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1. 发明专利

MY7100058A BENZENESULPHONYL-UREAS AND PROCESS FOR THEIR MANUFACTURE 未知
公开(公告)号：MY7100058A
公开(公告)日：1971-12-31
申请号：MY7100058
申请日：1971-12-31
申请人： FARBWERKE HOESCHST AKTIENGESELLSCHAFT
IPC分类号： A61K31/64 , C07D309/14
摘要： 1,171,935. Benzenesulphonyl ureas. FARBWERKE HOECHST A.G. 1 Dec., 1966 [2 Dec., 1965], No. 53773/66. Heading C2C. The invention comprises compounds of formula wherein R is H, C 1-4 alkyl or phenyl-C 1-4 . alkyl; R 1 is a C 2-8 alkyl, alkenyl or mercaptoalkyl group, a C 4-8 alkoxyalkyl, alkylmercaptoalkyl or alkylsulphinylalkyl group containing at least 2 carbon atoms in the alkylene part, phenyl - C 1-4 - alkyl, phenylcyclopropyl, cyclohexyl - C 1-4 - alkyl, cycloheptylmethyl, cycloheptylethyl, cyclooctylmethyl, an endoalkylenecyclohexyl, -cyclohexenyl, -cyclohexylmethyl or cyclohexenylmethyl group containing 1 or 2 carbon atoms in the endoalkylene part, (C 1-4 alkyl)-cyclohexyl, (C 1-4 alkoxy)-cyclohexyl, C 5-8 cycloalkyl, cyclohexenyl, cyclohexenylmethyl, or a C 4-5 O or C 4-5 S heterocyclic ring optionally containing 1 or 2 ethylenic double bonds and connected to the nitrogen atom either directly or via a CH 2 group: Y is a C 1-4 hydrocarbon chain; Z is C 5-6 aliphatic hydrocarbyl, or a phenyl group optionally substituted by a member selected from C 1-4 alkyl, C 1-4 alkoxy, CF 3 , Cl, Br and F; X is H (provided that Z is optionally substituted phenyl), halogen, C 1-4 alkyl, C 1-4 alkoxy, CF 3 or NO 2 ; and wherein the "phenylene " group is optionally substituted by one or more members selected from C 1-4 alkyl, C 1-4 alkoxy and halogen; and the physiologically tolerable salts of such compounds. These compounds are prepared by (a) reacting R 1 NH 2 or a salt thereof with an appropriately substituted benzenesulphonyl-carbamic acid ester, - thiolcarbamic acid ester, -isocyanate, -urea, - semicarbazide, or -semicarbazone; or (b) reacting an R 1 -substituted isocyanate, carbamic acid ester, thiolcarbamic acid ester, carbamic acid halide or urea with an appropriately substituted benzenesulphonamide; or (c) hydrolysing a correspondingly substituted benzenesulphonyl-isourea ether, -isourea ester, -isothiourea ether, -parabanic acid or -haloformic acid amidine; or (d) hydration of a correspondingly substituted benzenesulphonyl-carbodiimide; or (e) replacing S by O in a correspondingly substituted benzenesulphonyl-thiourea; or (f) by acylating a compound of formula RNH.Y.phenylene.SO 2 .NH.CO.NH.R 1 . Variations of the above methods are also referred to. 4 - [#, - (2 - Phenoxy - benzamido) - ethyl]- benzene-sulphonamide is prepared by reacting 2- phenoxy-benzoyl chloride with 4-(#-aminoethyl)-benzenesulphonamide. N - {4 - [# - (2 - Phenoxy - benzamido) - ethyl]- benzenesulphonyl } - N 1 - cyclohexyl - thiourea is prepared by reacting 4-[#-(2-phenoxy-benzamido) - ethyl] - benzenesulphonamide with cyclohexyl isothiocyanate, and is convertible with mercuric oxide, methanol and K 2 CO 3 into the corresponding isourea methyl ether. N - {4 - [# - (2 - phenoxy - benzamido) - ethyl]- benzenesulphonyl} - urea is prepared by reacting 4 - [# - (2 - phenoxy - benzamido) - ethyl]- benzenesulphonamide with potassium cyanate. N - {4 - [γ - (2 - chloro - 5 - nitro - benzamido)- propyl] - benzenesulphonyl} - N 1 - cyclohexylurea is prepared by reacting 2-chloro-5-nitrobenzoyl chloride with N-[4-(γ-amino-propyl)- benzenesulphonyl} - N 1 - cyclohexyl - urea, the last-named compound being in turn prepared by hydrolysis of the corresponding γ-acetamidopropyl compound. N - {4 - [# - (2 - phenoxy - benzamido)- ethyl] - benzenesulphonyl} - N 1 - (2,5 - endomethylene - cyclohexyl - methyl) - thiourea is prepared by reacting 4 - [# - (2 - phenoxybenzamido) - ethyl] - benzenesulphonamide with 2,5 - endomethylene - cyclohexyl - methyl isothiocyanate. N - {4 - [# - (2 - phenoxy - benzamido) - ethyl]- benzenesulphonyl} - N 1 - cyclohexyl - isothiourea methyl ether is prepared from the corresponding thiourea by reaction with methyl iodide. The benzenesulphonyl-ureas of the invention and their physiologically tolerable salts are stated to possess hypoglemic action and may be made up with carriers into pharmaceutical compositions suitable for oral administration. The salts may be alkali metal or alkaline earth metal salts.

2. 发明授权

US5994438A Pulverulent adhesive composition 失效
标题翻译：粉煤灰组合物
公开(公告)号：US5994438A
公开(公告)日：1999-11-30
申请号：US825951
申请日：1997-04-03
申请人： Ulrich Geissler , Helmut Hintz , Ulrike Vogt-Saggau
发明人： Ulrich Geissler , Helmut Hintz , Ulrike Vogt-Saggau
IPC分类号： C08G8/34 , C09J125/14 , C09J131/02 , C09J133/04 , C09J133/06 , C08L93/04 , C08L45/00 , C08L33/10 , C09J193/04
CPC分类号： C09J131/02 , C09J125/14 , C09J133/06
摘要： A pulverulent adhesive composition which comprises (a) at least one polymer selected from the group consisting of vinyl ester polymers, (meth)acrylate polymers and styrene(meth)acrylate polymers, (b) at least one tackifying resin (tackifier) and, optionally, (c) one or more protective colloids, and, optionally, (d) one or more anticaking agents. The present composition is suitable for use in formulations used for the adhesive bonding of porous and/or semiporous substrates.
摘要翻译：一种粉状粘合剂组合物，其包含（a）至少一种选自乙烯基酯聚合物，（甲基）丙烯酸酯聚合物和苯乙烯（甲基）丙烯酸酯聚合物的聚合物，（b）至少一种增粘树脂（增粘剂）和任选地，（c）一种或多种保护性胶体，和（d）一种或多种防结块剂。本发明的组合物适合用于多孔和/或半孔基材的粘合剂的制剂中。

3. 发明授权

US4029565A Electrolytic apparatus 失效
标题翻译：电解设备
公开(公告)号：US4029565A
公开(公告)日：1977-06-14
申请号：US718341
申请日：1976-08-27
申请人： Werner Bender , Dieter Bergner , Kurt Hannesen , Helmut Hund , Wilfried Schulte
发明人： Werner Bender , Dieter Bergner , Kurt Hannesen , Helmut Hund , Wilfried Schulte
IPC分类号： C25B9/00 , C25B9/08 , C25B9/18 , C25B9/20 , C25B1/26
CPC分类号： C25B9/20
摘要： In an electrolytic apparatus for the production of chlorine from aqueous alkali metal chloride solution, comprising at least one electrolytic cell with equipment for the supply of the current, the supply of the starting product and the discharge of the products of electrolysis and a separating wall for separating the anode and cathode, the housing of the cell is composed of two hemispherical shells, the electrodes are connected with the hemispherical shells by conductive bolts projecting through the wall of the shells and the projecting end faces of the bolts are in contact with current supply means and means to clamp together the supply means, the shells, the electrodes and the separating wall, which wall is positioned between electrically insulating spacers mounted in the extension of the bolts on the electrolytically active side of the electrodes and clamped between the edges of the hemispherical shells by packing elements.
摘要翻译：在用于从碱金属氯化物水溶液中生产氯的电解设备中，包括至少一个电解池，其具有用于供应电流的设备，起始产物的供应和电解产物的排放以及用于分离阳极和阴极，电池的壳体由两个半球形壳体组成，电极通过穿过壳体的壁突出的导电螺栓与半球形壳体连接，并且螺栓的突出端面与电流供应用于将供应装置，壳体，电极和分隔壁夹紧在一起的装置和装置，该壁被安置在电极的电解活性侧的螺栓的延伸部分中的电绝缘间隔件之间并夹在通过包装元件的半球形壳。

4. 发明授权

US5374184A Photopolymerizable material and process for the production of a colored image 失效
标题翻译：可光聚合材料和生产彩色图像的方法
公开(公告)号：US5374184A
公开(公告)日：1994-12-20
申请号：US222393
申请日：1994-04-04
申请人： Stephan J. W. Platzer , Gerhard Buhr , Manfred Michel , Andrea Buchmann
发明人： Stephan J. W. Platzer , Gerhard Buhr , Manfred Michel , Andrea Buchmann
IPC分类号： G03F3/10 , G03F7/004 , G03F7/027 , G03F7/028 , G03F7/105 , G03F7/11 , G03F7/34 , G03C11/12
CPC分类号： G03F3/106 , G03F7/34
摘要： A photopolymerizable material having(A) a flexible, transparent film support;(B) a colored, polymerizable layer containing an organic binder, a free-radical-polymerizable compound, containing at least one terminal ethylenically unsaturated group, and a dye or colored pigment;(C) an adhesion layer containing a thermoplastic polymer and having a T.sub.g of from 25.degree. to 100.degree. C.; and(D) an uncolored photopolymerizable layer which contains a polymeric organic binder, a free-radical-polymerizable compound containing at least one terminal ethylenically unsaturated group and a photopolymerization initiator between the film support (A) and the colored polymerizable layer (B),where the cohesion of layers (B), (C) and (D) and the adhesion of these layers to one another and to the film support (A) provides the relationship wherein the adhesion (a.sub.2) of the photopolymerizable layer (D) to the colored layer (B) in the unexposed state is lower than: (i) the adhesion (a.sub.3) of the colored layer (B) to the adhesion layer (C); (ii) the adhesion (a.sub.1) of the photopolymerizable layer (D) to the film support (A); and (iii) the cohesion (c.sub.1), (c.sub.2) and (c.sub.3) of layers (D), (B) and (C) and the adhesion (a.sub.3 ') of the colored layer (B) to the adhesion layer (C) in the exposed state is lower than: (i) the adhesion (a.sub.1 ') of the photopolymerized layer (D) to the film support (A); (ii) the adhesion (a.sub.2 ') of the photopolymerized layer (D) to the colored layer (B); and (iii) than the cohesion (c.sub.1 '), (c.sub.2 ') and (c.sub.3 ') of layers (D) , (B) and (C). The material is processed by "peel-apart" development and yields color images with lower background discoloration.
摘要翻译：一种可光聚合材料，其具有（A）柔性透明膜载体; （B）含有有机粘合剂，含有至少一个末端烯属不饱和基团的自由基聚合性化合物和染料或着色颜料的着色聚合层; （C）含有热塑性聚合物的Tg为25〜100℃的粘合层。和（D）含有聚合有机粘合剂，含有至少一个末端烯属不饱和基团的自由基聚合性化合物和薄膜载体（A）和着色聚合层（B）之间的光聚合引发剂的未着色光聚合层，其中层（B），（C）和（D）的内聚力以及这些层彼此和膜载体（A）的粘附性提供了这样的关系，其中可光聚合层（D）的粘合力（a2）未曝光状态下的着色层（B）低于（i）着色层（B）对粘合层（C）的粘合力（a3）。（ii）可光聚合层（D）与膜载体（A）的粘合（a1）; 和（iii）层（D），（B）和（C）的层压（c1），（c2）和（c3）和着色层（B）对粘合层（C ）低于（i）光聚合层（D）与膜载体（A）的粘合力（a1'）; （ii）光聚合层（D）与着色层（B）的粘合（a2'）; 和（iii）层（D），（B）和（C）的内聚力（c1'），（c2'）和（c3'）。通过“剥离”开发处理材料，并产生具有较低背景变色的彩色图像。

5. 发明授权

US06159539A Process for preparing organically modified aerogels and use thereof 失效
标题翻译：制备有机改性气凝胶的方法及其用途
公开(公告)号：US06159539A
公开(公告)日：2000-12-12
申请号：US981802
申请日：1998-01-08
申请人： Fritz Schwertfeger , Andreas Zimmermann
发明人： Fritz Schwertfeger , Andreas Zimmermann
IPC分类号： C01B33/16 , C07F7/10 , C08G77/02 , B01D7/00 , B01J12/00 , B32B21/02 , C01B33/12
CPC分类号： C07F7/10 , Y10T428/2995
摘要： The inventive process concerns the preparation of organically modified aerogels and their use.The process the invention comprises:a) introducing a siliceous lyogel or hydrogel,b) optionally subjecting the gel prepared in a) to complete or partial solvent exchange with an organic solvent,c) reacting the gel obtained in step a) or b) with at least one silylation agent,d) optionally washing the silylated gel obtained in step c) with an organic solvent, ande) drying the gel obtained in step c) or d) subcritically, which comprises reacting in step c) the gel obtained in step a) or b) with at least one chlorine-free silylation agent.
摘要翻译： PCT No.PCT / EP96 / 02894 Sec。 371日期1998年1月8日 102（e）1998年1月8日PCT PCT 1996年7月2日PCT公布。公开号WO97 / 03017 日期1997年1月30日本发明方法涉及有机改性气凝胶的制备及其用途。本发明的方法包括：a）引入硅质溶胶凝胶或水凝胶，b）任选地使a）中制备的凝胶与有机溶剂进行完全或部分溶剂交换，c）将步骤a）或b）中获得的凝胶与至少一种甲硅烷基化剂，d）任选地用有机溶剂洗涤在步骤c）中获得的甲硅烷基化凝胶，以及e）将步骤c）中得到的凝胶干燥或d）亚临界地干燥，其包括在步骤c）步骤a）或b）与至少一种无氯甲硅烷化剂反应。

6. 发明授权

US4885383A Process for the preparation of carboxylic acid methyl esters 失效
标题翻译：羧酸甲酯的制备方法
公开(公告)号：US4885383A
公开(公告)日：1989-12-05
申请号：US248544
申请日：1988-09-23
申请人： Jurgen Weber , Helmut Springer , Peter Lappe
发明人： Jurgen Weber , Helmut Springer , Peter Lappe
IPC分类号： C07B61/00 , B01J27/02 , C07C67/08 , C07C69/003
CPC分类号： C07C67/08 , C07C2101/14
摘要： A process for the preparation of methyl carboxylates by the reaction of mono or dicarboxylic acids having more than 5 carbon atoms and methanol in the presence of acidic catalysts at temperatures from 100.degree. to 150.degree. C. and below the boiling point of the carboxylates being produced.
摘要翻译：在酸性催化剂存在下，在100-150℃的温度和低于所生产的羧酸盐的沸点下，通过使具有多于5个碳原子的一元或二元酸与甲醇反应制备甲基羧酸酯的方法。

7. 发明授权

US5965744A Ortho-substituted benzoylguanidines, including composition and methods of using them 失效
标题翻译：正构取代的苯甲酰胍，包括使用它们的组合物和方法
公开(公告)号：US5965744A
公开(公告)日：1999-10-12
申请号：US805321
申请日：1997-02-24
申请人： Andreas Weichert , Hans-Jochen Lang , Heinz-Werner Kleemann , Jan-Robert Schwark , Wolfgang Scholz , Udo Albus
发明人： Andreas Weichert , Hans-Jochen Lang , Heinz-Werner Kleemann , Jan-Robert Schwark , Wolfgang Scholz , Udo Albus
IPC分类号： A61K31/155 , A61K31/4164 , A61P9/00 , A61P9/06 , A61P9/08 , A61P9/10 , A61P13/02 , A61P15/00 , A61P25/00 , A61P43/00 , C07C233/78 , C07C235/50 , C07C237/34 , C07C279/22 , C07C323/60 , C07D233/54 , C07D233/60 , C07D233/61 , A61K31/495 , C07C277/08 , C07D401/14 , C07D403/12
CPC分类号： C07D233/64 , C07C279/22
摘要： The present invention relates to ortho-substituted benzoylguanidines of the formula I, defined in the specification. The invention also embraces processes for making these compounds, as well as compositions and methods of using them. The compounds of the invention exhibit very good antiarrhythmic properties, making them useful in treating or preventing infarction, angina pectoris, and pathophysiological processes associated with ischemically induced damage.
摘要翻译：本发明涉及在说明书中定义的式I的邻位取代的苯甲酰胍基。本发明还包括制备这些化合物的方法，以及使用它们的组合物和方法。本发明的化合物表现出非常好的抗心律失常性质，使其可用于治疗或预防与缺血诱导的损伤相关的梗死，心绞痛和病理生理过程。

8. 发明授权

US5296355A Method for assaying immunologically active substance and reagent therefor 失效
标题翻译：用于测定免疫活性物质及其试剂的方法
公开(公告)号：US5296355A
公开(公告)日：1994-03-22
申请号：US678326
申请日：1991-06-12
申请人： Shoichi Shutoh , Akinori Suginaka , Mikio Akita
发明人： Shoichi Shutoh , Akinori Suginaka , Mikio Akita
IPC分类号： C08L71/00 , C08L71/02 , G01N33/53 , G01N33/531 , G01N33/543 , G01N33/536
CPC分类号： G01N33/53 , G01N33/5306 , G01N33/531 , G01N33/54393 , Y10S435/962 , Y10S436/826
摘要： A method for assaying an immunologically active substance based on the antigen-antibody reaction in a liquid phase, and a reagent for use in the method are disclosed. This method comprises adding a reagent containing a compound represented by the general formulaR.sup.1 O---[(CH.sub.2 CH.sub.2 O).sub.m (AO).sub.n ]--R.sup.2(wherein R.sup.1 and R.sup.2 each represents a hydrogen atom or a hydrocarbyl group containing 1 to 5 carbon atoms, AO represents an oxyalkylene group containing 3 to 4 carbon atoms, m and n represent the number of oxyethylene groups and that of oxyalkylene groups, respectively, with said oxyethylene groups and oxyalkylene groups forming a random copolycondensate and having a molecular weight of 1000 to 20000, and the ratio of m/n being 60/40 to 90/10).
摘要翻译： PCT No.PCT / JP89 / 01051 Sec。 371日期1991年6月12日 102（e）日期1991年6月12日PCT提交1989年10月12日PCT公布。公开号WO90 / 04179 日本1990年04月19日。基于液相中的抗原 - 抗体反应测定免疫活性物质的方法和用于该方法的试剂。该方法包括加入含有通式R 1 -O - （（CH 2 CH 2 O）m（AO）n）-R 2（其中R 1和R 2各自表示氢原子或含有1至5个碳原子的烃基） AO表示含有3〜4个碳原子的氧化烯基，m和n分别表示氧化乙烯基和氧化烯基的数量，所述氧化乙烯基和氧化烯基形成无规共聚缩聚物，分子量为1000〜20000， m / n的比例为60/40〜90/10）。

9. 发明授权

US4825008A Acetylketene dialkyl acetals and a process for their preparation 失效
标题翻译：乙烯酮二烷基缩醛及其制备方法
公开(公告)号：US4825008A
公开(公告)日：1989-04-25
申请号：US138309
申请日：1987-12-28
申请人： Klaus Gunther , Gunter Mau
发明人： Klaus Gunther , Gunter Mau
IPC分类号： C07C45/64 , C07C45/71 , C07C45/82 , C07C49/255
CPC分类号： C07C49/255 , C07C45/71 , C07C45/82
摘要： The invention relates to a process for the preparation of acetylketene dialkyl acetals of the formula CH.sub.3 CO--CH.dbd.C(OR.sup.2).sub.2 in which R.sup.2 can be an alkyl radical with 1 to 12 carbon atoms, and also these compounds themselves, providing that R.sup.2 is an alkyl radical with 3 to 12 carbon atoms. In the preparation process an alkyl acetoacetate of the formula CH.sub.3 CO--CH.sub.2 COOR.sup.1 is reacted with a saturated primary or secondary alcohol R.sup.2 OH in the presence of an acid catalyst, in which R.sup.2 has the abovementioned meaning and in which R.sup.2 OH or is higher boiling than R.sup.1 OH.
摘要翻译：本发明涉及一种制备式CH3CO-CH = C（OR2）2的乙酰基乙烯基二烷基缩醛的方法，其中R 2可以是具有1至12个碳原子的烷基，以及这些化合物本身，其中R 2为具有3至12个碳原子的烷基。在制备方法中，在酸催化剂存在下，使式CH3CO-CH2COOR1的烷基乙酰乙酸酯与饱和的伯醇或仲醇ROHOH反应，其中R 2具有上述含义，并且其中R 2 OH或沸点高于R 1 OH。

10. 发明授权

US4725526A Process for reducing halations using lubricant in the course of irradiating and developing reproduction layers used for preparing printing plates 失效
标题翻译：在照射和显影用于制备印版的再生层的过程中减少使用润滑剂的方法
公开(公告)号：US4725526A
公开(公告)日：1988-02-16
申请号：US766691
申请日：1985-08-19
申请人： Werner Frass , Engelbert Pliefke
发明人： Werner Frass , Engelbert Pliefke
IPC分类号： G03C1/00 , G03F1/00 , G03F7/00 , G03F7/004 , G03F7/09 , G03F7/20 , G03F7/08 , G03F7/10
CPC分类号： G03F7/092 , Y10S430/151
摘要： In a process for reducing halations during the imagewise irradiation of a reproduction layer exposed through a planar image original, at least one lubricant either is contained in the layer or is interposed between the layer and the image original. Suitable lubricants include organic polysiloxanes, hydrocarbon polymers, polyaryl esters, and alkanoic acids or alkenoic acids having at least 9 carbon atoms. Excluded are lubricants comprising copolymers of dimethyl dichlorosilane, ethylene oxide and propylene oxide, provided they are located in the reproduction layer.
摘要翻译：在通过平面图像原稿暴露的再现层的成像照射期间减少晕影的过程中，至少一种润滑剂被包含在该层中或者介于该层与图像原件之间。合适的润滑剂包括具有至少9个碳原子的有机聚硅氧烷，烃聚合物，聚芳基酯和链烷酸或链烯酸。排除的是包含二甲基二氯硅烷，环氧乙烷和环氧丙烷的共聚物的润滑剂，只要它们位于再生层中。

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