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1. 发明专利

NL147801B 未知
公开(公告)号：NL147801B
公开(公告)日：1975-11-17
申请号：NL6405428
申请日：1964-05-15
申请人： DIAMOND ALKALI CO
IPC分类号： C07C37/14 , D06M15/37 , D06M15/53 , D06M13/18
摘要： Compounds suitable for use in the treatment of textile materials and polymeric sheet materials are produced by condensing an aromatic compound containing an aromatic moiety and an aromatic phenolic moiety having at least one phenolic hydroxy group, of which a -methyl benzyl para phenol a -methyl benzyl ortho phenol, ortho phenyl phenol, para phenyl phenol and 4-methyl-41-hydroxy diphenyl sulphone are specified, with 5-20 moles of ethylene oxide per phenolic hydroxy group contained within the compound. In Example I a -methyl benzyl para phenol is prepared by the reaction of phenol with styrene in the presence of a catalyst consisting of boron trifluoride and an aqueous solution of hypophosphorous acid, and is then condensed with 9 moles of ethylene oxide.ALSO:Compounds suitable for use in the treatment of textile materials and polymeric sheet materials are produced by condensing an aromatic compound containing an aromatic moiety and an aromatic phenolic moiety having at least one phenolic hydroxy group, of which a -methyl benzyl para phenol, a -methyl benzyl ortho phenol, ortho phenyl phenol, para phenyl phenol and 4-methyl-41-hydroxy diphenyl sulphone are specified, with 5-20 moles of ethylene oxide per phenolic hydroxy group contained within the compound. In Example XI, a resin mixture is prepared from polyvinyl chloride, di-2-ethyl hexyl phthalate, epoxidized soya bean oil, stearic acid, a barium octoate-zinc octoate stabilizer and a condensate of 1 mole of a -methyl benzyl ortho phenol with 9.1 moles of ethylene oxide and made into sheet material.ALSO:A catalytic composition comprises boron trifluoride and an aqueous solution of hypophosphorous acid.ALSO:Natural and synthetic textile materials in the form of fibre, continuous or spun yarns, filaments, rovings, slivers or tops are lubricated and rendered antistatic by treating them with a water-soluble compound produced by condensing an aromatic compound containing an aromatic moiety and an aromatic phenolic moiety having at least one phenolic hydroxy group with 5-20 moles of ethylene oxide per phenolic hydroxy group contained in the compound. The aromatic compound which is condensed with the ethylene oxide may be in which R is an aryl or substituted aryl radical containing 6-24 carbon atoms, e.g. phenyl. chlorophenyl, octyl phenyl, diphenyl, hydroxy benzyl, dioctyl-o-hydroxy benzyl or 2-hydroxy-3-(ortho hydroxy benzyl) phenyl, X is hydrogen, chlorine, bromine or a straight or branched chain alkyl radical containing 1-15 carbon atoms and R1 and R2 which may be the same or different are hydrogen or alkyl radicals containing 1-5 carbon atoms. The compounds may be applied to the textile materials from an aqueous solution or solution in an organic solvent, e.g. ether, methyl alcohol, ethyl alcohol or acetone, in an amount of from 0.01-1.3% by weight. Textile materials made from cellulose acetate, nylon, polyethylene terephthalate, acrylic, viscose rayon, polyvinylidene chloride, copolymers of acrylonitrile and polyvinyl alcohol, polyethylene, polypropylene, cotton, wool, linen, silk, casein or vicara fibres may be treated.

2. 发明专利

GB1182346A Improvements in or relating to Haloalkylated Polymers and the Preparation of Ion Exchange Resins Therefrom 未知
公开(公告)号：GB1182346A
公开(公告)日：1970-02-25
申请号：GB3292467
申请日：1967-07-18
申请人： DIAMOND ALKALI CO
发明人： BUFTON RICHARD GEORGE
IPC分类号： C08F8/24
摘要： 1,182,346. Haloalkylation of vinyl aromatic polymers. DIAMOND ALKALI CO. 18 July, 1967 [20 July, 1966], No. 32924/67. Heading C3P. A vinyl aromatic polymer, which may be cross-linked, is haloalkylated by reaction with a haloalkylation agent, e.g. methyl chloromethyl ether, in the presence of titanium tetrachloride or tetrabromide as a haloalkylation catalyst. The polymer may be polystyrene which may be cross-linked with divinyl benzene or by reaction with a halo-sulphonic acid/ aldehyde complex, e.g. a chloro-sulphonic acid/ para-formaldehyde complex. The haloalkylated polymer may be converted to an ion exchange resin by replacing the halogen atoms with quaternary ammonium, sulphonium, carboxylic acid or phosphonic acid groups, e.g. by treatment with trimethylamine, triethylphosphite with the phosphonium intermediate being hydrolysed, dimethyl sulphoxide and sodium cyanide followed by hydrolysis, or dimethyl sulphide.

3. 发明专利

DE1289942B 未知
公开(公告)号：DE1289942B
公开(公告)日：1969-02-27
申请号：DES0063727
申请日：1954-01-11
申请人： DIAMOND ALKALI CO
发明人： LUCIEN SELLET
IPC分类号： C14C9/00 , D06M15/423

4. 发明专利

GB1141386A Improvements in or relating to anion exchange resins 未知
公开(公告)号：GB1141386A
公开(公告)日：1969-01-29
申请号：GB4608566
申请日：1966-10-14
申请人： DIAMOND ALKALI CO
IPC分类号： C08F8/00 , C08F220/42 , C08F220/44
摘要： 1,141,386. ion exchange resins. DIAMOND ALKALI CO. 14 Oct., 1966 [18 Oct., 1965 (2)], No. 46085/66. Heading C3P. A weak-base anion exchange resin has (1) a cross-linked polymeric matrix obtained by copolymerizing a polymerizable unsaturated nitrile with a compound containing at least two polymerizable unsaturated groups, and (2) attached to the polymeric matrix, substituent anion-active radicals selected from wherein X is a divalent ortho aromatic radical, R 1 and R 2 are each a hydrogen atom or an alkyl, aminoalkyl or amino-aza-alkyl radical containing 2 to 12 carbon atoms and R 3 is a hydrogen atom or an alkyl radical containing 2 to 12 carbon atoms. The matrix is produced by copolymerization of acrylonitrile, methacrylonitrile or vinyl benzyl cyanide with divinyl benzene, divinyl toluene, trivinyl benzene or ethylene glycol dimethacrylate and optional additional monomers, e.g. ethyl vinyl benzene. The imidazole resins containing groups of Formula I are produced by reacting the matrix with an ortho-aromatic diamine such as ophenylene diamine or 2,3-naphthylene diamine. The imide resins containing groups of Formula II are formed by hydrolysing the matrix and reacting the resulting carboxyl-group containing matrix with an alkylene polyamine. The thioamide resins containing groups of Formula III may be formed by reacting the matrix with H 2 S and then with an amine. In Examples 1 and 2, an acrylonitrile-divinyl benzene or methacrylonitrile-divinyl benzene resin is hydrolysed prior to being reacted with diethylene thiamine. An acrylonitrile-divinyl benzene resin is reacted with o-phenylene diamine in Example 3.

5. 发明专利

GB1137029A Improvements in or relating to chemical reactions involving gaseous materials 未知
公开(公告)号：GB1137029A
公开(公告)日：1968-12-18
申请号：GB1686767
申请日：1967-04-12
申请人： DIAMOND ALKALI CO
IPC分类号： B01J19/08 , C01B21/06 , C01B21/076 , C01B21/16 , C01B21/20 , C01C3/00 , C01C3/02 , C07C2/80 , C22B4/00 , C22B9/22 , C22B21/02 , H05H1/42
摘要： 1,137,029. Treating gases with discharges. DIAMOND ALKALI CO. 12 April, 1967 [14 April, 1966], No. 16867/67. Heading C1A. [Also in Divisions C5 and H5] A reactor for the electrical-arc-promoted production of chemical materials has feed inlets 20 to a central zone 2 of the discharge zone 3 between spaced electrodes 18, 19 for a primary gas or fluidized solid entrained in a gaseous vehicle, and secondary gas introduction ports 8, 13, downstream from zone 2 such that a secondary gas is bled into and flows along the walls 7, 14 of zone 3 forming a sheath around the primary gas, the reactor having gas discharge passages 15, 16 (see also Divisions H3-H5). Suitable feedstocks including nitrogen, for the preparation of cyanogen, hydrogen cyanide, nitrogen oxides, hydrazine, titanium nitride or tungsten nitride; hydrogen, for the preparation of hydrogen cyanide, acetylene, metallic aluminium from aluminium oxide and titanium nitride from titanium tetrachloride; ammonia, for the preparation of titanium nitride and hydrogen cyanide; oxygen, for the preparation of acetylene or nitrogen oxides; as well as fluidized solid reactants such as carbon, aluminium oxide, titanium metal powder and tungsten metal powder entrained in a gas.

6. 发明专利

ES338946A1 UN PROCEDIMIENTO PARA LA ELECTRODEPOSICION DE DEPOSITOS DE CROMO NEGROS. 未知
公开(公告)号：ES338946A1
公开(公告)日：1968-09-01
申请号：ES338946
申请日：1967-04-05
申请人： DIAMOND ALKALI CO
IPC分类号： C25D3/08 , C23B

7. 发明专利

FR1534688A 未知
公开(公告)号：FR1534688A
公开(公告)日：1968-08-02
申请号：FR76330
申请日：1966-09-14
申请人： DIAMOND ALKALI CO
发明人： KECKLER DAVID P , JR JOHN EDWARD LOEFFLER
IPC分类号： C07C2/80

8. 发明专利

FR1515648A 未知
公开(公告)号：FR1515648A
公开(公告)日：1968-03-01
申请号：FR100375
申请日：1967-03-28
申请人： DIAMOND ALKALI CO
IPC分类号： B05D3/02

9. 发明专利

FR1513660A 未知
公开(公告)号：FR1513660A
公开(公告)日：1968-02-16
申请号：FR92702
申请日：1967-01-27
申请人： DIAMOND ALKALI CO
发明人： HORVATH ROLAND JOSEPH , PARSONS CHARLES GRIMM , ZETTLER TOBY THOMAS
IPC分类号： C02F1/50

10. 发明专利

CA776186A VINYL FLUORIDE POLYMER DISPERSION COMPOSITIONS 未知
公开(公告)号：CA776186A
公开(公告)日：1968-01-16
申请号：CA776186D
申请人： DIAMOND ALKALI CO
发明人： FORDHAM JAMES W L , SIEGLAFF CHARLES L

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