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1. 发明授权

US06767636B2 Thermal spray rare earth oxide particles, sprayed components, and corrosion resistant components 有权
标题翻译：热喷涂稀土氧化物颗粒，喷涂组分和耐腐蚀组分
公开(公告)号：US06767636B2
公开(公告)日：2004-07-27
申请号：US10101612
申请日：2002-03-21
申请人： Yasushi Takai , Takao Maeda , Toshihiko Tsukatani
发明人： Yasushi Takai , Takao Maeda , Toshihiko Tsukatani
IPC分类号： B32B516
CPC分类号： C23C4/11 , Y10T428/24372 , Y10T428/24413 , Y10T428/256 , Y10T428/2982
摘要： Rare earth oxide particles having an average particle diameter of 3-20 &mgr;m, a dispersion index of up to 0.4, and an aspect ratio of up to 2 are suitable for thermal spraying. Despite their high melting point, the rare earth oxide particles of high purity can form an adherent coating by thermal spraying.
摘要翻译：平均粒径为3-20μm的稀土氧化物粒子，分散指数为0.4以上，纵横比为2以下，适用于热喷涂。尽管高熔点，但高纯度的稀土氧化物颗粒可以通过热喷涂形成粘附涂层。

2. 发明授权

US06733843B2 Method for thermal spray coating and rare earth oxide powder used therefor 有权
标题翻译：热喷涂法和稀土氧化物粉末的使用方法
公开(公告)号：US06733843B2
公开(公告)日：2004-05-11
申请号：US10423903
申请日：2003-04-28
申请人： Toshihiko Tsukatani , Yasushi Takai , Takao Maeda
发明人： Toshihiko Tsukatani , Yasushi Takai , Takao Maeda
IPC分类号： C23C410
CPC分类号： C23C4/11 , Y10T428/25 , Y10T428/26 , Y10T428/2982
摘要： The invention discloses an efficient method for the formation of a highly corrosion- or etching-resistant thermal spray coating layer of a rare earth oxide or rare earth-based composite oxide by a process of plasma thermal spray method by using a unique thermal spray powder consisting of granules of the oxide. The thermal spray granules are characterized by a specified average particle diameter of 5 to 80 &mgr;m with a specified dispersion index of 0.1 to 0.7 and a specified BET specific surface area of 1 to 5 m2/g as well as a very low content of impurity iron not exceeding 5 ppm by weight as oxide. The flame spat powder used here is characterized by several other granulometric parameters including globular particle configuration, particle diameter D90, bulk density and cumulative pore volume.
摘要翻译：本发明公开了一种通过使用独特的热喷涂粉末等离子体热喷涂方法形成稀土氧化物或稀土类复合氧化物的高耐腐蚀或耐蚀刻热喷涂层的有效方法，的氧化物颗粒。热喷雾颗粒的特征在于指定的平均粒径为5-80μm，指定的分散指数为0.1-0.7，指定的BET比表面积为1-5m 2 / g，并且含量非常低的杂质铁作为氧化物不超过5ppm。这里使用的火焰喷雾粉的特征在于几种其他粒度参数，包括球状颗粒构型，粒径D90，体积密度和累积孔体积。

3. 发明授权

US06576354B2 Method for thermal spray coating and rare earth oxide powder used therefor 有权
公开(公告)号：US06576354B2
公开(公告)日：2003-06-10
申请号：US09893565
申请日：2001-06-29
申请人： Toshihiko Tsukatani , Yasushi Takai , Takao Maeda
发明人： Toshihiko Tsukatani , Yasushi Takai , Takao Maeda
IPC分类号： B32B1504
CPC分类号： C23C4/11 , Y10T428/25 , Y10T428/26 , Y10T428/2982
摘要： The invention discloses an efficient method for the formation of a highly corrosion- or etching-resistant thermal spray coating layer of a rare earth oxide or rare earth-based composite oxide by a process of plasma thermal spray method by using a unique thermal spray powder consisting of granules of the oxide. The thermal spray granules are characterized by a specified average particle diameter of 5 to 80 &mgr;m with a specified dispersion index of 0.1 to 0.7 and a specified BET specific surface area of 1 to 5 m2/g as well as a very low content of impurity iron not exceeding 5 ppm by weight as oxide. The flame spat powder used here is characterized by several other granulometric parameters including globular particle configuration, particle diameter D90, bulk density and cumulative pore volume.

4. 发明申请

US20110272725A1 WAVELENGTH CONVERTING MEMBER, LIGHT-EMITTING DEVICE, AND METHOD FOR MANUFACTURING WAVELENGTH CONVERTING MEMBER 有权
标题翻译：波长转换构件，发光装置和制造波长转换构件的方法
公开(公告)号：US20110272725A1
公开(公告)日：2011-11-10
申请号：US13102147
申请日：2011-05-06
申请人： Kazuhiro Wataya , Toshihiko Tsukatani , Yasushi Takai
发明人： Kazuhiro Wataya , Toshihiko Tsukatani , Yasushi Takai
IPC分类号： H01L33/50 , C04B35/64 , F21V9/00
CPC分类号： C04B35/44 , C04B35/01 , C04B35/62685 , C04B2235/3222 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3286 , C04B2235/3418 , C04B2235/3427 , C04B2235/3463 , C04B2235/5445 , C04B2235/6567 , C04B2235/6581 , C04B2235/764 , C04B2235/77 , C04B2235/786 , C04B2235/80 , C04B2235/87 , C04B2235/963 , C09K11/7774 , H01L33/502
摘要： A polycrystalline sintered ceramic including (A) a garnet phase and (B) a perovskite, monoclinic or silicate phase wherein fine grains of phase (B) are included and dispersed in phase (A) is used as a wavelength converting member. Since the light transmitting through the wavelength converting member is scattered at the interface between the garnet phase and the perovskite, monoclinic or silicate phase, a light emitting device including the wavelength converting member produces light of more uniform color with a minimized loss thereof.
摘要翻译：使用包含（A）石榴石相的（A）和（B）其中包含相和（A）相的细晶粒并分散在相（A）中的钙钛矿，单斜晶系或硅酸盐相的多晶烧结陶瓷作为波长转换部件。由于通过波长转换构件透射的光在石榴石相和钙钛矿，单斜晶系或硅酸盐相之间的界面处散射，所以包括波长转换构件的发光器件产生更均匀的颜色的光并以最小的损耗产生。

5. 发明授权

US06733882B2 Rare earth hydroxide and method for the preparation thereof 有权
标题翻译：稀土氢氧化物及其制备方法
公开(公告)号：US06733882B2
公开(公告)日：2004-05-11
申请号：US09923441
申请日：2001-08-08
申请人： Yasushi Takai , Toshihiko Tsukatani
发明人： Yasushi Takai , Toshihiko Tsukatani
IPC分类号： B32B516
CPC分类号： C01F17/0043 , C01P2002/60 , C01P2004/61 , C01P2006/12 , C01P2006/60 , C01P2006/80 , C04B35/50 , Y10T428/2982
摘要： The invention discloses a method for the preparation of a rare earth hydroxide powder in which, different from the conventional wet-process hydroxide precipitation method in an aqueous solution of a rare earth salt by the addition of an alkali, a powder of a rare earth oxide is brought into contact with a limited amount of water in the form of either liquid or vapor and kept in contact with water at a temperature of 30 to 200° C. The thus prepared rare earth hydroxide powder is characterized by a small crystallite diameter not exceeding 40 nm and outstandingly low contents of impurity chlorine and nitrate ions originating in the starting rare earth salt in the hydroxide prepared by the conventional wet-process method. The inventive rare earth hydroxide powder is advantageous as a component ingredient or as an adjuvant in the ceramic compositions for the preparation of a sintered dielectric ceramic bodies in respects of the greater dielectric constant and smaller temperature dependency of the dielectric constant than similar ceramic bodies prepared from a conventional rare earth hydroxide or oxide.
摘要翻译：本发明公开了一种制备稀土氢氧化物粉末的方法，其中不同于常规湿法氢氧化物沉淀法，在稀土盐水溶液中加入碱，稀土氧化物粉末与液体或蒸气形式的有限量的水接触，并在30至200℃的温度下与水接触。由此制备的稀土氢氧化物粉末的特征在于微晶直径不超过 40nm，并且通过常规湿法制备的氢氧化物中源自起始稀土盐的杂质氯和硝酸根离子的含量显着低。本发明的稀土氢氧化物粉末作为陶瓷组合物中的组分成分或佐剂是有利的，所述陶瓷组合物用于制备烧结介电陶瓷体的介电常数和介电常数的较小的温度依赖性比由常规稀土氢氧化物或氧化物。

6. 发明申请

US20120175559A1 PHOSPHOR PARTICLES AND MAKING METHOD 有权
标题翻译：磷化物颗粒和制备方法
公开(公告)号：US20120175559A1
公开(公告)日：2012-07-12
申请号：US13336137
申请日：2011-12-23
申请人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
发明人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
IPC分类号： C09K11/80 , C09K11/00
CPC分类号： C09K11/7774 , C01F17/0025 , C01P2002/50 , C01P2002/72 , C01P2002/84 , C01P2002/85 , C01P2004/03 , C01P2004/30 , C01P2004/61 , C01P2004/62
摘要： Phosphor particles are provided in the form of spherical polycrystalline secondary particles consisting of a multiplicity of primary particles, including a garnet phase having the composition: (AxByCz)3C5O12 wherein A is Y, Gd, and/or Lu, B is Ce, Nd, and/or Tb, C is Al and/or Ga, and x, y and z are in the range: 0.002
摘要翻译：由多种一次粒子构成的球状多晶二次粒子的形式提供荧光体粒子，其包括具有以下成分的石榴石相：（AxByCz）3C5O12，其中A为Y，Gd和/或Lu，B为Ce，Nd，和/或Tb，C是Al和/或Ga，x，y和z在以下范围内：0.002

7. 发明授权

US08445931B2 Wavelength converting member, light-emitting device, and method for manufacturing wavelength converting member 有权
标题翻译：波长变换部件，发光元件及波长转换部件的制造方法
公开(公告)号：US08445931B2
公开(公告)日：2013-05-21
申请号：US13102147
申请日：2011-05-06
申请人： Kazuhiro Wataya , Toshihiko Tsukatani , Yasushi Takai
发明人： Kazuhiro Wataya , Toshihiko Tsukatani , Yasushi Takai
IPC分类号： H01L33/00
CPC分类号： C04B35/44 , C04B35/01 , C04B35/62685 , C04B2235/3222 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3286 , C04B2235/3418 , C04B2235/3427 , C04B2235/3463 , C04B2235/5445 , C04B2235/6567 , C04B2235/6581 , C04B2235/764 , C04B2235/77 , C04B2235/786 , C04B2235/80 , C04B2235/87 , C04B2235/963 , C09K11/7774 , H01L33/502
摘要： A polycrystalline sintered ceramic including (A) a garnet phase and (B) a perovskite, monoclinic or silicate phase wherein fine grains of phase (B) are included and dispersed in phase (A) is used as a wavelength converting member. Since the light transmitting through the wavelength converting member is scattered at the interface between the garnet phase and the perovskite, monoclinic or silicate phase, a light emitting device including the wavelength converting member produces light of more uniform color with a minimized loss thereof.
摘要翻译：使用包含（A）石榴石相的（A）和（B）其中包含相和（A）相的细晶粒并分散在相（A）中的钙钛矿，单斜晶系或硅酸盐相的多晶烧结陶瓷作为波长转换部件。由于通过波长转换构件透射的光在石榴石相和钙钛矿，单斜晶系或硅酸盐相之间的界面处散射，所以包括波长转换构件的发光器件产生更均匀的颜色的光并以最小的损耗产生。

8. 发明授权

US08865022B2 Phosphor particles and making method 有权
标题翻译：磷光体颗粒及其制备方法
公开(公告)号：US08865022B2
公开(公告)日：2014-10-21
申请号：US13336137
申请日：2011-12-23
申请人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
发明人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
IPC分类号： C09K11/08 , C09K11/77 , C01F17/00
CPC分类号： C09K11/7774 , C01F17/0025 , C01P2002/50 , C01P2002/72 , C01P2002/84 , C01P2002/85 , C01P2004/03 , C01P2004/30 , C01P2004/61 , C01P2004/62
摘要： Phosphor particles are provided in the form of spherical polycrystalline secondary particles consisting of a multiplicity of primary particles, including a garnet phase having the composition: (AxByCz)3C5O12 wherein A is Y, Gd, and/or Lu, B is Ce, Nd, and/or Tb, C is Al and/or Ga, and x, y and z are in the range: 0.002
摘要翻译：由多种一次粒子构成的球状多晶二次粒子的形式提供荧光体粒子，其包括具有以下成分的石榴石相：（AxByCz）3C5O12，其中A为Y，Gd和/或Lu，B为Ce，Nd，和/或Tb，C是Al和/或Ga，x，y和z在以下范围内：0.002

9. 发明申请

US20120175658A1 PHOSPHOR PARTICLES, MAKING METHOD, AND LIGHT-EMITTING DIODE 有权
标题翻译：磷化物颗粒，制造方法和发光二极管
公开(公告)号：US20120175658A1
公开(公告)日：2012-07-12
申请号：US13336152
申请日：2011-12-23
申请人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
发明人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
IPC分类号： C09K11/78 , H01L33/50
CPC分类号： C09K11/7774 , C01F17/0025 , C01P2002/52 , C01P2002/72 , C01P2002/84 , C01P2004/03 , C01P2004/32 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/80
摘要： Phosphor particles are provided in the form of spherical polycrystalline secondary particles consisting of a multiplicity of primary particles, including a garnet phase having the compositional formula: (A1-xBx)3C5O12 wherein A is Y, Gd, and/or Lu, B is Ce, Nd, and/or Tb, C is Al and/or Ga, and 0.002≦x≦0.2, the secondary particles having an average particle size of 5-50 μm.
摘要翻译：以由多种一次粒子组成的球状多晶二次粒子的形式提供荧光体颗粒，其包括具有组成式：（A1-xBx）3C5O12的石榴石相，其中A为Y，Gd和/或Lu，B为Ce ，Nd和/或Tb，C为Al和/或Ga，和0.002≤n1E; x和nlE; 0.2，二次粒子的平均粒径为5-50μm。

10. 发明授权

US09617469B2 Phosphor particles, making method, and light-emitting diode 有权
公开(公告)号：US09617469B2
公开(公告)日：2017-04-11
申请号：US13336152
申请日：2011-12-23
申请人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
发明人： Toshihiko Tsukatani , Kazuhiro Wataya , Yasushi Takai , Takehisa Minowa
IPC分类号： C09K11/80 , C09K11/77 , C01F17/00
CPC分类号： C09K11/7774 , C01F17/0025 , C01P2002/52 , C01P2002/72 , C01P2002/84 , C01P2004/03 , C01P2004/32 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/80
摘要： Phosphor particles are provided in the form of spherical polycrystalline secondary particles consisting of a multiplicity of primary particles, including a garnet phase having the compositional formula: (A1-xBx)3C5O12 wherein A is Y, Gd, and/or Lu, B is Ce, Nd, and/or Tb, C is Al and/or Ga, and 0.002≦x≦0.2, the secondary particles having an average particle size of 5-50 μm.

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