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    • 6. 发明公开
    • Means for forming a hermetic seal between glass and metal
    • Verfahren zur Herstellung einer hermetischen Dichtung zwischen Glas und Metall。
    • EP0259008A1
    • 1988-03-09
    • EP87306818.3
    • 1987-07-31
    • The Harshaw Chemical Company
    • Utts, Bradley K.Tailor, Ramesh C.
    • C03C27/04
    • C03C27/04
    • A rugged scintillation detector uses a hermetically sealed window assembly welded or otherwise bonded to the detector housing. A method and apparatus useful in forming a reproducible hermetic seal between the glass (22) and an annular metal retaining ring (24) is described. The glass (22) and ring (24) are chosen so that the ring diameter is slightly larger than that of the glass at room temperature. A thin layer of frit (26, 28) at the interface ensures a very tight mechan­ical seal, and a surface layer of chromium oxide on the ring ensures a secure chemical bond. The assembly device uses pressure (36) and counterpressure (14) to uniformly and reproducibly assemble the glass window into the retainer ring at elevated temperatures.
    • 坚固的闪烁检测器使用焊接或以其他方式结合到检测器壳体的气密密封窗组件。 描述了可用于在玻璃(22)和环形金属保持环(24)之间形成可再现气密密封的方法和装置。 选择玻璃(22)和环(24)使得环直径在​​室温下稍大于玻璃的直径。 在界面处的薄层玻璃料(26,28)确保非常紧密的机械密封,并且环上的氧化铬表面层确保了牢固的化学键。 组装装置使用压力(36)和反压力(14)在升高的温度下将玻璃窗均匀且可重复地组装到保持环中。
    • 8. 发明公开
    • Alumina-titania composition
    • Aluminiumoxid-Titanoxid-Zusammenstellung。
    • EP0339640A1
    • 1989-11-02
    • EP89107646.5
    • 1989-04-27
    • The Harshaw Chemical Company
    • Rigge, Ronald J.Belding, William A.Graham, James R.Yanik, Steve J.
    • B01J21/06B01D53/36
    • B01J21/063B01D53/8603
    • An alumina-titania composite, suitable for catalysts and catalyst supports, is made by controlled coprecipitation of the alumina and titania constituents of the composite. The composite contains from about 0.5% up to about 50% by weight titania (based on the total weight of the composite). The titania content of the composite, due to the controlled precipitation, is distributed throughout the composite in such a uniform manner that the average size of the titania particles is below about 50 angstroms and the individual titania particles cannot be observed by X-ray diffraction examination of the calcined composite. Due to the uniform distribution of the titania content in the composite, the composite exhibits significantly improved catalytic properties in comparison to conventionally prepared alumina-titania compounds.
    • 适用于催化剂和催化剂载体的氧化铝 - 二氧化钛复合材料通过复合材料的氧化铝和二氧化钛组分的可控共沉淀制备。 复合材料含有约0.5重量%至约50重量%的二氧化钛(基于复合材料的总重量)。 由于受控的沉淀,复合材料的二氧化钛含量以均匀的方式分布在整个复合材料中,使得二氧化钛颗粒的平均尺寸低于约50埃,并且通过X射线衍射检查不能观察到单独的二氧化钛颗粒 的煅烧复合材料。 由于复合材料中二氧化钛含量的均匀分布,与常规制备的氧化铝 - 二氧化钛化合物相比,复合材料显示出显着改善的催化性能。