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1. 发明专利

JPS58197314A Fibrous carbon 失效
标题翻译：纤维素
公开(公告)号：JPS58197314A
公开(公告)日：1983-11-17
申请号：JP7750082
申请日：1982-05-11
申请人： Morinobu Endo
发明人： ENDOU MORINOBU , KOYAMA TSUNEO
IPC分类号： D01F9/12 , D01F9/127
摘要： PURPOSE: Fibrous carbon that consists of the core part with a form that carbon hexagonal network surfaces like truncated cone vessels are piled up and of the peripheral layer where the carbon hexagonal surfaces are arranged annularly, thus having a novel shape suitable for use as an electric material.
CONSTITUTION: The oil bath 1 is controlled in its temperature and the starting material such as benzene is vaporized 2, mixed with an inert carrier gas and introduced into an electric oven 3 where a plate or cylindrical base of carbon containing volatile hydrocarbons is placed. The temperature in the electric oven 3 is changed to produce fibrous carbon consisting of two layers, the core that has such a shape as carbon hexagonal surfaces like truncated cone vessels are piled up and the periphery where the carbon hexagonal network surfaces are arranged annularly.
EFFECT: It has a tendency to form easily an interlaminar compound with a reductive substance such as alkali metal or an oxidative substance such as AsF
6 or halogen. The compound has high electroconductivity and is used as an electric material.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：将由碳六角形网状表面如圆锥形容器形成的核心部分和碳六角形表面环绕的外围层组成的纤维碳，因此具有适合用作电气的新颖形状材料。构成：将油浴1控制在其温度下，将诸如苯的原料蒸发2，与惰性载气混合并引入电炉3中，其中放置有含有挥发性碳氢化合物的碳板或圆柱形基底。电炉3中的温度被改变以产生由两层组成的纤维状碳，堆积有诸如截头圆锥体的碳六角形形状的芯和碳六角网状表面环形排列的周边。效果：易于形成具有还原性物质如碱金属或氧化物质如AsF 6或卤素的层间化合物的倾向。该化合物具有高导电性并用作电材料。

2. 发明专利

JPS58180615A Preparation of carbon fiber by vapor phase method 失效
标题翻译：通过蒸气相法制备碳纤维
公开(公告)号：JPS58180615A
公开(公告)日：1983-10-22
申请号：JP5896682
申请日：1982-04-10
申请人： Morinobu Endo , Tsuneo Koyama , Showa Denko Kk
发明人： ENDOU MORINOBU , KOYAMA TSUNEO
IPC分类号： D01F9/12 , D01F9/127 , D01F9/133
摘要： PURPOSE: To obtain carbon fibers in high yield with high productivity, by thermally decomposing a hydrocarbon in the presence of a floating ultrafine powder of a high-melting metal (or a compound thereof).
CONSTITUTION: A hydrocarbon and a carrier gas, e.g. H
2 , are introduced from an introductory pipe 4 into a reaction tube 1 heated at 950W1,300°C by a heater 2 in the direction of arrow (A), and an ultrafine powder of a high-melting metal (or a compound thereof), e.g. Fe, is simultaneously introduced from a nozzle 8 of a spray 3 into the reaction tube 1 by the injection of a volatile medium 7. In the reaction zone, the hydrocarbon is thermally decomposed to grow carbon fibers 10 in the presence of the floating ultrafine powder 9 as a catalyst, and the ultrafine powder is stuck to the resultant carbon fibers 10 and give the aimed branched carbon fibers 12. The floating branched carbon fibers 12 are then collected from an outlet pipe 5. On the other hand, the carbon fibers 11 dropped onto a substrate 6 continue the growing even on the substrate 6 and then are collected.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：以高产率高产率获得碳纤维，通过在高熔点金属（或其化合物）的漂浮超细粉末存在下热分解烃。构成：烃和载气，例如 H2通过加热器2沿着箭头（A）的方向从引入管4引入加热到950-1300℃的反应管1中，并且将高熔点金属（或其化合物）的超细粉末），例如 Fe通过喷射挥发性介质7同时从喷雾3的喷嘴8引入反应管1中。在反应区中，在浮选的超细粉末存在下，将烃热分解成碳纤维10 9作为催化剂，将超细粉末粘贴到所得碳纤维10上，得到目标的支化碳纤维12.然后从出口管5收集浮动的支链碳纤维12.另一方面，碳纤维11 落在基板6上，即使在基板6上继续生长，然后被收集。

3. 发明专利

JPS59179816A Graphite fiber forming interlaminar compound 失效
标题翻译：石墨纤维形成层间化合物
公开(公告)号：JPS59179816A
公开(公告)日：1984-10-12
申请号：JP5044283
申请日：1983-03-28
申请人： Morinobu Endo , Tsuneo Koyama , Showa Denko Kk
发明人： ENDOU MORINOBU , KOYAMA TSUNEO , IWAKI HIDEHIKO
IPC分类号： D01F9/12 , D01F9/127
摘要： PURPOSE: The titled graphite fiber forming high electrical conductivity comparable with metal, good wetting properties with metal, and stability in air, wherein FeCl
3 is penetrated into crystal face of graphite fiber having a concentric crystal structure to form an interlaminar compound.
CONSTITUTION: Graphite fiber and FeCl
3 are put in a glass tube, heated preferably at 250W400°C under reduced pressure, FeCl
3 is evaporated, and the interior of the tube is kept in an atmosphere of FeCl
3 gas, to give the desired graphite fiber wherein FeCl
3 is penetrated into crystal face of graphite fiber having a concentric crystal structure to form an interlaminar compound.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：形成与金属相当的高导电性，与金属具有良好的润湿性能和空气稳定性的标准石墨纤维，其中FeCl 3渗透到具有同心晶体结构的石墨纤维的晶面中以形成层间化合物。构成：将石墨纤维和FeCl 3放入玻璃管中，优选在250-400℃减压下加热，将FeCl 3蒸发，将管内保持在FeCl 3气体气氛中，得到所需的石墨纤维，其中FeCl 3渗透到具有同心晶体结构的石墨纤维的晶面中以形成层间化合物。

4. 发明专利

JPS5939527B2 JPS5939527B2 - 失效
公开(公告)号：JPS5939527B2
公开(公告)日：1984-09-25
申请号：JP315081
申请日：1981-01-14
申请人： Showa Denko Kk , Tsuneo Koyama , Morinobu Endo
发明人： ENDO MORINOBU , KOYAMA TSUNEO
IPC分类号： D06M11/00 , D01F9/12 , D01F9/127 , D06M11/36 , D06M11/74 , D06M11/83 , D06M23/08 , D06M101/00 , D06M101/40

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