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92. 发明授权

EP2796598B1 Carbon fiber and catalyst for manufacture of carbon fiber 有权
标题翻译：碳纤维和用于生产碳纤维的催化剂
公开(公告)号：EP2796598B1
公开(公告)日：2015-12-09
申请号：EP14168033.0
申请日：2007-12-21
申请人： SHOWA DENKO K.K.
发明人： Kitazaki, Akihiro , Kanbara, Eiji
IPC分类号： D01F9/127 , B01J23/887
CPC分类号： D01F9/12 , B01J21/04 , B01J21/08 , B01J21/185 , B01J23/002 , B01J23/88 , B01J23/881 , B01J23/882 , B01J23/883 , B01J23/887 , B01J23/8872 , B01J23/8877 , B01J23/8878 , B01J23/888 , B01J23/8993 , B01J27/232 , B01J37/0201 , B01J37/0203 , B01J37/18 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/162 , C01B2202/36 , D01F9/127 , D01F9/1273 , Y10T428/13 , Y10T428/2918 , B01J2523/31 , B01J2523/55 , B01J2523/69 , B01J2523/842 , B01J2523/47 , B01J2523/67 , B01J2523/68 , B01J2523/845 , B01J2523/23 , B01J2523/847 , B01J2523/41 , B01J2523/22

93. 发明公开

EP2913303A1 Starke Festkörpersäure auf der Basis eines Polyoxometalats 审中-公开
标题翻译：多金属氧酸盐的基础上强固体酸
公开(公告)号：EP2913303A1
公开(公告)日：2015-09-02
申请号：EP15000212.9
申请日：2015-01-24
申请人： Forschungszentrum Jülich GmbH
发明人： Botar, Bogdan
IPC分类号： C01G39/00 , B01J23/28 , B01J35/10
CPC分类号： C01G39/00 , B01J23/28 , B01J23/881 , B01J35/002 , B01J35/1057 , B01J35/1061 , B01J37/031 , B01J37/30 , C01P2006/16
摘要： Im Rahmen der Erfindung wurde eine Festkörpersäure entwickelt. Diese umfasst einen anionischen Anteil aus einer Mehrzahl von Oxyanionen mindestens eines Metalls sowie einen kationischen Anteil, der durch Protonen teilsubstituiert ist. Erfindungsgemäß liegt das Metall des anionischen Anteils mindestens teilweise in einer niedrigeren als der höchsten Oxidationsstufe vor.
Es wurde erkannt, dass der anionische Anteil auf diese Weise mit besonders vielen negativen Ladungen ausgestattet werden kann. Es lässt sich nun im Vergleich zu den bekannten Festkörpersäuren eine deutlich größere Anzahl an kationischen Einheiten pro anionischer Einheit durch Protonen substituieren, so dass die gleiche Stoffmenge an Säure deutlich mehr katalytisch aktive Zentren (Sites) aufweist.
Das Verfahren zur Herstellung einer Festkörpersäure aus einem wasserlöslichen Polyoxometalatsalz mit einem anionischen Anteil und einem kationischen Anteil ist erfindungsgemäß zweistufig. Zuerst wird der kationische Anteil des Salzes mindestens teilweise durch größere, hydrophobe oder amphiphile kationische Einheiten ersetzt. Anschließend werden die hydrophoben oder amphiphilen kationischen Einheiten durch Protonen teilsubstituiert. Durch die erste Substitution des kationischen Anteils wird das Polyoxometalat gleichzeitig stabilisiert und wasserunlöslich gemacht. Dies schafft die Voraussetzung dafür, dass anschließend kationische Einheiten durch Protonen ersetzt werden können, ohne dass die Struktur zusammenbricht.
摘要翻译：在本发明的固体酸的开发。这包括多个含氧阴离子的至少一种金属和其部分被质子取代的阳离子部分的阴离子部分。根据本发明，阴离子部分的金属是至少部分地位于在比最高氧化态的低。人们认识到，阴离子部分可以以这种方式配备大量的负电荷。现在可以与已知的固体酸被质子替换每单位阴离子阳离子单元的显著数量较多，从而使酸的物质相同量的具有显著多种催化活性中心（点）。用于由水溶性多金属氧酸盐的固体酸与阴离子成分和阳离子成分的方法，是根据本发明分两个阶段。首先，该盐的阳离子部分至少部分地与较大的，疏水性或两亲性阳离子单元代替。然后将疏水性或两亲性阳离子单元部分由质子取代。由多金属氧酸盐的阳离子部分的第一置换同时稳定和由不溶于水的。该选项可设置然后阳离子单元可以被质子替换的阶段，没有结构坍塌。

94. 发明公开

EP2902106A1 OXIDE CATALYST, METHOD FOR PRODUCING SAME, AND METHOD FOR PRODUCING UNSATURATED ALDEHYDE, DIOLEFIN OR UNSATURATED NITRILE 审中-公开
标题翻译：氧化物催化剂的方法，用于产生和生产不饱和醛，二烯烃或不饱和腈的方法
公开(公告)号：EP2902106A1
公开(公告)日：2015-08-05
申请号：EP13841762.1
申请日：2013-09-27
申请人： Asahi Kasei Chemicals Corporation
发明人： YOSHIDA, Jun , YAMAGUCHI, Tatsuo
IPC分类号： B01J23/88 , C07C5/48 , C07C11/167 , C07C45/35 , C07C47/22 , C07C253/26 , C07C255/08 , C07B61/00
CPC分类号： B01J23/8898 , B01J21/08 , B01J23/88 , B01J23/881 , B01J23/8871 , B01J23/8872 , B01J23/8876 , B01J35/002 , B01J35/006 , B01J35/023 , B01J35/026 , B01J35/1009 , B01J37/0009 , B01J37/0045 , B01J37/04 , B01J37/08 , B01J2523/00 , C07C5/3332 , C07C5/48 , C07C45/35 , C07C47/22 , C07C253/26 , C07C2523/18 , C07C2523/28 , C07C2523/31 , C07C2523/745 , C07C2523/887 , Y02P20/52 , C07C47/02 , C07C255/08 , C07C11/12 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/15 , B01J2523/3706 , B01J2523/845 , B01J2523/3712 , B01J2523/14 , B01J2523/23 , B01J2523/44 , B01J2523/41 , B01J2523/3718 , B01J2523/22 , B01J2523/847 , B01J2523/13 , B01J2523/27 , C07C11/167 , B01J2523/72
摘要： An object of the present invention is to provide an oxide catalyst that prevents the reduction degradation of the catalyst even during industrial operation for a long time and less reduces unsaturated aldehyde yields, diolefin yields, or unsaturated nitrile yields, and a method for producing the same, and methods for producing unsaturated aldehyde, diolefin, and unsaturated nitrile using the oxide catalyst. The present invention provides an oxide catalyst for use in the production of unsaturated aldehyde, diolefin, or unsaturated nitrile from olefin and/or alcohol, the oxide catalyst satisfying the following (1) to (3): (1) the oxide catalyst comprises molybdenum, bismuth, iron, cobalt, and an element A having an ion radius larger than 0.96 Å (except for potassium, cesium, and rubidium); (2) an atomic ratio a of the bismuth to 12 atoms of the molybdenum is 1 ≤ a ≤ 5, an atomic ratio b of the iron to 12 atoms of the molybdenum is 1.5 ≤ b ≤ 6, an atomic ratio c of the element A to 12 atoms of the molybdenum is 1 ≤ c ≤ 5, and an atomic ratio d of the cobalt to 12 atoms of the molybdenum is 1 ≤ d ≤ 8; and (3) the oxide catalyst comprises a disordered phase consisting of a crystal system comprising the molybdenum, the bismuth, the iron, and the element A.
摘要翻译：本发明的一个目的是提供一种氧化催化剂确实防止甚至相当长的时间和更少的工业操作期间，催化剂的还原降解减少不饱和醛的产率，二烯烃的产率，或不饱和腈的产率，和用于生产其的方法，及其制造方法的不饱和醛，二烯烃和不饱和腈使用氧化物催化剂。对本发明的氧化物催化剂提供用于生产不饱和醛，二烯烃，或从烯烃和/或醇的不饱和腈，满足的氧化物催化剂的下述（1）〜（3）：（1）氧化物催化剂包含钼，铋，铁，钴，和元件的具有上离子半径大于0.96埃（除了钾，铯和铷）; （2）在铋与钼的12原子的原子比a为1‰¤â‰¤5，在铁与钼的12原子的原子比b为1.5‰¤b‰¤6，以原子比元素A与钼的原子12的c为1‰¤ç‰¤5，并在钴的原子比值d至12原子钼的是1‰¤ð‰¤8; 和（3）的氧化物催化剂包括无序相的结晶系统的由含有钼，铋，铁，和元件A.

95. 发明公开

EP2454015A4 CATALYST AND METHODS FOR PRODUCING MULTI-WALL CARBON NANOTUBES 有权
标题翻译：催化剂及其制备方法多壁碳纳米管
公开(公告)号：EP2454015A4
公开(公告)日：2015-06-24
申请号：EP10800624
申请日：2010-07-16
申请人： SOUTHWEST NANOTECHNOLOGIES INC
发明人： SILVY RICARDO PRADA , TAN YONGQIANG
IPC分类号： B01J23/00 , B01J23/84
CPC分类号： B01J27/22 , B01J21/04 , B01J21/10 , B01J23/002 , B01J23/005 , B01J23/75 , B01J23/881 , B01J23/882 , B01J35/0006 , B01J35/006 , B01J35/023 , B01J37/0009 , B01J37/031 , B01J37/04 , B01J37/08 , B01J2523/00 , B82Y30/00 , B82Y40/00 , C01B31/0233 , C01B32/162 , C01B2202/04 , C01B2202/06 , C01B2202/36 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/22
摘要： The present invention provides a catalyst precursor and a catalyst suitable for preparing multi-wall carbon nanotubes. The resulting multi-wall carbon nanotubes have a narrow distribution as to the number of walls forming the tubes and a narrow distribution in the range of diameters for the tubes. Additionally, the present invention provides methods for producing multi-wall carbon nanotubes having narrow distributions in the number of walls and diameters. Further, the present invention provides a composition of spent catalyst carrying multi-wall nanotubes having narrow distribution ranges of walls and diameters.

96. 发明公开

EP2700740A3 Carbon fibers and catalyst for production of carbon fibers 审中-公开
标题翻译：碳纤维，用于生产碳纤维的催化剂。
公开(公告)号：EP2700740A3
公开(公告)日：2014-03-19
申请号：EP13181176.2
申请日：2013-08-21
申请人： SHOWA DENKO KABUSHIKI KAISHA
发明人： Yamamoto, Ryuji , Yamada, Yuusuke , Nakamura, Takeshi
IPC分类号： D01F9/127 , B01J23/847 , B01J23/745 , B01J23/88 , B01J23/881 , H01M4/88 , C01B31/02
CPC分类号： C01B31/02 , B01J21/185 , B01J23/8472 , B01J23/881 , B01J23/8877 , B01J37/0234 , B01J37/0238 , B01J37/04 , B82Y30/00 , B82Y40/00 , C01B32/162 , D01F9/127 , D01F9/1273 , H01G11/40 , H01G11/86 , H01M4/663 , Y02E60/13
摘要： Provided are carbon fibers with low metal ion elution amount without subjecting to high-temperature heat treatment, in which the metal ion may be sometimes precipitated on an electrode of electrochemical devices such as batteries and capacitors to cause short-circuit. The carbon fibers comprises Fe, at least one catalyst metal selected from the group consisting of Mo and V, and a carrier; wherein the carbon fibers have an R value (ID/IG) as measured by Raman spectrometry of 0.5 to 2.0 and have an electrochemical metal elution amount of not more than 0.01 % by mass.

97. 发明授权

EP1965911B1 SCHALENKATALYSATOR, INSBESONDERE ZUR OXIDATION VON METHANOL ZU FORMALDEHYD SOWIE VERFAHREN ZU DESSEN HERSTELLUNG 有权转让
标题翻译：壳催化剂，尤其是对甲醇氧化甲醛及其制造方法
公开(公告)号：EP1965911B1
公开(公告)日：2013-08-14
申请号：EP06818776.4
申请日：2006-11-23
申请人： Süd-Chemie IP GmbH & Co. KG
发明人： GÜCKEL, Christian , WANNINGER, Klaus , ESTENFELDER, Marvin , FISCHER, Claudia , DÜRR, Uwe
IPC分类号： B01J23/881 , B01J35/02 , B01J37/02 , B01J37/08 , C07C45/38
CPC分类号： B01J35/04 , B01J19/30 , B01J23/881 , B01J23/8871 , B01J35/008 , B01J35/023 , B01J35/026 , B01J35/1009 , B01J35/1038 , B01J37/0219 , B01J2219/30215 , B01J2219/30223 , B01J2219/30416 , B01J2219/30475 , C07C45/38 , C07C47/04

99. 发明公开

EP2616425A2 VERFAHREN ZUR HERSTELLUNG VON ACRYLSÄURE AUS METHANOL UND ESSIGSÄURE 无效
标题翻译：工艺生产丙烯酸的甲醇和醋酸
公开(公告)号：EP2616425A2
公开(公告)日：2013-07-24
申请号：EP11758432.6
申请日：2011-09-09
申请人： BASF SE
发明人： HERZOG, Stefanie , ALTWASSER, Stefan , MÜLLER-ENGEL, Klaus Joachim
IPC分类号： C07C45/38 , C07C51/353 , C07C47/04 , C07C47/052
CPC分类号： C07C45/38 , B01J23/002 , B01J23/881 , B01J27/198 , B01J35/0006 , B01J35/023 , B01J37/0009 , B01J37/0045 , B01J2523/00 , C07B2200/05 , C07C51/353 , C07C51/44 , C07C57/04 , C07C47/04 , B01J2523/51 , B01J2523/55 , B01J2523/842
摘要： A process for preparing acrylic acid from methanol and acetic acid, in which, in a reaction zone A, the methanol is partially oxidized to formaldehyde in a heterogeneously catalyzed gas phase reaction, the product gas mixture A obtained and an acetic acid source are used to obtain a reaction gas input mixture B which comprises acetic acid and formaldehyde and has the acetic acid in excess over the formaldehyde, and the formaldehyde present in reaction gas input mixture B is aldol-condensed to acrylic acid under heterogeneous catalysis in a reaction zone B with acetic acid present in reaction gas input mixture B, and unconverted acetic acid still present alongside the acrylic acid target product in the product gas mixture B obtained is removed therefrom, and the acetic acid removed is recycled into the production of reaction gas input mixture B.

100. 发明公开

EP2595744A2 METHOD AND APPARATUS FOR FORMING NANOPARTICLES 审中-公开
标题翻译： VERFAHREN UND VORRICHTUNG ZUR HERSTELLUNG VON NANOPARTIKELN
公开(公告)号：EP2595744A2
公开(公告)日：2013-05-29
申请号：EP11741269.2
申请日：2011-07-19
申请人： Cambridge Enterprise Limited
发明人： ROBERTSON, John , ESCONJAUREGUI, C., Santiago
IPC分类号： B01J21/04 , B01J23/74 , B01J23/745 , B01J35/00 , B01J37/08 , B01J37/12 , B01J37/34 , B01J21/18 , B82Y30/00 , B82Y40/00 , C01B31/02
CPC分类号： B01J37/0221 , B01J19/088 , B01J23/74 , B01J23/745 , B01J23/75 , B01J23/755 , B01J23/881 , B01J23/882 , B01J23/883 , B01J35/002 , B01J35/006 , B01J37/0201 , B01J37/0205 , B01J37/0238 , B01J37/024 , B01J37/0244 , B01J37/08 , B01J37/12 , B01J37/18 , B01J37/349 , B82Y30/00 , B82Y40/00 , C01B32/162
摘要： A first layer of a catalyst material is formed on a substrate and heat treated to form a first plurality of nanoparticles. A second layer of a catalyst material is then formed over the substrate and the first plurality of nanoparticles and heat treated to form a second plurality of nanoparticles. The first layer of nanoparticles is advantageously not affected by the deposition or heat treatment of the second layer of catalyst material, for example being pinned or immobilised, optionally by oxidation, before formation of the second layer.
摘要翻译：催化剂材料的第一层形成在基底上并被热处理以形成第一多个纳米颗粒。然后在衬底和第一多个纳米颗粒上形成第二层催化剂材料，并进行热处理以形成第二多个纳米颗粒。第一层纳米颗粒有利地不受第二层催化剂材料的沉积或热处理的影响，例如在形成第二层之前可任选地通过氧化被固定或固定。

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