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11. 发明公开

EP0065354A1 Process for the preparation of 1,1-bis phenyl-2-haloalkan-1-ols 失效
标题翻译： Verfahren zur Herstellung von 1.1-双 - 苯基-2-卤代烷-1-醇。
公开(公告)号：EP0065354A1
公开(公告)日：1982-11-24
申请号：EP82301964.1
申请日：1982-04-16
申请人： IMPERIAL CHEMICAL INDUSTRIES PLC
发明人： Falconer, James Alexander , Fleming, Ian George Cameron , Jones, Raymond Vincent Heavon , Ewins, Robert Comgall
IPC分类号： C07C33/46 , C07C29/62 , C07C29/66
CPC分类号： A01N43/653 , C07C29/40 , C07C29/62 , C07C29/66 , C07C33/46
摘要： Halohydrins of the formula:
wherein R and R 1 , which may be the same or different, are hydrogen or alkyl; X, Y and Z are each independently hydrogen, fluorine or chlorine and A is chlorine or bromine, are prepared by reacting a tertiary alcohol of the formula
or a substituted alkene of the formula
with chlorine, bromine, hypochlorous acid or hypobromous acid in an aqueous medium. Preferably the aqueous medium is a mixture of water and an amide solvent selected from dimethyl formamide, diethyl formamide and dimethyl acetamide and the reaction is carried out in the presence of hydrogen peroxide.
The halohydrins are useful intermediates for fungicides.
摘要翻译：下式的卤代醇：其中R和R 1可以相同或不同，是氢或烷基; X，Y和Z各自独立地为氢，氟或氯，A为氯或溴，通过使式的叔醇或式CHEM的取代烯与氯，溴，次氯酸反应制备或次溴酸。优选地，水性介质是水和选自二甲基甲酰胺，二乙基甲酰胺和二甲基乙酰胺的酰胺溶剂的混合物，反应在过氧化氢存在下进行。卤代醇是杀真菌剂的有用中间体。

12. 发明公开

EP0016433A1 Verfahren zur kontinuierlichen Herstellung von Propylenchlorhydrinen 无效
标题翻译： Verfahren zur kontinuierlichen Herstellung von Propylenchlorhydrinen。
公开(公告)号：EP0016433A1
公开(公告)日：1980-10-01
申请号：EP80101341.8
申请日：1980-03-14
申请人： BASF Aktiengesellschaft
发明人： Koehler, Waldemar, Dr. , Langensiepen, Hans-Werner, Dr. Dipl.-Ing. , Volkamer, Klaus, Dr.
IPC分类号： C07C29/66 , C07C31/36
CPC分类号： C07C29/66 , C07C31/36
摘要： Kontinuierliche Herstellung von Propylenchlorhydrin durch Umsetzung von Chlor und Proppylen in wäßrigerLösung bei 20 bis 80°C und erhöhtem Druck, indem man die Ausgangsstoffe, Chlor, Propylen und Wasser in gleichgerichteter Strömung unter einem Druck von 15 bis40 bar umsetzt, ohne einen Teilstrom des Umsetzungsgemisches wieder in die Umsetzungszone zurückzuführen.
摘要翻译： 1.一种通过在20〜80℃的超大气压下使水溶液中的氯化钴和丙烯反应连续制备丙烯氯醇的方法，其特征在于以并流流动的原料氯，丙烯和水为在15至40巴的压力下反应，而不将反应混合物的一部分物流再循环到反应区。

13. 发明授权

EP0767771B2 CHLOROHYDRIN PROCESS 失效
标题翻译：氯醇法
公开(公告)号：EP0767771B2
公开(公告)日：2004-05-06
申请号：EP95922108.6
申请日：1995-05-24
申请人： THE DOW CHEMICAL COMPANY
发明人： JORGE, Edward, M.
IPC分类号： C07C29/66 , C07C31/36 , C07D301/26 , C01B11/06
CPC分类号： C07D301/26 , C01B11/06 , C01B11/062 , C01B11/064 , C07C29/66 , C07C31/36
摘要： This invention is a process for preparing chlorohydrins by reacting a chlorinating species, such as hypochlorous acid, with at least one unsaturated organic compound, such as propylene or butylene, at a pH of greater than 6.0. The chlorinating species is formed in a first step by reacting a source of chlorine, such as Cl2 gas, with an aqueous pH adjusting source, such as aqueous NaOH.

14. 发明公开

EP0537846A1 Production of dichlorohydrin 失效
标题翻译： Herstellung von Dichlorhydrin。
公开(公告)号：EP0537846A1
公开(公告)日：1993-04-21
申请号：EP92203109.1
申请日：1992-10-08
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： John, Christopher Stephen , Maas, Wilfridus Petrus Maria
IPC分类号： C07C31/36 , C07C29/66
CPC分类号： C07C29/66 , C07C31/36
摘要： The invention relates to a process for the production of dichlorohydrin which comprises reacting allylchloride, water and chlorine in a reaction zone to form an aqueous dichlorohydrin solution together with other chlorinated organic byproducts, and contacting the aqueous reaction zone effluent with 1,2,3-trichloropropane to obtain an aqueous layer comprising the dichlorohydrin and an organic layer comprising the trichloropropane and said chlorinated organic byproducts, separating both layers and if desired working up the dichlorohydrin containing aqueous solution in a manner known per se.
摘要翻译：本发明涉及一种制备二氯丙醇的方法，该方法包括在反应区中使烯丙基氯，水和氯与其他氯化有机副产物一起形成二氯丙醇水溶液，并将含水反应区流出物与1,2,3- 得到包含二氯丙醇的水层和包含三氯丙烷和所述氯化有机副产物的有机层，分离两层，如果需要，以本身已知的方式处理含二氯丙醇的水溶液。

15. 发明公开

EP0253448A1 Process for the production of dichlorohydrin 失效
标题翻译： Herstellungsverfahren von Dichlorohydrin。
公开(公告)号：EP0253448A1
公开(公告)日：1988-01-20
申请号：EP87201336.2
申请日：1987-07-13
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Blytas, George Constantin , Grimsby, Frank Norman , Scamehorn, John Frederick
IPC分类号： C07C31/36 , C07C29/66 , C07C29/76
CPC分类号： C07C31/36 , B01D61/025 , C07C29/76
摘要： The invention relates to a continuous process for the production of dichlorohydrin which comprises:

(a) reacting allyl chloride, water and chlorine in a reaction zone to form an aqueous reaction mixture of dichlorohydrin and reaction by-products,
(b) passing said reaction mixture from said reaction zone as feed to a reverse osmosis zone,
(c) subjecting said feed to reverse osmosis to afford: (1) a retentate stream having a dichlorohydrin content higher than said feed, and (2) a permeate stream having a dichlorohydrin content less than 10 per cent by weight of the dichlorohydrin content in said feed,
(d) withdrawing said retentate stream, and
(e) recycling at least part of said permeate stream to said reaction zone.
摘要翻译：本发明涉及一种用于制备二氯丙醇的连续方法，其包括：（a）在反应区中使烯丙基氯，水和氯反应以形成二氯丙醇和反应副产物的水反应混合物，（b）使所述反应混合物（c）使所述进料反向渗透得到：（1）二氯代丙醇含量高于所述进料的滞留物流，和（2）具有二氯丙醇含量的渗透物流所述进料中二氯丙醇含量小于10重量％，（d）取出所述滞留物流，和（e）将至少部分所述渗透物流再循环至所述反应区。一世

16. 发明公开

EP0228118A2 Process for the production of dichlorohydrin 失效
标题翻译：生产二氯丙醇的方法
公开(公告)号：EP0228118A2
公开(公告)日：1987-07-08
申请号：EP86202158.1
申请日：1986-12-03
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： Blytas, George Constantin , Foster, Elton Gordon , Grimsby, Frank Norman
IPC分类号： C07C29/66 , C07C29/86 , C07C31/36 , C07C31/10
CPC分类号： C07C31/36 , B01D61/44 , B01D2311/04 , B01D2311/10 , B01D2311/12
摘要： The invention relates to a continuous process for the production of an organic solvent solution of dichlorohydrin, which comprises:

a) reacting allyl chloride, water and chlorine in a reaction zone to form an aqueous solution of dichlorohydrin,
b) contacting in an extraction zone the reaction zone effluent with a water-immiscible inert organic solvent for the dichlorohydrin to obtain a dichlorohydrin-enriched solvent and an aqueous phase,
c) passing said dichlorohydrin-enriched solvent from said extraction zone,
d) passing said aqueous phase from the extraction zone to an electrodialysis zone,
e) electrodialyzing said aqueous phase in said electrodialysis zone to obtain: (1) a concentrate stream having chloride content higher than said aqueous phase, and (2) a diluate stream having chloride content lower than said aqueous phase,
f) withdrawing said concentrate stream, and
g) recycling at least part of said diluate stream from step (e) to the reaction zone of step (a).
摘要翻译：本发明涉及生产二氯丙醇有机溶剂溶液的连续方法，该方法包括：a）使烯丙基氯，水和氯在反应区中反应以形成二氯丙醇水溶液，b）在提取区中使反应区流出物与水不混溶的惰性有机溶剂混合以得到二氯丙醇富集溶剂和水相，c）使所述富含二氯丙醇的溶剂从所述萃取区通过，d）将所述水相从萃取区通入 e）在所述电渗析区中对所述水相进行电渗析以获得：（1）具有比所述水相高的氯化物含量的浓缩物流，和（2）具有比所述水相低的氯化物含量的稀释物流，f）回收所述浓缩物流，和g）将来自步骤（e）的至少部分所述稀释物流再循环至步骤（a）的反应区。

17. 发明授权

EP0065354B1 Process for the preparation of 1,1-bis phenyl-2-haloalkan-1-ols 失效
标题翻译：制备1,1-BIS苯基-2-羟基烷-1-醇的方法
公开(公告)号：EP0065354B1
公开(公告)日：1985-07-03
申请号：EP82301964.1
申请日：1982-04-16
申请人： IMPERIAL CHEMICAL INDUSTRIES PLC
发明人： Falconer, James Alexander , Fleming, Ian George Cameron , Jones, Raymond Vincent Heavon , Ewins, Robert Comgall
IPC分类号： C07C33/46 , C07C29/62 , C07C29/66
CPC分类号： A01N43/653 , C07C29/40 , C07C29/62 , C07C29/66 , C07C33/46

18. 发明公开

EP0008581A1 METHOD OF PREPARING E-4-ACETOXY-2-METHYL-2-BUTENAL. 失效
标题翻译： PRODUCING方法E-4-乙酰氧基-2-甲基-2-烯醛。
公开(公告)号：EP0008581A1
公开(公告)日：1980-03-05
申请号：EP79900203
申请日：1979-07-31
申请人： BABLER JAMES H
发明人： BABLER JAMES H
IPC分类号： C07C29/66 , C07C67/28
CPC分类号： C07C29/66 , C07B2200/09 , C07C67/00 , C07C67/29 , C07C67/293 , C07C33/423 , C07C69/145 , C07C69/63
摘要： On prepare le E-4-acetoxy-2-methyl-2-butenal par: 1) preparation d'un halogenure allylique intermediaire; et 2) par reaction de cet halogenure avec de l'oxysulfure de dimethyle en presence d'une base non-nucleophile, pour former le produit desire.

19. 发明公开

EP3365275A1 ASYMMETRIC ELECTROCHEMICAL CELL APPARATUS, AND OPERATING METHODS THEREOF 审中-公开
公开(公告)号：EP3365275A1
公开(公告)日：2018-08-29
申请号：EP16855018.4
申请日：2016-08-25
申请人： Bar-Ilan University
发明人： AURBACH, Doron , AVRAHAM, Eran , COHEN, Izaak
IPC分类号： C01B11/04 , C01B11/06 , C07C29/66 , C07C33/42 , C02F1/46 , C25B1/26
CPC分类号： C02F1/4618 , C01B11/04 , C01B11/06 , C02F1/46109 , C02F1/467 , C02F2001/46133 , C02F2001/46185 , C02F2201/4618 , C02F2209/06 , C02F2307/02 , C25B1/26 , C25B9/06 , C25B11/0415 , C25B15/02 , C25B15/08
摘要： Asymmetric electrochemical cell apparatus, and methods of operating such apparatus to produce electrolyzed water.

20. 发明公开

EP1140752A1 PROCESS FOR PREPARING CHLOROHYDRINS 审中-公开
标题翻译：用于生产氯代
公开(公告)号：EP1140752A1
公开(公告)日：2001-10-10
申请号：EP99966146.5
申请日：1999-12-13
申请人： THE DOW CHEMICAL COMPANY
发明人： GREEN, Daniel, Patrick , KLIER, John , TUCKER, Christopher, J. , FERRITTO, Michael, S.
IPC分类号： C07C29/66
CPC分类号： C07C29/66 , C07C31/36
摘要： A process for hypochlorinating unsaturated alpha-olefins to produce chlorohydrins which comprises forming a microemulsion of water and an unsaturated alpha-olefin and then adding an oxidant to the microemulsion under conditions sufficient to form the chlorohydrins. The microemulsion is formed by adding a non-nucleophilic surfactant and, optionally, a co-surfactant, to the mixture of water and unsaturated alpha-olefin.

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