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21. 发明公开

EP0877936A1 DISCONTINUOUS COUNTERCURRENT CHROMATOGRAPHIC PROCESS AND APPARATUS 失效
标题翻译：不连续逆流色谱过程和设备
公开(公告)号：EP0877936A1
公开(公告)日：1998-11-18
申请号：EP96939008.0
申请日：1996-11-12
申请人： MERCK PATENT GmbH
发明人： GRILL, M., Charles , HAMPTON, W., Thomas
IPC分类号： G01N30 , B01D15
CPC分类号： B01D15/1814 , B01D15/1857 , B01D15/1864 , G01N30/44
摘要： A preparative chromatographic cyclical process comprising, at steady state: establishing a figure-of-eight circulating chromatographic profile between two chromatographic columns with the provision that said chromatographic profile never passes through a pump; discontinuously and periodically injecting a sample comprising at least two components, into said circulating profile; and collecting, discontinuously and periodically, at least two enriched fractions from said circulating profile, the apparatus for conducting this process comprising only two chromatographic columns, at least one solvent pump, and injection pump, two 4-way valves, and conduit communicating said columns and the two 4-way valves in the form of a figure-of-eight pattern without traversing a pump, and conduit communicating said at least one solvent pump and at least one of said columns.
摘要翻译：一种制备色谱循环方法，其包括：在稳定状态下：在两个色谱柱之间建立八数循环色谱分布图，条件是所述色谱分布图不会通过泵; 不连续地和周期性地将包含至少两种组分的样品注入到所述循环分布中; 并且不连续地且周期性地从所述循环分布中收集至少两种富集级分，用于进行该方法的装置仅包括两个色谱柱，至少一个溶剂泵和喷射泵，两个四通阀以及连通所述柱以及八个八字形式的两个四通阀不经过泵，以及连通所述至少一个溶剂泵和至少一个所述柱的导管。

22. 发明公开

EP0279946A3 Method of chromatographic separation 失效
标题翻译：色谱分离方法
公开(公告)号：EP0279946A3
公开(公告)日：1990-05-30
申请号：EP87119111.0
申请日：1987-12-23
申请人： Mitsubishi Kasei Engineering Company
发明人： Ando, Masao c/o Mitsubishi-Kasai , Tanimura, Masatake c/o Mitsubishi-Kasai , Tamura, Masao c/o Mitsubishi-Kasai
IPC分类号： B01D15/08
CPC分类号： B01D15/1814
摘要： A chromatographic separation process employing fewer beds packed with an adsorbent, while enabling separation of feedstock fluid, containing a plurality of components which have different degrees of affinity for the adsorbent, into constituent fractions which are withdrawn separately. According to at least one preferred embodiment, a step of supplying feedstock fluid to the simplified separation apparatus is preceded and followed by a step of circulating the fluid through the apparatus, a cycle of supply - desorbing - circulation being carried out repeatedly.

23. 发明公开

EP0279946A2 Method of chromatographic separation 失效
标题翻译： Trennung色谱法。
公开(公告)号：EP0279946A2
公开(公告)日：1988-08-31
申请号：EP87119111.0
申请日：1987-12-23
申请人： Mitsubishi Kasei Engineering Company
发明人： Ando, Masao c/o Mitsubishi-Kasai , Tanimura, Masatake c/o Mitsubishi-Kasai , Tamura, Masao c/o Mitsubishi-Kasai
IPC分类号： B01D15/08
CPC分类号： B01D15/1814
摘要： A chromatographic separation process employing fewer beds packed with an adsorbent, while enabling separation of feedstock fluid, containing a plurality of components which have different degrees of affinity for the adsorbent, into constituent fractions which are withdrawn separately. According to at least one preferred embodiment, a step of supplying feedstock fluid to the simplified separation apparatus is preceded and followed by a step of circulating the fluid through the apparatus, a cycle of supply - desorbing - circulation being carried out repeatedly.
摘要翻译：使用更少的填充有吸附剂的床的色谱分离方法，同时能够将含有对吸附剂具有不同亲和力的多种组分的原料流体分离成分开取出的组成部分。根据至少一个优选实施例，在简化分离装置之前供给原料流体的步骤之前和之后是使流体循环通过该装置的步骤，循环重复进行供给 - 解吸循环。

24. 发明公开

EP4384298A1 INDUSTRIAL METHOD FOR ISOLATING AN ANALYTE FROM A LIQUID MIXTURE 审中-实审
公开(公告)号：EP4384298A1
公开(公告)日：2024-06-19
申请号：EP22765454.8
申请日：2022-08-11
申请人： Bluetech ApS
发明人： PÅLSSON, Michael , HARLOW, Kenneth
IPC分类号： B01D15/18 , B01D15/24 , G01N30/44
CPC分类号： B01D15/1814 , B01D15/1807 , B01D15/24 , G01N2030/883120130101

25. 发明公开

EP3082991A4 A CHROMATOGRAPHY SYSTEM AND METHOD 有权转让
标题翻译：色谱系统解决方案
公开(公告)号：EP3082991A4
公开(公告)日：2017-08-02
申请号：EP14870681
申请日：2014-12-15
申请人： GE HEALTHCARE BIO-SCIENCES AB
发明人： OLOVSSON BJORN
IPC分类号： B01D15/18 , F16K11/02 , F16K11/074 , G01N30/20
CPC分类号： B01D15/1842 , B01D15/1814 , B01D15/1821 , B01D2215/023 , B01D2215/024 , F16K11/02 , F16K11/074 , G01N30/20 , G01N30/468 , G01N30/6034 , G01N2030/202
摘要： A chromatography system comprising at least two chromatography columns, where a feed recirculation of outflow from a primary load column to the inlet of a secondary load column is combined such that the feed recirculation outflow from all columns that will be used as primary load columns in the system will pass through one and the same feed recirculation flow path.
摘要翻译：包括至少两个色谱柱的色谱系统，其中将从主要负载柱流出到二级负载柱入口的进料再循环组合，使得来自将用作主要负载柱的所有柱的进料再循环流出系统将通过同一个进料再循环流动路径。

26. 发明授权

EP0279946B1 Method of chromatographic separation 失效
标题翻译：色谱分离方法
公开(公告)号：EP0279946B1
公开(公告)日：1993-08-18
申请号：EP87119111.0
申请日：1987-12-23
申请人： Mitsubishi Kasei Engineering Company
发明人： Ando, Masao c/o Mitsubishi-Kasai , Tanimura, Masatake c/o Mitsubishi-Kasai , Tamura, Masao c/o Mitsubishi-Kasai
IPC分类号： B01D15/08
CPC分类号： B01D15/1814

27. 发明授权

EP0309380B1 Recycle chromatograph with supercritical fluid 失效
标题翻译：具有超临界流体的回收色谱
公开(公告)号：EP0309380B1
公开(公告)日：1992-11-25
申请号：EP88710032.9
申请日：1988-09-26
申请人： JASCO CORPORATION
发明人： Saito, Muneo , Yamauchi, Yoshio
IPC分类号： B01D15/08
CPC分类号： B01D15/40 , B01D15/1814 , G01N30/02

28. 发明公开

EP0464277A1 Process for the separation by adsorption of 2,6- or 3,5-diethyltoluene from a mixture thereof with another diethyltoluene isomer 失效
标题翻译：一种用于从与另一Diethyltoluolisomer它们的混合物通过2,6-或3,5-二乙基的吸附分离过程。
公开(公告)号：EP0464277A1
公开(公告)日：1992-01-08
申请号：EP90307281.7
申请日：1990-07-03
申请人： UOP
发明人： Zinnen, Herman A.
IPC分类号： C07C15/02 , C07C7/13
CPC分类号： B01D15/08 , B01D15/1814 , C07C7/13 , C07C15/02
摘要： 3,5-diethyltoluene (3,5-DET) and/or 2,6-diethyltoluene (2,6-DET) is selectively separated from a feed mixture comprising at least one isomer from the group 3,5-DET or 2,6-DET and at least one other DET isomer by contacting the feed mixture at adsorption conditions with an adsorbent selected from the Groups consisting of A) X zeolite exchanged with a potassium cation; B) X zeolite exchanged with sodium or copper or Y zeolite exchanged with copper, sodium, barium or calcium; and C) X zeolite exchanged with barium or lithium or with potassium and barium or Y zeolite exchanged with potassium, sodium, barium or calcium, thereby selectively adsorbing one of the DET isomers contained in the feed; thereby selectively adsorbing one or more of said DET isomers and removing one or more relatively non-adsorbed isomer(s) from contact with the adsorbent to form a raffinate stream depleted in the adsorbed isomer relative to feed and thereafter contacting the rich adsorbent with a desorbent comprising a monocyclic alkyl-substituted aromatic hydrocarbon at desorption conditions effective to form an extract stream enriched in the adsorbed isomer relative to the feed.
摘要翻译： 3.5二乙基（3,5- DET）和/或2,6-二乙基（2,6- DET）被选择性地从供料混合物选自3,5- DET或2，其包含至少一种异构体分离， 6-DET以及通过在从所述组包括A）X沸石与钾交换的阳离子选择吸附剂与接触在吸附条件下的进料混合物中的至少一种其它DET异构体; B）X沸石交换了钠或铜或Y型沸石与铜，钠，钡或钙交换的; 和C）X沸石交换了钡或锂或钾和钡或Y型沸石与钾，钠，钡或钙，从而选择性地吸附进料中所含的DET异构体之一交换的; 从而选择性地吸附。所述DET异构体的一个或多个以及去除一个或多个相对非吸附从与吸附剂接触的异构体（一个或多个），以形成吸附异构体相对于在贫萃余液料流喂后，用解吸剂接触富吸附剂包含有效解吸条件下的单环烷基芳烃substituiertem以形成提取吸附的异构体相对于进料的富含流。

29. 发明公开

EP0309380A2 Recycle chromatograph with supercritical fluid 失效
标题翻译： Umlaufchromatograph mitüberkritischem流体。
公开(公告)号：EP0309380A2
公开(公告)日：1989-03-29
申请号：EP88710032.9
申请日：1988-09-26
申请人： JASCO CORPORATION
发明人： Saito, Muneo , Yamauchi, Yoshio
IPC分类号： B01D15/08
CPC分类号： B01D15/40 , B01D15/1814 , G01N30/02
摘要： It is an object to provide a recycle chromatograph with supercritical fluid mobile phase for separating a sample into components by recycling a mobile phase which includes modifier solvent for the purpose of taking a desired component.
It is structured in such a manner that a recycling pump (10), a column (14), a detector (16), and a three-way valve (18) are connected in a sequential order as described above to form a closed loop which acts as a recycle flow line. A back-pressure regulator (20) is connected to the remainder port (C) of this three-way valve (18), and a mobile phase supplying device (30, 38, 30A, 38A, 48) for supplying the mobile phase under a predetermined pressure is connected to a flow line between the three-way valve (18) and the recycling pump (10).
By means of this mobile phase supplying device and the recycle closed loop (the column pressure drop Δ p)/(column plate number) can be reduced, whereupon the column effective plate number can be increased. Thus, a sufficient resolution rate for fractionating a component can be obtained after appropriate recycling times.
Furthermore, by combining the mobile phase supplying device (30, 38, 30A, 38A, 48) and the back-pressure regulator (20), the internal pressures in the column and the detector can be kept above the critical pressure even if unnecessary components are being removed or a necessary component is being fractionated. As a result of which fractionation can be performed.
摘要翻译：本发明的目的是提供一种具有超临界流体流动相的再循环色谱仪，用于通过循环包含改性剂溶剂的流动相将样品分离成组分，以获得所需组分。以如上所述的顺序连接回收泵（10），塔（14），检测器（16）和三通阀（18）的结构，形成闭环其充当循环流动线。背压调节器（20）连接到该三通阀（18）的剩余端口（C），以及流动相供应装置（30,38,30A，38A，48）预定压力连接到三通阀（18）和回收泵（10）之间的流动管线。通过该流动相供给装置和再循环闭环（柱压降DELTA p）/（塔板数）可以减少，从而可以增加柱有效板数。因此，在适当的回收时间之后，可以获得用于分馏成分的足够的分离率。此外，通过组合流动相供给装置（30,38,30A，38A，48）和背压调节器（20），即使不需要的组分，也可以将柱和检测器中的内部压力保持在临界压力以上正在被去除或必要的组件被分馏。结果可以进行分馏。

30. 发明公开

EP0067372A1 Liquid chromatography process 失效
标题翻译：液相色谱法。
公开(公告)号：EP0067372A1
公开(公告)日：1982-12-22
申请号：EP82104869.1
申请日：1982-06-03
申请人： Asahi Kasei Kogyo Kabushiki Kaisha
发明人： Tanouchi, Masatoshi , Akiyama, Hirohumi
IPC分类号： B01D15/08 , G01N31/08
CPC分类号： G01N30/00 , B01D15/1814 , B01D53/025 , C07C7/13 , C10G25/03 , G01N30/80 , C07C15/08
摘要： An adsorptive separation method capable of effectively separating the desired component from a mixture containing the same at a high purity and a high recovery ratio, and easily which copes with scale-up of the apparatus is disclosed. This method comprises alternately supplying a starting mixture A, comprising a plurality of substances, and a desorbent into a column packed with an adsorbent, treating to form and move an adsorption band of the starting mixture A and recovering the intended component at a purity higher than the aimed purity from an eluate, wherein after the entire amount of the intended component passing through the column is increased over the amount of the intended component in the starting mixture A and the intended component is separated and recovered, the portion B which is at least a part of the remaining intended component-containing portion, and in which the desorbent is separated and removed to a concentration lower than the desorbent concentration in the starting mixture A and the intended component is contained at a concentration higher than the concentration of the intended component in the starting mixture A is mixed with the starting material A and supplied to the column or said portion B and the starting mixture A are supplied to the column one by one, and then, the desorbent is supplied successively.

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