished granular fertilizer product to compete in the commercial agricultural fertilizer marketplace. Further, the invention reduces odors associated with said organic-containing sludges.

36. 发明公开

EP2462086A2 NEUER N/S-FLÜSSIGDÜNGER MIT HOHEM NÄHRSTOFFGEHALT 有权
标题翻译： NEW N /营养物的含量高S液位肥料
公开(公告)号：EP2462086A2
公开(公告)日：2012-06-13
申请号：EP10743025.8
申请日：2010-07-28
申请人： SKW STICKSTOFFWERKE PIESTERITZ GmbH
发明人： REINHARDT, Petra , NICLAS, Hans-Joachim , RADICS, Ute , FUCHS, Michael
IPC分类号： C05G5/00 , C05G3/08 , C05C1/00 , C05B7/00 , C05C9/00 , C05G3/00 , C05C3/00 , C05F7/00
CPC分类号： C05C1/00 , C05B7/00 , C05C3/00 , C05C9/00 , C05F7/00 , C05G3/0076 , C05G3/08 , Y02A40/213 , Y02P60/218
摘要： The invention relates to a nutrient-rich nitrogen-sulphur liquid fertiliser having a total nutrient content of more than 25% and a nitrogen-sulphur ratio of 4-5:1, and containing between 28 and 30% of ammonium nitrate, between 22 and 28 % of urea, between 8 and 9 % of ammonium sulfate, between 7 and 10% of ammonium thiosulfate, and at least one phosphate salt in a concentration inhibiting steel corrosion.

37. 发明授权

EP1685084B1 VERFAHREN UND VORRICHTUNG ZUR GEWINNUNG VON STICKSTOFFDÜNGER AUS ORGANISCHEN ABFALLPRODUKTEN 有权
标题翻译：方法和装置用于获得氮肥有机废物
公开(公告)号：EP1685084B1
公开(公告)日：2012-05-09
申请号：EP04803163.7
申请日：2004-11-15
申请人： Phoenix Beteiligungs GmbH
发明人： SPINDLER, Herbert , BAUERMEISTER, Ute , MEIER, Thomas , TESKE, Michael
IPC分类号： C05C3/00 , C05D3/02 , C05F3/00 , C01C1/242 , C01F11/18
CPC分类号： C05F17/0018 , C05C3/005 , C05D3/02 , C05F3/00 , Y02A40/205 , Y02E50/343 , Y02P20/145 , Y02W30/43 , C05D9/00 , C05F3/06
摘要： The invention relates to a method and device for obtaining nitrogenous fertilisers from organic waste products in liquid phase (suspension, emulsion, solution), for the sanitation of the wastes and for emission reduction by thermal treatment using mineral or organic adjuncts. According to the invention, the above is achieved by means of a method in which the waste product is heated to a temperature of between 40 °C and 90 °C at a reduced pressure, the gas emitted, which contains carbon dioxide and ammonia, is cooled and introduced into an aqueous absorption agent, the nitrogenous fertiliser thus produced is removed and the excess unabsorbed gas containing carbon dioxide is pumped back into the waste chamber, whereby the vacuum generated at the beginning of the process by a vacuum pump is self-maintaining. The recycling of the excess gas into the circuit is advantageously achieved either directly above the waste product for treatment, or via a gas cooling system directly above the waste product for treatment, or in divided form, with a part stream through the waste product and a part stream above the waste product. A gypsum slurry is preferably used as aqueous absorption agent.

38. 发明公开

EP2414307A2 PASTILLATION OF AMMONIUM SULFATE NITRATE 有权转让
标题翻译： PASTILLIERUNG VON AMMONIUMSULFATNITRAT
公开(公告)号：EP2414307A2
公开(公告)日：2012-02-08
申请号：EP10762164.1
申请日：2010-03-30
申请人： Honeywell International Inc.
发明人： SMITH, Michael R.
IPC分类号： C05C13/00 , C05C1/02 , C05C3/00 , B01J2/20
摘要： A process is presented for the production of ammonium sulfate nitrate. The process provides for producing a highly uniform product and having a substantially uniform size. The process includes reacting ammonium sulfate and ammonium nitrate to form an FASN slurry melt. The slurry melt is continuously stirred and heated to keep the slurry melt under a shear thinned condition and at a uniform temperature until the slurry melt is extruded, cooled and solidified.
摘要翻译：介绍了生产硝酸铵的方法。该方法提供生产高度均匀的产品并具有基本均匀的尺寸。该方法包括使硫酸铵和硝酸铵反应形成FASN浆料熔体。将浆料熔体连续搅拌和加热，以使浆料熔融在剪切变稀条件下并且在均匀的温度下直到浆料熔体被挤出，冷却和固化。

39. 发明公开

EP2303803A1 PELLETIZED AMMONIUM SULFATE PARTICLES 审中-公开
标题翻译：丸形硫酸铵
公开(公告)号：EP2303803A1
公开(公告)日：2011-04-06
申请号：EP09802490.4
申请日：2009-07-22
申请人： DSM IP Assets B.V.
发明人： HUFFMANN, Steven , PARKINSON IV, James Franklin , FINE, Justive
IPC分类号： C05C3/00
CPC分类号： C05C3/005 , C01C1/24 , C01P2004/50
摘要： The invention relates to a method for preparing pelletized ammonium sulfate particles, the method comprising - providing ammonium sulfate crystals; - isolating a fraction comprising crystals having an intermediate size from crystals having a small size and from crystals having a large size, thereby obtaining remaining crystals comprised of crystals having small size and crystals having large size; and - pelletizing through a die at least part of the remaining crystals, i.e. at least part of the crystals from which the fraction comprising crystals having the intermediate size have been isolated, thereby forming pelletized ammonium sulfate particles.

40. 发明授权

EP2051953B1 GRANULATED FERTILIZER CONTAINING WATER SOLUBLE FORMS OF NITROGEN, MAGNESIUM AND SULPHUR, AND METHOD OF ITS PREPARATION 有权
标题翻译：肥料颗粒使氮，镁，硫成分：水可溶性形式，以及生产方法
公开(公告)号：EP2051953B1
公开(公告)日：2010-04-28
申请号：EP07769076.6
申请日：2007-07-25
申请人： Duslo, A.S.
发明人： LENCSES, Ladislav , KRALIK, Milan , LEHOCKY, Peter , STEFANCOVA, Radka , KERDO, Pavol , FERENCI, Michal , POLAK, Anton
IPC分类号： C05C1/00 , C05C3/00 , C05D5/00 , C05D9/00
CPC分类号： C01C1/18 , C01C1/24 , C01F5/40 , C05C1/00 , C05C3/00 , C05D5/00 , C05G3/0058
摘要： Granulated fertilizer, containing water soluble forms of nitrogen, magnesium and sulphur, contains 15 to 30 % by weight of nitrogen, 1 to 18 % by weight of sulphur, 2 to 10 % by weight of magnesium, expressed as magnesium oxide MgO, in the form of boussingaultite - (NH4)2SO4.MgSO4.6H2O and binary salts ammonium nitrate - 2NH4NO3.(NH4)2SO4 and 3NH4NO3.(NH4)2SO4, wherein the content of boussingaultite in the fertilizer is 40 to 45 % by weight. Magnesite is treated with concentrated nitric acid containing 30 to 80 % of HNO3 at a temperature of 60 °C to 130 °C, under formation of reaction mixture containing magnesium nitrate, calcium nitrate, or possibly, according to the content of metallic compounds in magnesite, nitrates of iron, manganese and further metallic elements, and the remainder of undecomposed magnesite, the reaction mixture is subseguently neutralized with an alkaline agent to pH of 3 to 7.5, the neutralized reaction mixture is subseguently left to react with ammonium sulphate at a temperature of 80 to 130 °C for 20 to 80 minutes under formation of a slurry of boussingaultite (NH4)2SO4-MgSO4.6H2O, containing 10 to 30 % by weight of water, which slurry is mixed with dried recycle from the preceding production in the ratio of 1 :2 to 1 :10 and it is granulated under formation of wet granulate, from which, after removing free water, the final product is obtained.

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