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1. 发明授权

US07790930B2 Method for purifying cyclic ketones 有权
标题翻译：环酮纯化方法
公开(公告)号：US07790930B2
公开(公告)日：2010-09-07
申请号：US12306815
申请日：2007-06-27
申请人： Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/27
CPC分类号： C07C45/85 , C07C45/34 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with a catalyst comprising at least one transition metal and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization. Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one catalyst comprising at least one transition metal for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with a catalyst comprising at least one transition metal.
摘要翻译：本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用包含至少一种过渡金属的催化剂热处理组合物（I）并进一步纯化通过选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及至少一种包含至少一种过渡金属的催化剂用于纯化组合物（I）的用途，所述组合物（I）包含至少一种具有7〜 16个碳原子通过用包含至少一种过渡金属的催化剂热处理组合物（I）。

2. 发明授权

US07714172B2 Method for the production of cyclic ketones 失效
标题翻译：环酮生产方法
公开(公告)号：US07714172B2
公开(公告)日：2010-05-11
申请号：US12306827
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C45/85 , C07C2601/18 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic alkene which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B), (c) hydrogenation of the composition (B) in the presence of at least one catalyst to give a composition (C), (d) purification of the composition (C), comprising at least the steps (di) thermal treatment of the composition (C) with at least one acid or at least one catalyst comprising at least one transition metal, (dii) further purification by a method selected from the group consisting of distillation, extraction and crystallization.
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）氧化包含至少一个具有7至16个碳原子的环烯烃的组合物（I）和至少一个C-C双键，得到组合物（A），（b）用至少一种碱处理组合物（A），得到组合物（B），（c）氢化所述组合物（B）在至少一种催化剂的存在下反应以得到组合物（C），（d）组合物（C）的纯化，所述组合物（C）至少包含步骤（ii）组合物（C）至少一种酸或至少一种包含至少一种过渡金属的催化剂，（dii）通过选自蒸馏，萃取和结晶的方法进一步纯化。

3. 发明授权

US07714171B2 Method for purifying cyclic ketones 有权
标题翻译：环酮纯化方法
公开(公告)号：US07714171B2
公开(公告)日：2010-05-11
申请号：US12306807
申请日：2007-06-27
申请人： Rolf Pinkos , Gerd Tebben , Alexander Hauk , Christian Müller , Harald Rust
发明人： Rolf Pinkos , Gerd Tebben , Alexander Hauk , Christian Müller , Harald Rust
IPC分类号： C07C45/27
CPC分类号： C07C45/85 , C07C45/33 , C07C45/34 , C07C45/58 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C49/413 , C07C49/607
摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with at least one acid and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization, Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one acid for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with the acid.
摘要翻译：本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用至少一种酸对组合物（I）进行热处理，并进一步通过选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及使用至少一种酸来纯化至少包含（I）的组合物一种具有7-16个碳原子的环酮，通过组合物（I）与酸的热处理。

4. 发明申请

US20090326277A1 METHOD FOR PURIFYING CYCLIC KETONES 有权
标题翻译：纯化循环克隆的方法
公开(公告)号：US20090326277A1
公开(公告)日：2009-12-31
申请号：US12306807
申请日：2007-06-27
申请人： Rolf Pinkos , Gerd Tebben , Alexander Hauk , Christian Müller , Harald Rust
发明人： Rolf Pinkos , Gerd Tebben , Alexander Hauk , Christian Müller , Harald Rust
IPC分类号： C07C45/00
CPC分类号： C07C45/85 , C07C45/33 , C07C45/34 , C07C45/58 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C49/413 , C07C49/607
摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with at least one acid and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization, Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one acid for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with the acid.
摘要翻译：本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用至少一种酸对组合物（I）进行热处理，并进一步通过选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及使用至少一种酸来纯化至少包含（I）的组合物一种具有7-16个碳原子的环酮，通过组合物（I）与酸的热处理。

5. 发明申请

US20090326276A1 METHOD FOR THE PRODUCTION OF CYCLIC KETONES 失效
标题翻译：生产环状酮的方法
公开(公告)号：US20090326276A1
公开(公告)日：2009-12-31
申请号：US12306827
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Rößler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Joaquim Henrique Teles , Beatrice Rößler , Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/80 , C07C45/81 , C07C45/82 , C07C45/85 , C07C2601/18 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps(a) oxidation of a composition (I) comprising at least one cyclic alkene which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A),(b) treatment of the composition (A) with at least one base to give a composition (B),(c) hydrogenation of the composition (B) in the presence of at least one catalyst to give a composition (C),(d) purification of the composition (C), comprising at least the steps(di) thermal treatment of the composition (C) with at least one acid or at least one catalyst comprising at least one transition metal,(dii) further purification by a method selected from the group consisting of distillation, extraction and crystallization.
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）氧化包含至少一个具有7至16个碳原子的环烯烃的组合物（I）和至少一个CC双键，得到组合物（A），（b）用至少一种碱处理组合物（A），得到组合物（B），（c）组合物的氢化（B）在至少一种催化剂的存在下，得到组合物（C），（d）组合物（C）的纯化，至少包括步骤（ii）组合物（C）的热处理至少一种酸或至少一种包含至少一种过渡金属的催化剂，（dii）通过选自蒸馏，萃取和结晶的方法进一步纯化。

6. 发明申请

US20090318733A1 METHOD FOR PURIFYING CYCLIC KETONES 有权
标题翻译：纯化循环克隆的方法
公开(公告)号：US20090318733A1
公开(公告)日：2009-12-24
申请号：US12306815
申请日：2007-06-27
申请人： Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
发明人： Rolf Pinkos , Gerd Tebben , Christian Müller , Harald Rust
IPC分类号： C07C45/78
CPC分类号： C07C45/85 , C07C45/34 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with a catalyst comprising at least one transition metal and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization. Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one catalyst comprising at least one transition metal for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with a catalyst comprising at least one transition metal.
摘要翻译：本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用包含至少一种过渡金属的催化剂热处理组合物（I）并进一步纯化通过选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及至少一种包含至少一种过渡金属的催化剂用于纯化组合物（I）的用途，所述组合物（I）包含至少一种具有7〜 16个碳原子通过用包含至少一种过渡金属的催化剂热处理组合物（I）。

7. 发明申请

US20090281357A1 METHOD FOR THE PRODUCTION OF CYCLIC KETONES 失效
标题翻译：生产环状酮的方法
公开(公告)号：US20090281357A1
公开(公告)日：2009-11-12
申请号：US12306841
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Rössler , Rolf Pinkos , Gerd Tebben , Christian Müller
发明人： Joaquim Henrique Teles , Beatrice Rössler , Rolf Pinkos , Gerd Tebben , Christian Müller
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/85 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic olefin which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B).
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）包含至少一种具有7至16个碳原子的环烯烃的组合物（I）的氧化和至少一个CC双键，得到组合物（A），（b）用至少一个碱处理组合物（A）以得到组合物（B）。

8. 发明授权

US07649119B2 Method for the production of cyclic ketones 失效
标题翻译：环酮生产方法
公开(公告)号：US07649119B2
公开(公告)日：2010-01-19
申请号：US12306841
申请日：2007-06-27
申请人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller
发明人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Gerd Tebben , Christian Müller
IPC分类号： C07C45/27
CPC分类号： C07C45/28 , C07C45/62 , C07C45/85 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing a cyclic ketone having from 7 to 16 carbon atoms, which comprises at least the steps (a) oxidation of a composition (I) comprising at least one cyclic olefin which has from 7 to 16 carbon atoms and at least one C—C double bond by means of dinitrogen monoxide to give a composition (A), (b) treatment of the composition (A) with at least one base to give a composition (B).
摘要翻译：本发明涉及一种制备具有7至16个碳原子的环酮的方法，其至少包括步骤（a）包含至少一种具有7至16个碳原子的环烯烃的组合物（I）的氧化和至少一个CC双键，得到组合物（A），（b）用至少一个碱处理组合物（A）以得到组合物（B）。

9. 发明申请

US20100168445A1 PROCESS FOR PREPARING EPSILON-CAPROLACTONE 审中-公开
标题翻译：制备EPSILON-CAPROLACTONE的方法
公开(公告)号：US20100168445A1
公开(公告)日：2010-07-01
申请号：US12602837
申请日：2008-06-06
申请人： Rolf Pinkos , Gerd Tebben , Christophe Bauduin , Daniel Breuninger , Maria Guixa Guardia , Tilman Sirch , Thomas Krug
发明人： Rolf Pinkos , Gerd Tebben , Christophe Bauduin , Daniel Breuninger , Maria Guixa Guardia , Tilman Sirch , Thomas Krug
IPC分类号： C07D313/04
CPC分类号： C07D313/04
摘要： The present invention provides a process for preparing ε-caprolactone in a purity above 99%, in which 6-hydroxycaproic ester comprising from 0.5 to 40% by weight of adipic diester is cyclized in the gas phase at from 150 to 450° C. in the presence of oxidic catalysts and ε-caprolactone is obtained from the cyclization product by distillation.
摘要翻译：本发明提供了一种制备纯度高于99％的己内酯的方法，其中包含0.5至40重量％的己二酸二酯的6-羟基己酸酯在150至450℃的气相中环化。在氧化催化剂的存在下，通过蒸馏从环化产物得到ε-己内酯。

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