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1. 发明申请

WO2006068157B1 PROCESS FOR PRODUCING ACETIC ACID 审中-公开
标题翻译：生产乙酸的方法
公开(公告)号：WO2006068157B1
公开(公告)日：2006-11-02
申请号：PCT/JP2005023420
申请日：2005-12-14
申请人： DAICEL CHEM , KOJIMA HIDETAKA
发明人： KOJIMA HIDETAKA
IPC分类号： C07C51/12 , C07C53/08
CPC分类号： C07C51/02 , C07C53/08
摘要： A process for producing a carboxylic acid comprises allowing an alcohol having a carbon number of "n" to continuously react with carbon monoxide in. the presence of a carbonylation catalyst system, and a limited amount of water, continuously withdrawing the reaction mixture from the reaction system 1, introducing the withdrawn reaction mixture into a distillation step (distillation columns 3a and 3b), and separating a higher-boiling component and a lower-boiling component containing a carboxylic acid having a carbon number of "n+1", respectively. In the process, the amount of carbon monoxide and/or hydrogen contained in a liquid phase of the reaction system is adjusted to at least one of the following conditions (i) and (ii): (i) the amount of carbon monoxide relative to 1 kilogram of the liquid phase by weight is at least 2 mmol per 1 MPa of carbon monoxide partial pressure of the reaction system, and (ii) the amount of hydrogen relative to 1 kilogram of the liquid phase by weight is at least 50 mmol per 1 MPa of hydrogen partial pressure of the reaction system. Such a process inhibits deactivation of a metal catalyst and deterioration in a reaction rate, and decreases formation of by-products in producing a carboxylic acid under a low water content.
摘要翻译：一种制备羧酸的方法包括在羰基化催化剂体系和有限量的水的存在下，使碳数为“n”的醇与一氧化碳连续反应，连续地从反应中取出反应混合物系统1，将抽出的反应混合物引入蒸馏步骤（蒸馏塔3a和3b）中，分别分离含有碳数为“n + 1”的羧酸的高沸点组分和低沸点组分。在此过程中，将反应体系的液相中所含的一氧化碳和/或氢的量调节至以下条件（i）和（ii）中的至少一个：（i）一氧化碳相对于 1千克液相重量比为每1MPa反应体系的一氧化碳分压至少2毫摩尔，和（ii）相对于1千克液相重量的氢的量为至少50毫摩尔/ 1MPa的氢分压反应体系。这种方法抑制金属催化剂的失活和反应速度的劣化，并且在低水含量下生产羧酸时减少副产物的形成。

2. 发明申请

WO2005075446A9 UNSATURATED CARBOXYLIC ACID HEMIACETAL ESTER, POLYMER, AND RESIN COMPOSITION FOR PHOTORESIST 审中-公开
标题翻译：不饱和羧酸乙酯，聚合物和树脂组合物
公开(公告)号：WO2005075446A9
公开(公告)日：2005-10-06
申请号：PCT/JP2005000794
申请日：2005-01-17
申请人： DAICEL CHEM , KOYAMA HIROSHI , INOUE KEIZO , IWAHAMA TAKAHIRO , SUMIDA MARI
发明人： KOYAMA HIROSHI , INOUE KEIZO , IWAHAMA TAKAHIRO , SUMIDA MARI
IPC分类号： C07C69/54 , C07D307/00 , C07D307/94 , G03F7/039 , C08F220/26 , H01L21/027
CPC分类号： C07D307/00 , C07C69/54 , C07D307/94 , G03F7/0397
摘要： A polymer comprising repeating units corresponding to an unsaturated carboxylic acid hemiacetal ester represented by the following formula (1): (1) (wherein R represents hydrogen, halogeno, C1-6 alkyl, or C1-6 haloalkyl; R represents a hydrocarbon group having a hydrogen atom in the 1-position; R represents hydrogen or a hydrocarbon group; and R represents an organic group containing a cyclic skeleton). The polymer may further contain repeating units corresponding to at least one monomer selected among monomers having a lactone skeleton, monomers having a cyclic ketone skeleton, monomers having an acid anhydride group, and monomers having an imide group [excluding the repeating units corresponding to the unsaturated carboxylic acid hemiacetal ester] and/or repeating units corresponding to at least one monomer selected among monomers having a hydroxy group, etc. When used in a photoresist, this polymer has the excellent property to release an acid.
摘要翻译：包含对应于下式（1）表示的不饱和羧酸半缩醛酯的重复单元的聚合物：（1）（其中R a表示氢，卤代，C 1-6烷基或C 1-6卤代烷基; R b >表示在1位具有氢原子的烃基，R c表示氢或烃基，R d表示含有环状骨架的有机基团。聚合物可以进一步含有对应于至少一种选自具有内酯骨架的单体，具有环酮骨架的单体，具有酸酐基的单体和具有酰亚胺基的单体的单体的重复单元[不包括与不饱和单体相应的重复单元羧酸半缩醛酯]和/或对应于选自具有羟基的单体中的至少一种单体的重复单元等。当在光致抗蚀剂中使用时，该聚合物具有优异的脱酸性质。

3. 发明申请

WO2004033407A3 PROCESS FOR PRODUCING CARBOXYLIC ACID AND SYSTEM FOR PRODUCING THE SAME 审中-公开
标题翻译：生产羧酸的方法及其制备方法
公开(公告)号：WO2004033407A3
公开(公告)日：2005-02-24
申请号：PCT/JP0312696
申请日：2003-10-03
申请人： DAICEL CHEM , HORIGUCHI AKIRA , INA TOMOHIDE , MIURA HIROYUKI
发明人： HORIGUCHI AKIRA , INA TOMOHIDE , MIURA HIROYUKI
IPC分类号： B01D3/14 , C07B61/00 , C07C51/12 , C07C51/44 , C07C53/08 , C07C53/122 , C07C53/124
CPC分类号： C07C51/12 , C07C51/44 , C07C53/08 , C07C53/122
摘要： In the presence of a catalytic system, an alcohol having "n" carbon atom(s) or a derivative thereof is allowed to react with carbon monoxide in a reactor 3 continuously, a higher by catalyst component is separated from the resultant reaction mixture by a catalyst-separating column 5 to give a crude mixture, the crude mixture is fed to a higher by component-separation column 8 to separate an overhead fraction from a bottom fraction containing at least a carboxylic acid having "n+2" carbon atoms, the overhead fraction is fed to a carboxylic acid-separating column 11, and are distilled in the presence of at least water and an ester of the carboxylic acid with the alcohol to separate a overhead fraction containing at least the ester and water from a bottom fraction containing the carboxylic acid having "n+l" carbon atoms. The overhead fraction from the carboxylic acid-separating column is fed to an aldehyde-separating column 14 to remove an overhead fraction containing an aldehyde. Such a process insures that impurities are efficiently separated from a reaction mixture by carbonylation of an alcohol, and that a carboxylic acid is purified easily at a lower cost.
摘要翻译：在催化体系的存在下，使具有“n”个碳原子的醇或其衍生物的醇连续地与反应器3中的一氧化碳反应，通过催化剂组分将较高的催化剂组分与所得反应混合物分离催化剂分离塔5以得到粗混合物，粗混合物通过组分分离塔8进料到较高的分离塔8中，以分离塔塔馏分与至少含有“n + 2”碳原子的羧酸的塔底级分，将塔顶馏分进料到羧酸分离塔11中，并在至少水和羧酸的酯存在下与醇蒸馏，以从含有至少含有酯和水的塔底馏分分离含有具有“n + 1”个碳原子的羧酸。将来自羧酸分离塔的塔顶馏分进料到醛分离塔14以除去含有醛的塔顶馏分。这样的方法确保通过醇的羰基化有效地将杂质与反应混合物分离，并且以较低的成本容易地纯化羧酸。

4. 发明申请

WO1982003219A1 COPOLYMERIZED POLYAMIDE RESIN 审中-公开
标题翻译：共聚聚酰胺树脂
公开(公告)号：WO1982003219A1
公开(公告)日：1982-09-30
申请号：PCT/JP1982000068
申请日：1982-03-16
申请人： DAICEL CHEM IND CO LTD , ARITA KOICHIRO , SUZUKI HAJIME
发明人： DAICEL CHEM IND CO LTD
IPC分类号： C08G69/02
CPC分类号： C08G69/00 , C08G69/44 , C08G69/48 , C08G81/028
摘要： Resine polyamide copolimerisee composee de 5 a 99 parties en poids d'un composant polyamide contenant au moins un type d'unites recurrentes representees par la formule generale (1) ou (2): (ou r represente un nombre entier compris entre 5 et 11) (ou X represente CmH2m (ou m est un nombre entier allant de 6 a 12), un groupe isophorone, un groupe phenylene ou un groupe cyclohexylene, et Y represente C1H21 (ou 1 est un nombre entier allant de 4 a 10), un groupe phenylene ou un groupe cyclohexylene), et de 1 a 95 parties en poids d'un composant de polyolefine d'un poids moleculaire moyen compris entre 500 et 10000 possedant des groupes d'acide carboxylique, des groupes amines ou hydroxy a ses deux terminaux. Cette resine possede une absorptivite extremement faible.

5. 发明申请

WO2004108686A3 BENZIMIDAZOLE COMPOUNDS HAVING HYPOGLYCEMIC ACTIVITY 审中-公开
标题翻译：具有高分子活性的苯并咪唑化合物
公开(公告)号：WO2004108686A3
公开(公告)日：2005-05-26
申请号：PCT/JP2004008064
申请日：2004-06-03
申请人： FUJISAWA PHARMACEUTICAL CO , DAICEL CHEM , HAYASHIDA HISASHI , HATANAKA KEIKO , KATO TAKESHI , KIDO YOSHIYUKI , TOMISHIMA MASAKI , KAYAKIRI HIROSHI , TAKASE ICHIRO , HIRAMURA TAKAHIRO
发明人： HAYASHIDA HISASHI , HATANAKA KEIKO , KATO TAKESHI , KIDO YOSHIYUKI , TOMISHIMA MASAKI , KAYAKIRI HIROSHI , TAKASE ICHIRO , HIRAMURA TAKAHIRO
IPC分类号： C07D235/08 , C07D235/10 , C07D235/26 , C07D235/28 , C07D401/06 , C07D401/12 , C07D413/06 , C07D417/06 , A61K31/4184 , C07D235/30 , C07D401/04 , C07D401/10 , C07D401/14 , C07D403/04 , C07D403/10 , C07D409/04 , C07D413/04
CPC分类号： C07D401/06 , C07D235/08 , C07D235/10 , C07D235/26 , C07D235/28 , C07D401/12 , C07D413/06 , C07D417/06
摘要： The present invention provides novel benzimidazole compounds of the formula (I): wherein each symbol is as defined in the specification, salts thereof and prodrugs thereof, which are useful in treating, for example, the diseases curable through decrease in blood sugar level.
摘要翻译：本发明提供新的式（I）的苯并咪唑化合物：其中每个符号如本说明书中所定义，其盐和前药，其可用于治疗例如通过降低血糖水平可治愈的疾病。

6. 发明申请

WO02070717A3 NITRILE HYDRATASE AND A METHOD FOR PRODUCING AMIDES 审中-公开
标题翻译： NITRILE HYDRATASE和一种生产AMIDES的方法
公开(公告)号：WO02070717A3
公开(公告)日：2003-03-27
申请号：PCT/JP0201912
申请日：2002-03-01
申请人： DAICEL CHEM , NAGASAWA TOHRU , MATSUYAMA AKINOBU
发明人： NAGASAWA TOHRU , MATSUYAMA AKINOBU
IPC分类号： C12N15/09 , C12N1/15 , C12N1/19 , C12N1/21 , C12N5/10 , C12N9/88 , C12N15/60 , C12P13/02 , C12P17/00 , C12R1/01
CPC分类号： C12P13/02 , C12N9/88
摘要： An objective of the present invention is to provide a nitrile hydratase capable of producing 2-hydroxy-4-methylthiobutyroamide. The present invention provides a novel nitrile hydratase producing alpha -hydroxyamide using alpha -hydroxynitrile as the substrate, and the encoding DNA thereof. The enzyme can be obtained from Rhodococcus sp. Further, the enzymatic activity of the enzyme can be maintained stably during the reaction. The present invention provides a method for producing amide compounds,the method comprising the step of reacting this enzyme to nitrile compounds. According to the present invention, from hydroxy nitrile compounds, corresponding amide compounds can be produced biochemically without reducing the enzyme activity of nitrile hydratase.
摘要翻译：本发明的目的是提供能够生产2-羟基-4-甲硫基丁酰胺的腈水合酶。本发明提供使用α-羟基腈作为底物产生α-羟基酰胺的新型腈水合酶及其编码DNA。该酶可以从红球菌（Rhodococcus sp。）获得。此外，酶的酶活性可以在反应期间保持稳定。本发明提供了一种制备酰胺化合物的方法，所述方法包括使该酶与腈化合物反应的步骤。根据本发明，由羟基腈化合物可以生物化学地制备相应的酰胺化合物，而不会降低腈水合酶的酶活性。

7. 发明申请

WO2005005346A3 POLYMERIZABLE ADAMANTANE DERIVATIVE, PROCESS FOR PRODUCING THE SAME, AND POLYMER 审中-公开
标题翻译：可聚合的ADAMANTANE衍生物，其制备方法和聚合物
公开(公告)号：WO2005005346A3
公开(公告)日：2005-03-31
申请号：PCT/JP2004008856
申请日：2004-06-17
申请人： DAICEL CHEM , KOYAMA HIROSHI , TSUTSUMI KIYOHARU
发明人： KOYAMA HIROSHI , TSUTSUMI KIYOHARU
IPC分类号： C07C69/533 , C07C20060101 , C07C67/08 , C07C67/14 , C07C69/00 , C08F20/16 , C08F20/18 , G03C1/76
CPC分类号： C07C67/14 , C07C69/653 , C07C2603/74 , C08F220/18
摘要： A polymerizable adamantane derivative represented by the following formula (1): (1) wherein R represents fluorine or fluoroalkyl and the adamantane ring may be substituted. Examples of the fluoroalkyl include trifluoromethyl, pentafluoroethyl, 2,2,2-trifluoroethyl, 2,2,2-trifluoro-1-(trifluoromethyl)ethyl, and heptafluoropropyl.
摘要翻译：由下式（1）表示的可聚合金刚烷衍生物：（1）其中R 1表示氟或氟代烷基并且金刚烷环可以被取代。氟代烷基的实例包括三氟甲基，五氟乙基，2,2,2-三氟乙基，2,2,2-三氟-1-（三氟甲基）乙基和七氟丙基。

8. 发明申请

WO2010005122A3 METHOD OF MANUFACTURING SUBSTANCES BY SUPERCRITICAL FLUID CHROMATOGRAPHY 审中-公开
标题翻译：超临界液相色谱法制备物质的方法
公开(公告)号：WO2010005122A3
公开(公告)日：2010-04-01
申请号：PCT/JP2009068544
申请日：2009-10-22
申请人： DAICEL CHEM , MIYAZAWA KENICHIRO , ISHIGURO TAKESHI
发明人： MIYAZAWA KENICHIRO , ISHIGURO TAKESHI
IPC分类号： G01N30/34 , B01D15/40
CPC分类号： G01N30/34 , B01D15/166 , B01D15/40 , G01N30/84
摘要： Provided is a method of manufacturing target substances with use of supercritical fluid chromatography, by which the following are achieved: increase in throughput of samples containing the target substances; an increase of a treatment amount of separation per unit time; and improvement of efficiency in separation. The method includes the steps of : injecting the sample containing the target substances into a mobile phase; and returning the composition of the mobile phase to a pre-change state after changing the composition of the mobile phase. The steps of changing the composition of the mobile phase and returning it to its pre-change state are performed during a period of time between detection of the peak of the last target substance of interest to elute from the column and injection of the next sample.
摘要翻译：提供了使用超临界流体色谱法制造目标物质的方法，通过该方法实现以下目的：增加含有目标物质的样品的通过量; 每单位时间处理量的增加; 并提高分离效率。该方法包括以下步骤：将含有目标物质的样品注入流动相中; 并且在改变流动相的组成之后将流动相的组成返回到预改变状态。改变流动相的组成并将其返回到其预变化状态的步骤是在检测最后一个目标物质的峰值从色谱柱洗脱出来并在下一个样品的注入之间的一段时间内进行的。

9. 发明申请

WO2005044899A8 PREPOLYMER, PREPOLYMER COMPOSITION, HIGH MOLECULAR WEIGHT POLYMER HAVING STRUCTURE CONTAINING HOLE AND ELECTRICALLY INSULATING FILM 审中-公开
标题翻译：预聚物，预聚物组合物，具有包含孔和电绝缘膜的结构的高分子量聚合物
公开(公告)号：WO2005044899A8
公开(公告)日：2005-06-30
申请号：PCT/JP2004015870
申请日：2004-10-20
申请人： DAICEL CHEM , TAKARAGI AKIRA , FUNAKI YOSHINORI , HASHIMOTO JIICHIRO
发明人： TAKARAGI AKIRA , FUNAKI YOSHINORI , HASHIMOTO JIICHIRO
IPC分类号： C08G73/06 , C07C251/08 , C07C251/18 , C07C251/20 , H01L21/312 , H01L21/768 , H01L23/522 , C08G85/00
CPC分类号： C08G73/22 , C07C251/08 , C07C251/18 , C07C251/20 , C07C2601/14 , C08G69/00 , C08G73/10 , C08G73/18 , C08G85/00
摘要： A prepolymer, characterized in that it is prepared by the reaction of two compounds A and B which have two or more functional moieties or two or more groups of functional moieties, respectively, and are capable of undergoing a polymerization through the bonding of a functional moiety or a group of functional moieties of one compound with a functional moiety or a group of functional moieties of the other compound to form a high molecular weight polymer having a structure containing a hole. The prepolymer has a weight average molecular weight of ca. 200 to 100000. In a preferred embodiment, the compound A has a carboxyl moiety or an amino moiety as the above functional moiety or a group of functional moieties, and the compound B has two amino moieties, an amino moiety and a hydroxyl moiety, an amino moiety and a mercapto moiety, or two carboxyl moieties as the above functional moiety or a group of functional moieties.
摘要翻译：一种预聚物，其特征在于其通过分别具有两个或更多个官能部分或两个或多个官能部分组的两种化合物A和B的反应制备，并且能够通过键合官能部分进行聚合或一组化合物与一种其它化合物的官能部分或一组官能部分的官能部分组成，以形成具有含孔结构的高分子量聚合物。预聚物的重均分子量约为在优选的实施方案中，化合物A具有作为上述官能部分的羧基部分或氨基部分或一组官能部分，化合物B具有两个氨基部分，氨基部分和羟基部分，氨基部分和巯基部分，或两个羧基部分作为上述官能部分或一组官能部分。

10. 发明申请

WO0013470A8 MATERIAL FOR ORGANIC ELECTROLUMINESCENCE DEVICE AND METHOD FOR PRODUCING THE SAME 审中-公开
标题翻译：有机电致发光器件的材料及其制造方法
公开(公告)号：WO0013470A8
公开(公告)日：2000-06-29
申请号：PCT/JP9904668
申请日：1999-08-27
申请人： DAICEL CHEM , KITAGUCHI TORU , FUKUMURA HIROSHI
发明人： KITAGUCHI TORU , FUKUMURA HIROSHI
IPC分类号： H01L51/00 , H01L51/30 , H01L51/50 , H05B33/10 , H05B33/14
CPC分类号： H05B33/10 , H01L51/0013 , H01L51/0042 , H01L51/005 , H01L51/0059 , H01L51/5012
摘要： A material adapted for an organic electroluminescence device and having a radiative recombination center is produced by bringing a source (1) containing a radiative recombination center formig compound capable of absorbing laser light into contact with a target (2) transmitting laser light and having at least one of an electron transport function and a hole transport function, irradiating the surface on the source (1) side (or on the target (2) side) with a laser beam the intensity of which is less than the laser ablation threshold of the source (1), and injecting a radiative recombination center forming compound (3) in the source (1) into the target (2). Thus, the material can be subjected to fine patterning.
摘要翻译：通过使含有能够吸收激光的辐射复合中心化合物的源（1）与发射激光的靶（2）接触而产生具有辐射复合中心的材料，并具有至少电子传输功能和空穴传输功能之一，用激光束照射源（1）侧（或目标（2）侧）上的表面，该激光束的强度小于源的激光烧蚀阈值（1），并且将源（1）中的形成化合物（3）的辐射复合中心注入到靶（2）中。因此，可以对该材料进行精细图案化。

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