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1. 发明授权

US06941676B2 Apparatus for freeze-drying foodstuffs and medicaments 有权
标题翻译：用于冷冻食品和药物的设备
公开(公告)号：US06941676B2
公开(公告)日：2005-09-13
申请号：US10035421
申请日：2002-01-04
申请人： Hiromichi Akimoto , Ryoji Sunama
发明人： Hiromichi Akimoto , Ryoji Sunama
IPC分类号： A23L3/44 , A61J3/00 , F26B5/06 , F26B17/12
CPC分类号： F26B5/065 , F26B5/06
摘要： Disclosed is a freeze-drying apparatus for foodstuffs, medicaments, etc., wherein liquid material is directly and distributively poured into upright cylindrical tubes, then, in its isolated state from external atmosphere for perfect sterilization, the liquid material is frozen with uniform thickness onto inner wall surface of the tubes, with further possibility of uniform heating of the freeze-dried layer. The main body of this apparatus is constructed with upright cylindrical tubes for freezing liquid material onto inner surface of tubes and jackets to surround the outer periphery of each of the tubes in a substantially concentric cylindrical shape, within which to circulate heat medium; then, a duct communicating to the vacuum exhaust system is connected to the upper end side of these tubes, while, a recovery chamber provided with valve is connected to the lower end side of tubes; and an inlet port is defined for feeding liquid material into inner cavity of tubes.
摘要翻译：公开了一种用于食品，药物等的冷冻干燥装置，其中将液体材料直接并分配地倒入直立的圆柱形管中，然后在与外部气氛隔离的状态下完全灭菌，将液体材料以均匀的厚度冷冻至管的内壁表面，进一步有可能使冷冻干燥层均匀加热。该装置的主体由直立的圆柱形管构成，用于将液体材料冷冻到管和夹套的内表面上，以围绕每个管的外周围大致同心圆柱形，在其中循环热介质; 然后，与真空排气系统连通的管道连接到这些管的上端侧，而具有阀的回收室连接到管的下端侧; 并且限定了用于将液体材料供给到管的内腔中的入口。

2. 发明申请

US20020189127A1 Apparatus for freeze-drying foodstuffs, medicaments, and so forth 有权
标题翻译：用于冷冻食品，药物等的装置
公开(公告)号：US20020189127A1
公开(公告)日：2002-12-19
申请号：US10035421
申请日：2002-01-04
申请人： KYOWA VACUUM ENGINEERING CO., LTD.
发明人： Hiromichi Akimoto , Ryoji Sunama
IPC分类号： F26B013/30 , F26B019/00 , F26B025/06 , F26B005/06
CPC分类号： F26B5/065 , F26B5/06
摘要： By directly distributing liquid material into upright cylindrical tubes, such liquid material for foodstuffs, medicaments, etc. is kept in its state of being isolated from external atmosphere so as to be perfectly sterilized. That is to say, while simply and adequately securing the controlled cooling of the tube, by means of the heat medium which circulates within the jacket, the liquid material supplied into the tube is caused to freeze with uniform thickness onto the inner wall surface of the tube, with further possibility of uniform heating of the freeze-dried layer. The main body part of this freeze-drying apparatus is assembled with upright cylindrical tubes for freezing liquid material onto the inner wall surface of the tube and jackets to surround the outer periphery of each of the tubes surrounding the tubes in a substantially concentric outer cylindrical shape, within which to circulate the heat medium; then, on the upper end side of these tubes in this main body part, there is connected a duct which communicates to the vacuum exhaust system; while, on the lower end side of the tubes, there is connected a recovery chamber provided with an opening-and-closing valve, or equipped with a valve on the bottom part thereof; and, on the upper part of the lower part of the tube, there is defined an inlet port, through which the liquid material is fed into the inner cavity of the tube, the inlet port being formed contiguous to the downstream side of the tube-passageway for feeding the liquid material.
摘要翻译：通过将液体材料直接分配到直立的圆柱形管中，用于食品，药物等的这种液体材料保持与外部气氛隔离的状态，从而被完全消毒。也就是说，虽然通过在套管内循环的热介质简单且充分地确保管的受控制冷却，使供给到管中的液体材料以均匀的厚度冷冻到内壁表面上具有进一步的冷冻干燥层加热的可能性。该冷冻干燥装置的主体部分组装有直立的圆柱形管，用于将液体材料冷冻到管的内壁表面和夹套上，围绕围绕管的每个管的外围以基本同心的外圆柱形状，在其内循环热介质; 然后，在该主体部分的这些管的上端侧，连接有与真空排气系统连通的管道; 而在管的下端侧，连接有设置有开关阀的回收室，或者在其底部配备有阀; 并且在管的下部的上部限定有入口，液体材料通过该入口进入管的内腔中，入口端口邻近管状管的下游侧形成，用于供给液体材料的通道。

3. 发明申请

US20030006326A1 Device for pulverizing desiccated bulk product in a freeze-drying apparatus for foodstuffs, medicaments, and so forth 有权
标题翻译：在用于食品，药物等的冷冻干燥装置中粉碎干燥散装产品的装置
公开(公告)号：US20030006326A1
公开(公告)日：2003-01-09
申请号：US10091118
申请日：2002-03-06
申请人： Kyowa Vacuum Engineering Co. Ltd.
发明人： Masahiro Inoki , Tsunehiro Yoshidomi
IPC分类号： B02C019/00
CPC分类号： F26B5/06 , F26B5/065
摘要： Desiccated bulk of liquid material, which has completed its freezing and desiccation in a freeze-drying apparatus, is subjected to pulverization within the machine body of a freeze-drying apparatus. According to the present invention, liquid material is caused to freeze as a molded frozen body in the form of a cylinder following the shape of the inner wall surface of the tube; then, the water content in the material of the molded frozen body is sublimated under the vacuum condition, to cause it to dry in a freeze-drying apparatus, wherein a discharge port is defined at the lower end side of the tube, and jet nozzles are disposed, in the inner wall surface of the tube, for ejecting compressed air or gas toward the inner bore or space of the tube, thereby crushing and pulverizing the molded frozen body of liquid material as freeze-dried by freezing the liquid material within the tube, by jet current ejected from the jet nozzles.
摘要翻译：在冷冻干燥装置中完成冷冻干燥的液体材料的干燥体在冷冻干燥装置的机体内进行粉碎。根据本发明，使液体材料以与管的内壁表面的形状相对应的圆筒形式作为模制的冷冻体冷冻; 然后，在真空条件下将成型的冷冻体的材料中的水分升华，使其在冷冻干燥装置中干燥，其中在管的下端侧限定排出口，并且喷嘴设置在管的内壁表面中，用于将压缩空气或气体朝向管的内孔或空间排出，从而通过将液体材料冷冻干燥而将冷冻干燥的模制冷冻体粉碎并粉碎，通过从喷嘴喷射的喷射流。

4. 发明申请

US20020189126A1 Distributive ejection device for liquid material to be used in freeze-drying apparatus for foodstuffs, medicaments, and so on 有权
标题翻译：用于食品，药品等的冷冻干燥装置中的液体材料的分配喷射装置
公开(公告)号：US20020189126A1
公开(公告)日：2002-12-19
申请号：US10035307
申请日：2002-01-04
申请人： KYOWA VACUUM ENGINEERING CO. LTD.
发明人： Hiromichi Akimoto , Ryoji Sunama
IPC分类号： F26B013/30
CPC分类号： F26B5/06 , F26B5/065
摘要： This invention is concerned with a distributive ejection apparatus for liquid material in a freeze-drying apparatus for foodstuffs, medicaments, etc., wherein the liquid material adjusted from the starting material for foodstuffs, medicaments, etc. is caused to freeze onto the inner wall surface of the upright cylindrical tube, and the distributive ejection of the liquid material onto the tube at the time of its freeze-drying by sublimation of the moisture content in the material under the vacuum condition may be done in the state of supplying the liquid material over the entire surface of the inner wall surface of the tube with a substantially uniform thickness. A cylindrical wall a protruding upwardly of the jacket 2 for circulation of heat medium, provided on the outer periphery of the tube 1, is disposed on the upper end side of the upright cylindrical tube equipped on a freeze-drying apparatus w, in the form of extending the peripheral wall of the tube 1; then, onto this inner wall surface of this cylindrical wall, the liquid material is ejected from the distributive ejection nozzles 70 equipped on the downstream side of the tube passageway 5 for feeding the liquid material is sputtered, and the thus ejected liquid material is rendered uniform in the circumferential direction on and along the inner wall surface of the cylindrical wall a, and, while it flows down, in this state, on the inner surface of the cylindrical wall a, it is made to flow onto the inner wall surface 1a of the tube 1 which constitutes the freezing surface of the liquid material.
摘要翻译：本发明涉及用于食品，药物等的冷冻干燥装置中的液体材料的分配喷射装置，其中使从食品原料，药物等调节的液体材料冷冻到内壁上直立圆柱形管的表面，以及在真空条件下材料中的水分含量的升华使其冷冻干燥时液体材料分布喷射到管上，可以在供给液体材料的状态下进行在管的内壁表面的整个表面上具有基本均匀的厚度。设置在管1的外周上的用于循环热介质的护套2向上突出的圆柱形壁设置在装备有冷冻干燥装置w的形式的冷冻干燥装置w的直立圆筒管的上端侧延伸管1的周壁; 然后，在该圆筒壁的内壁面上，从配置在管路5下游侧的分配喷嘴70喷出液体材料，供给液体材料进行溅射，使喷出的液体材料均匀在圆筒壁壁a的内壁面上并沿着圆周方向的圆周方向，在该状态下，在该状态下，在圆筒壁a的内表面上流动到内壁面1a 构成液体材料的冷冻表面的管1。

5. 发明授权

EP1584879B1 Device for pulverising desiccated bulk product in a freeze-drying apparatus for foodstuffs, medicaments, and so forth 有权
标题翻译：一种用于在冷冻干燥装置粉碎干燥散装材料用于食品，药物等的装置
公开(公告)号：EP1584879B1
公开(公告)日：2016-06-01
申请号：EP05015511.8
申请日：2002-02-22
申请人： Kyowa Vacuum Engineering Co., Ltd. , Hosokawa Micron Co.,Ltd.
发明人： Inoki, Masahiro , Yoshidomi, Tsunehiro
IPC分类号： F26B5/06
CPC分类号： F26B5/06 , F26B5/065

6. 发明公开

EP1584879A2 Device for pulverising desiccated bulk product in a freeze-drying apparatus for foodstuffs, medicaments, and so forth 有权
标题翻译：一种用于在冷冻干燥装置粉碎干燥散装材料用于食品，药物等的装置
公开(公告)号：EP1584879A2
公开(公告)日：2005-10-12
申请号：EP05015511.8
申请日：2002-02-22
申请人： Kyowa Vacuum Engineering Co., Ltd. , Hosokawa Micron Co.,Ltd.
发明人： Inoki, Masahiro , Yoshidomi, Tsunehiro
IPC分类号： F26B5/06
CPC分类号： F26B5/06 , F26B5/065
摘要： Desiccated bulk of liquid material, which has completed its freezing and desiccation in a freeze-drying apparatus (W), is subjected to pulverization within the machine body of a freeze-drying apparatus (W).
According to the present invention, liquid material is caused to freeze as a molded frozen body (M) in the form of a cylinder following the shape of the inner wall surface (1a) of a tube (1); then, the water content in the material of the molded frozen body (M) is sublimated under the vacuum condition, to cause it to dry in a freeze-drying apparatus (W), wherein a discharge port (d) is defined at the lower end side of the tube (1), and jet nozzles (N) are disposed, in the inner wall surface (1a) of the tube (1), for ejecting compressed air or gas toward the inner bore or space of the tube (1), thereby crushing and pulverizing the molded frozen body (M) of liquid material as freeze-dried by freezing the liquid material within the tube (1), by jet current ejected from the jet nozzles (N).
摘要翻译：液体物质，其已经完成了其在冷冻干燥装置（W）冷冻和干燥的干燥的散装，进行粉碎的冷冻干燥装置的机体内（W）。。根据本发明，液体材料被导致冻结如在圆柱体的形式的模制冷冻体（M）按照在管的内壁表面（1a）的形状（1）; 然后，在模制的冷冻体（M）的材料中的水含量是在真空条件下升华，以使其在冷冻干燥装置（W）干燥，worin的排出口（D）在所述下被定义所述管（1），和喷嘴（N）的端侧在管（1）的内壁面（1A），其设置用于喷射压缩空气或气体朝向管的内孔或空间（1 ），从而破碎和粉碎液体材料的模制的冷冻体（M），为冷冻干燥通过冷冻管（1）内的液体材料，通过从喷嘴（N）喷射射流。

7. 发明公开

EP1336427A1 Method and apparatus for preparing slurry from starting materials 审中-公开
标题翻译： Verfahren und Vorrichtung zur Erzeugung einer暂停aus Ausgangsstoffen
公开(公告)号：EP1336427A1
公开(公告)日：2003-08-20
申请号：EP02251078.8
申请日：2002-02-18
申请人： Kyowa Vacuum Engineering Co., Ltd.
发明人： Akimoto, Hiromiti , Sunama, Ryouji
IPC分类号： B01F3/12 , B01F5/10 , B01F13/06 , B01F1/00 , B01F15/02
CPC分类号： B01F13/065 , B01F3/1207 , B01F3/1271 , B01F5/10 , B01F15/0202
摘要： The present invention is directed to a starting material adjusting apparatus for preparing the starting materials in the form of slurry, wherein no use is made of an agitator which is expensive in its installation cost and troublesome in its cleaning, thereby making it possible to perfectly dissolve the starting materials into solvent, and to obtain homogeneous slurry as a whole, in a short period of time.
The construction and function of such starting material adjusting apparatus are as follows: a material blending tank 1 is formed in a pressure-resistant, and tightly closable vessel, in its inner cavity, into which predetermined quantities of starting materials are charged, followed by hermetically sealing the tank; a material adjusting tank 2 is formed in a large size, into which a predetermined quantity of solvent is filled so as to be able to pump out from its bottom part by means of a pump P; the pump P functioning to pressure-feeding the solvent pumped out of the material adjusting tank 2 into the inner cavity of the material blending tank 1 through its bottom side. In the course of the pressure-feeding of the solvent, when the air within the material blending tank 1 is compressed to a high pressure level, the operation of the pump P is stopped and the solvent which has been pressure-fed into the material blending tank 1 is subjected to reverse flow through the inner cavity of the pump P into the material adjusting tank 2 by the pressure of the air compressed in the material blending tank 1. Subsequently, the process steps of: the pressure-feeding of the solvent into the material blending tank 1 due to re-starting of the pump P; and the reverse flow of the solvent into the material adjusting tank 2 due to stoppage of the pump P are repeated for a plurality of number of times to dissolve the starting materials into the solvent, thereby making it into slurry.
摘要翻译：本发明涉及一种用于制备浆料形式的起始材料的起始材料调节装置，其中没有使用其安装成本昂贵且其清洗麻烦的搅拌器，从而可以完全溶解将原料溶解成溶剂，并在短时间内获得均匀的浆料。这种起始材料调节装置的结构和功能如下：将材料混合罐1形成在其内腔中的耐压紧密封闭的容器中，其中装入预定量的原料，随后密封密封罐; 形成大尺寸的材料调节罐2，其中填充有预定量的溶剂，以便能够通过泵P从其底部泵出; 泵P用于将从材料调节罐2抽出的溶剂从其底侧向料料混合槽1的内腔进行加压。在溶剂的加压过程中，当将混合箱1内的空气压缩至高压水平时，停止泵P的运转，并将已经进料的溶剂进料到混合物罐1通过在料料1中压缩的空气的压力经过泵P的内腔反向流入材料调节罐2.随后，将溶剂压入由于泵P的重新启动，材料混合槽1; 并且由于泵P的停止而使溶剂进入材料调节罐2的反向流动多次，以将原料溶解到溶剂中，从而使其成为浆料。

8. 发明公开

EP1584879A3 Device for pulverising desiccated bulk product in a freeze-drying apparatus for foodstuffs, medicaments, and so forth 有权
标题翻译：一种用于在冷冻干燥装置粉碎干燥散装材料用于食品，药物等的装置
公开(公告)号：EP1584879A3
公开(公告)日：2012-08-29
申请号：EP05015511.8
申请日：2002-02-22
申请人： Kyowa Vacuum Engineering Co., Ltd. , Hosokawa Micron Co.,Ltd.
发明人： Inoki, Masahiro , Yoshidomi, Tsunehiro
IPC分类号： F26B5/06
CPC分类号： F26B5/06 , F26B5/065
摘要： Desiccated bulk of liquid material, which has completed its freezing and desiccation in a freeze-drying apparatus (W), is subjected to pulverization within the machine body of a freeze-drying apparatus (W).
According to the present invention, liquid material is caused to freeze as a molded frozen body (M) in the form of a cylinder following the shape of the inner wall surface (1a) of a tube (1); then, the water content in the material of the molded frozen body (M) is sublimated under the vacuum condition, to cause it to dry in a freeze-drying apparatus (W), wherein a discharge port (d) is defined at the lower end side of the tube (1), and jet nozzles (N) are disposed, in the inner wall surface (1a) of the tube (1), for ejecting compressed air or gas toward the inner bore or space of the tube (1), thereby crushing and pulverizing the molded frozen body (M) of liquid material as freeze-dried by freezing the liquid material within the tube (1), by jet current ejected from the jet nozzles (N).

9. 发明授权

EP1267138B1 Apparatus for freeze-drying foodstuffs, medicaments, and so forth 有权
标题翻译：一种用于食品，药品冷冻干燥等设备
公开(公告)号：EP1267138B1
公开(公告)日：2008-11-12
申请号：EP02251079.6
申请日：2002-02-18
申请人： Kyowa Vacuum Engineering Co., Ltd.
发明人： Akimoto, Hiromichi , Sunama, Ryoji
IPC分类号： F26B5/06
CPC分类号： F26B5/065 , F26B5/06

10. 发明公开

EP1273861A1 Device for pulverizing desiccated bulk product in a freeze-drying apparatus for foodstuffs, medicaments, and so forth 有权
标题翻译： GefriertrocknungsvorrichtungfürNahrungsmittel und Arzneimittel
公开(公告)号：EP1273861A1
公开(公告)日：2003-01-08
申请号：EP02251243.8
申请日：2002-02-22
申请人： Kyowa Vacuum Engineering Co., Ltd. , Hosokawa Micron Co.,Ltd.
发明人： Inoki, Masahiro , Yoshidomi, Tsunehiro
IPC分类号： F26B5/06
CPC分类号： F26B5/06 , F26B5/065
摘要： Desiccated bulk of liquid material, which has completed its freezing and desiccation in a freeze-drying apparatus, is subjected to pulverization within the machine body of a freeze-drying apparatus.
According to the present invention, liquid material is caused to freeze as a molded frozen body (M) in the form of a cylinder following the shape of the inner wall surface of the tube (1); then, the water content in the material of the molded frozen body (M) is sublimated under the vacuum condition, to cause it to dry in a freeze-drying apparatus (W), wherein a discharge port (d) is defined at the lower end side of the tube (1), and jet nozzles (N) are disposed, in the inner wall surface of the tube, for ejecting compressed air or gas toward the inner bore or space of the tube, thereby crushing and pulverizing the molded frozen body (M) of liquid material as freeze-dried by freezing the liquid material within the tube (1), by jet current ejected from the jet nozzles (N).
摘要翻译：在冷冻干燥装置中完成冷冻干燥的液体材料的干燥体积在冷冻干燥装置的机体内进行粉碎。根据本发明，使液体材料作为与管（1）的内壁表面形状的圆筒形式的模制冷冻体（M）冷冻; 然后将成型的冷冻体（M）的材料中的水分在真空条件下升华，使其在冷冻干燥装置（W）中干燥，其中排出口（d）定义在下部管（1）的端侧，喷管（N）设置在管的内壁表面，用于将压缩空气或气体朝向管的内孔或空间排出，从而粉碎和粉碎模制的冷冻通过从喷嘴（N）喷射的喷射流冷冻管（1）内的液体材料而使液体材料的体（M）冷冻干燥。

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