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1. 发明申请

WO2007004848A1 AROMATIC POLYAMIDE FILAMENT AND METHOD OF MANUFACTURING THE SAME 审中-公开
标题翻译：芳香族聚酰胺纤维及其制造方法
公开(公告)号：WO2007004848A1
公开(公告)日：2007-01-11
申请号：PCT/KR2006/002624
申请日：2006-07-05
申请人： KOLON INDUSTRIES, INC , HAN, In-Sik , LEE, Jae-Young , LEE, Seung-Hwan , KIM, Jae-Young , KWON, So-Yeon
发明人： HAN, In-Sik , LEE, Jae-Young , LEE, Seung-Hwan , KIM, Jae-Young , KWON, So-Yeon
IPC分类号： D01F6/60
CPC分类号： D01F6/605 , D01D5/06 , Y02P20/582 , Y10T428/2913 , Y10T428/2969
摘要： Disclosed are wholly aromatic polyamide filament and a method of manufacturing the same, characterized by comprising multi-stage injection of a coagulant with sulfuric acid concentration lowered sequentially stage by stage, to a spun material fed into a coagulant injection tank. The present invention enables increase of a spinning and take-up velocity without occurrence of thread cutting by uniformly and evenly coagulating surface and inside of the spun material. In addition, the present invention recovers the coagulant or water already used and reuses the recovered coagulant or water in the earlier stages, so that it has advantages of saving production costs and reducing environmental contamination. Accordingly, the wholly aromatic polyamide filament produced according to the present invention has high crystallinity X, large apparent crystal size ACS and reduced defects in the crystal itself, thereby exhibiting more improved physical properties such as strength and modulus.
摘要翻译：公开了全芳香族聚酰胺长丝及其制造方法，其特征在于，包括多阶段将硫酸浓度逐级降低的凝结剂注入供给到凝结剂注入槽中的纺丝材料。本发明通过使纺丝材料的表面和内部均匀均匀地凝固，能够提高纺丝和卷取速度，而不会产生螺纹切割。此外，本发明回收已经使用的凝结剂或水，并且在早期阶段重新使用回收的凝结剂或水，从而具有节省生产成本和减少环境污染的优点。因此，根据本发明生产的全芳族聚酰胺长丝具有高结晶度X，大的表观晶体尺寸ACS，并减少了晶体本身的缺陷，从而表现出更好的物理性能如强度和模量。

2. 发明申请

WO2009031869A2 CELLULOSE-BASED FIBER, AND TIRE CORD COMPRISING THE SAME 审中-公开
标题翻译：纤维素基纤维和包含该纤维的轮胎帘线
公开(公告)号：WO2009031869A2
公开(公告)日：2009-03-12
申请号：PCT/KR2008/005290
申请日：2008-09-08
申请人： KOLON INDUSTRIES, INC. , OH, Young-Se , KWON, So-Yeon , JEONG, Jong-Cheol , KIM, Woo-Chul , JEON, Ok-Hwa , CHUNG, Il , LEE, Jae-Woong , KIM, Gi-Woong
发明人： OH, Young-Se , KWON, So-Yeon , JEONG, Jong-Cheol , KIM, Woo-Chul , JEON, Ok-Hwa , CHUNG, Il , LEE, Jae-Woong , KIM, Gi-Woong
IPC分类号： D01F2/00 , D07B1/02
CPC分类号： D01F2/00 , D01F1/10 , D02G3/48 , D10B2201/20
摘要： The present invention provides cellulose-based fibers including cellulose and at least one polymer selected from the group consisting of a polysiloxane, a polyacrylic acid, a polyacrylamide, an m-aramid, and a poly vinylalcohol/ polystyrene copolymer, and a tire cord including the same. Furthermore, the cellulose-based fibers of the present invention have an advantage in superior elongation and tenacity of the prior cellulose fibers by blending at least one polymer having a functional group that is capable of a hydrogen bond with a hydroxyl group of a cellulose molecule.
摘要翻译：本发明提供了包含纤维素和至少一种选自聚硅氧烷，聚丙烯酸，聚丙烯酰胺，间芳族聚酰胺和聚乙烯醇/聚苯乙烯的聚合物的纤维素基纤维共聚物和包含其的轮胎帘线。此外，本发明的纤维素基纤维通过将至少一种具有能够形成氢键的官能团的聚合物与纤维素分子的羟基共混，具有优异的现有纤维素纤维的伸长率和韧性的优点。

3. 发明申请

WO2009031868A2 LYOCELL FILAMENT FIBER AND CELLULOSE BASED TIRE CORD 审中-公开
标题翻译： LYOCELL长丝纤维和纤维素基轮胎帘线
公开(公告)号：WO2009031868A2
公开(公告)日：2009-03-12
申请号：PCT/KR2008/005289
申请日：2008-09-08
申请人： KOLON INDUSTRIES, INC. , KIM, Gi-Woong , KWON, So-Yeon , JEON, Ok-Hwa , OH, Young-Se , JEONG, Jong-Cheol , KIM, Woo-Chul , CHUNG, Il , LEE, Jae-Woong
发明人： KIM, Gi-Woong , KWON, So-Yeon , JEON, Ok-Hwa , OH, Young-Se , JEONG, Jong-Cheol , KIM, Woo-Chul , CHUNG, Il , LEE, Jae-Woong
IPC分类号： D01F2/00 , D02G3/48
CPC分类号： D01F2/00 , B60C9/0042 , D01D10/06 , D02G3/48 , D10B2201/00
摘要： The present invention relates to lyocell filament fibers and a cellulose-based tire cord, and particularly to lyocell filament fibers of which the swelling anisotropy defined in the specification is 1.1 to 1.4. Furthermore, the present invention provides a cellulose based tire cord of which the swelling anisotropy is 1.1 to 1.4. According to the present invention, there is an effect of providing the lyocell filament fibers and the cellulose based tire cord of which the dimensional stability in a highly humid state is particularly good and thus the tenacity, the elongation, and the modulus are superior to common cellulose based fibers, such as rayon and so on, the property maintaining rate at the post manufacturing process is high, and the processibility is good.
摘要翻译：本发明涉及莱赛尔纤维长丝纤维和纤维素基轮胎帘线，并且特别涉及其在说明书中定义的膨胀各向异性为1.1至1.4的莱赛尔纤维长丝纤维。此外，本发明提供膨胀各向异性为1.1〜1.4的纤维素类轮胎帘线。根据本发明，具有提供在高湿度状态下的尺寸稳定性特别良好并且因此韧性，伸长率和模量优于普通的莱赛尔长丝纤维和纤维素基轮胎帘线的效果纤维素基纤维如人造丝等，后制造过程中的性能维持率高，加工性好。

4. 发明申请

WO2009028919A3 PREPARATION METHOD FOR LYOCELL FILAMENT FIBERS, LYOCELL FILAMENT FIBERS, TIRE CORD, AND PREPARATION METHOD FOR TIRE CORD 审中-公开
公开(公告)号：WO2009028919A3
公开(公告)日：2009-03-05
申请号：PCT/KR2008/005126
申请日：2008-09-01
申请人： KOLON INDUSTRIES, INC. , OH, Young-Se , KWON, So-Yeon , JEONG, Jong-Cheol , KIM, Woo-Chul , JEON, Ok-Hwa , CHUNG, Il , LEE, Jae-Woong , KIM, Gi-Woong
发明人： OH, Young-Se , KWON, So-Yeon , JEONG, Jong-Cheol , KIM, Woo-Chul , JEON, Ok-Hwa , CHUNG, Il , LEE, Jae-Woong , KIM, Gi-Woong
IPC分类号： D01F2/00 , D07B1/02
摘要： The present invention relates to a method of preparing lyocell filament fibers, and lyocell filament fibers. More particularly, the present invention relates to a method of preparing lyocell filament fibers using a solidifying bath of 30 to 60 0C in the step of solidifying the filaments, lyocell filament fibers, and a tire cord including the same. Furthermore, the present invention relates to a tire cord and a method of preparing the same. More particularly, the present invention relates to a tire cord including a twisted yarn of lyocell filament fibers and an adhesive, wherein the pick up rate of the adhesive is 6 to 10 wt%, and the degree of fatigue resistance is 70% or more at the fatigue condition of extension and contraction of +2% according to the ASTM D 6588 method by using a disk fatigue tester. The lyocell filament fibers according to the present invention show a dense structure advantageous for providing good elongation and make penetration of the dipping solution easy during preparing the tire cord, and the fatigue property and fatigue resistance are good, owing to the proper pick up rate of the adhesive, and thus there is an effect of improving the durability and safety of the tire.

5. 发明申请

WO2009028918A2 LYOCELL FILAMENT FIBERS AND TIRE CORD USING THE SAME 审中-公开
标题翻译： LYOCELL长丝纤维和使用该纤维的轮胎帘线
公开(公告)号：WO2009028918A2
公开(公告)日：2009-03-05
申请号：PCT/KR2008/005124
申请日：2008-09-01
申请人： KOLON INDUSTRIES, INC. , KIM, Gi-Woong , KWON, So-Yeon , JEON, Ok-Hwa , OH, Young-Se , JEONG, Jong-Cheol , KIM, Woo-Chul , CHUNG, Il , LEE, Jae-Woong
发明人： KIM, Gi-Woong , KWON, So-Yeon , JEON, Ok-Hwa , OH, Young-Se , JEONG, Jong-Cheol , KIM, Woo-Chul , CHUNG, Il , LEE, Jae-Woong
IPC分类号： D01F2/00 , D07B1/02
CPC分类号： D01F2/00 , B60C1/0008 , B60C9/0042 , D02G3/48 , D10B2201/20
摘要： The present invention is relates to lyocell filament fibers having fatigue resistance and durability, of which the dimensional stability at high temperature and the high speed driving performance are good, and a tire cord prepared therefrom.
摘要翻译：本发明涉及具有耐疲劳性和耐久性的莱塞尔长丝纤维以及由其制备的轮胎帘线，其中高温尺寸稳定性和高速驱动性能良好。 >

6. 发明申请

WO2008153241A1 LYOCELL FIBER FOR TIRE CORD AND TIRE CORD COMPRISING THE SAME 审中-公开
标题翻译：用于轮胎线的LYOCELL纤维和包含该轮胎的轮胎绳
公开(公告)号：WO2008153241A1
公开(公告)日：2008-12-18
申请号：PCT/KR2007/004276
申请日：2007-09-05
申请人： KOLON INDUSTRIES, INC. , KWON, So-Yeon , OH, Young-Se , JEONG, Jong-Cheol
发明人： KWON, So-Yeon , OH, Young-Se , JEONG, Jong-Cheol
IPC分类号： D01F2/02
CPC分类号： D01F2/00 , D01D5/06 , D01D10/06 , D02G3/48
摘要： The present invention relates to a lyocell fiber having superior the crystalline properties, which are measured by wet-treated and dry-treated condition under high temperature and high pressure conditions compared to measurement under standard conditions, and to a tire cord comprising the lyocell fiber. According to the present invention, the lyocell fiber has strength, elongation, and modulus that are superior to those of a conventional rayon, even when the lyocell fiber is wet- and dry-treated under high temperature and high pressure conditions by specifying water-washing conditions of a spinning machine, thereby improving dimensional stability of a tire cord when it is applied to the tire cord.
摘要翻译：本发明涉及具有优异的结晶性能的莱赛尔纤维，其与在标准条件下的测量相比，在高温高压条件下通过湿处理和干燥处理条件以及包含莱赛尔纤维的轮胎帘线测量。根据本发明，即使当在高温和高压条件下通过指定水洗将溶胞干燥纤维进行湿干和干燥处理时，莱赛尔纤维的强度，伸长率和模量优于传统的人造丝纺纱机的条件，从而在将轮胎帘线施加到轮胎帘线时提高轮胎帘线的尺寸稳定性。

7. 发明申请

WO2008153240A1 LYOCELL FIBER FOR TIRE CORD AND TIRE CORD COMPRISING THE SAME 审中-公开
标题翻译：用于轮胎线的LYOCELL纤维和包含该轮胎的轮胎绳
公开(公告)号：WO2008153240A1
公开(公告)日：2008-12-18
申请号：PCT/KR2007/004254
申请日：2007-09-04
申请人： KOLON INDUSTRIES, INC. , OH, Young-Se , KWON, So-Yeon , JEONG, Jong-Cheol
发明人： OH, Young-Se , KWON, So-Yeon , JEONG, Jong-Cheol
IPC分类号： D01F2/02
CPC分类号： D01F2/00 , B60C9/0042 , D01D5/06 , D01D10/06 , D02G3/48
摘要： The present invention relates to a lyocell fiber to which is performed a wet-treatment under a saturation vapor pressure state for 10 minutes at a temperature of 120¡É and then subsequently a dry-treatment for 2 hours at a temperature of 130¡É, wherein the strength of the lyocell fiber is higher than the strength of the untreated lyocell fiber, when measured under standard conditions, and to a tire cord comprising the lyocell fiber. According to the present invention, the lyocell fiber has strength, elongation, and modulus that are superior to those of a conventional rayon even when the lyocell fiber is wet- and dry-treated under high temperature and high pressure conditions by specifying a water-washing condition of a spinning machine, thereby improving dimensional stability of a tire cord when it is applied to the tire cord.
摘要翻译：本发明涉及在120℃的温度下在饱和蒸汽压状态下进行10分钟的湿法处理的莱赛尔纤维，然后在130℃的温度下干燥2小时，其中当在标准条件下测量时，莱赛尔纤维的强度高于未处理的莱赛尔纤维的强度，以及包含莱赛尔纤维的轮胎帘线。根据本发明，即使当在高温和高压条件下湿乳化和干法处理乳清纤维时，通过指定水洗，莱赛尔纤维的强度，伸长率和模量优于常规人造纤维纺纱机的状态，从而提高轮胎帘线施加到轮胎帘线时的尺寸稳定性。

8. 发明申请

WO2008030045A1 METHOD OF MANUFACTURING WHOLLY AROMATIC POLYAMIDE FILAMENT AND WHOLLY AROMATIC POLYAMIDE FILAMENT MANUFACTURED THEREBY 审中-公开
标题翻译：制造芳香族聚酰胺纤维的方法和制造的芳香族聚酰胺纤维
公开(公告)号：WO2008030045A1
公开(公告)日：2008-03-13
申请号：PCT/KR2007/004303
申请日：2007-09-06
申请人： KOLON INDUSTRIES, INC , KWON, So-Yeon
发明人： KWON, So-Yeon
IPC分类号： D01F6/60
CPC分类号： D01F6/605 , D01D1/02 , Y10T428/2913
摘要： Disclosed are a method of manufacturing wholly aromatic polyamid filaments and wholly aromatic polyamid filaments produced by the same. The present inventive process comprises control of a timing for introducing wholly aromatic polyamid polymer into an extruder for preparation of a spinning dope based on particle size and/or inherent viscosity (IV) of the polyamid polymer. The present invention can significantly reduce brittleness of the wholly aromatic polyamid polymer due to a sulfuric acid solvent during preparation of the spinning dope so as to improve strength and, especially, side impact strength of the wholly aromatic polyamid filaments and can also use even polymers with lower IVs which are necessarily generated during the polymerization, thereby reducing production costs of the polyamid filaments.
摘要翻译：公开了制造全芳族聚酰胺长丝和由其制造的全芳族聚酰胺长丝的方法。本发明的方法包括基于聚酰胺聚合物的粒度和/或特性粘度（IV）来控制将全芳族聚酰胺聚合物引入用于制备纺丝原液的挤出机中的时间。本发明可以在制备纺丝原液时由于硫酸溶剂而显着降低全芳族聚酰胺聚合物的脆性，从而提高全芳族聚酰胺长丝的强度，特别是侧面冲击强度，并且还可以使用甚至具有在聚合期间必然产生的较低的IV，从而降低聚酰胺长丝的生产成本。

9. 发明申请

WO2007004851A1 AROMATIC POLYAMIDE FILAMENT AND METHOD OF MANUFACTURING THE SAME 审中-公开
标题翻译：芳香族聚酰胺纤维及其制造方法
公开(公告)号：WO2007004851A1
公开(公告)日：2007-01-11
申请号：PCT/KR2006/002627
申请日：2006-07-05
申请人： KOLON INDUSTRIES, INC. , HAN, In-Sik , LEE, Jae-Young , KIM, Jae-Young , PARK, Tae-Hak , KWON, So-Yeon
发明人： HAN, In-Sik , LEE, Jae-Young , KIM, Jae-Young , PARK, Tae-Hak , KWON, So-Yeon
IPC分类号： D01F6/60
CPC分类号： D01F6/605 , B01F7/00766 , B01F2215/0454 , C08G69/32 , Y10T428/2913 , Y10T428/2969
摘要： Disclosed are wholly aromatic polyamide filament and a method of manufacturing the same, characterized in that, in the process of preparing the wholly aromatic polyamide polymer, the aromatic diamine, aromatic diacid chlrodie and polymerization solvent put into the reactor (20) are agitated by an agitation device which is installed in the reactor (20) and consists of: (i) a rotor (3) driven by a motor (2) and having a plurality of pins (3a); and (ii) a stator (4) having a plurality of pins (4a), wherein spin speed of the rotor (3) is controlled to 10 to 100 times of both of feeding rates for the aromatic diacid chloride and the aromatic diamine in the polymerization solvent into the reactor and, at the same time, contact frequency between the pins (3a) and the pins (4a) is regulated within a range of 100 to 1,000 Hz. The present invention is effective to progress uniform and homogeneous polymerization over all of area of a polymerization reactor (20), thereby reducing deviation in degree of polymerization, since polymeric monomers are miscible and react together very well in the reactor (20). Accordingly, the wholly aromatic polyamide filament produced exhibits narrow PDI and lowered paracrystalline parameter gπ leading to reduction of defects of a crystal itself, so as to considerably improve strength and modulus thereof.
摘要翻译：公开了全芳族聚酰胺长丝及其制造方法，其特征在于，在制备全芳香族聚酰胺聚合物的过程中，将放入反应器（20）中的芳族二胺，芳族二酸氯乙烯和聚合溶剂搅拌搅拌装置，其安装在所述反应器（20）中并且包括：（i）由电动机（2）驱动并具有多个销（3a）的转子（3）; 和（ii）具有多个销（4a）的定子（4），其中转子（3）的旋转速度被控制在芳族二酰氯和芳族二胺的进料速率的10到100倍聚合溶剂进入反应器，并且同时，引脚（3a）和引脚（4a）之间的接触频率调节在100至1,000Hz的范围内。本发明有效地在聚合反应器（20）的所有区域上进行均匀均匀的聚合，从而减少聚合度的偏差，因为聚合单体是可混溶的并且在反应器（20）中非常好地一起反应。因此，所制备的全芳族聚酰胺长丝表现出窄的PDI和降低的结晶参数gp，导致晶体本身缺陷的减少，从而显着提高其强度和模量。

10. 发明申请

WO2007004849A1 AROMATIC POLYAMIDE FILAMENT AND METHOD OF MANUFACTURING THE SAME 审中-公开
标题翻译：芳香族聚酰胺纤维及其制造方法
公开(公告)号：WO2007004849A1
公开(公告)日：2007-01-11
申请号：PCT/KR2006/002625
申请日：2006-07-05
申请人： KOLON INDUSTRIES, INC. , HAN, In-Sik , LEE, Jae-Young , LEE, Seung-Hwan , LEE, Chang-Bae , KWON, So-Yeon
发明人： HAN, In-Sik , LEE, Jae-Young , LEE, Seung-Hwan , LEE, Chang-Bae , KWON, So-Yeon
IPC分类号： D01F6/60
CPC分类号： D01F6/605 , Y10T428/2913 , Y10T428/2969
摘要： Disclosed are wholly aromatic polyamide filament and a method of manufacturing the same, characterized in that, in a process of preparing wholly aromatic polyamide polymer, a multiple tubular feed pipe for polymeric monomer and polymerization solvent with specific construction of adjacent inner paths (11a) and outer paths (11b) which are alternately arranged one another is used to feed either aromatic diacid chloride A or aromatic diamine dissolved in the polymerization solvent B into a polymerization reactor (20) through corresponding one among the inner and outer paths (11a) and (l1b). The present invention is effective to progress uniform and homogeneous polymerization over all of area of a polymerization reactor (20) leading to reduction of deviation in degree of polymerization, since polymeric monomers are miscible and react together very well immediately after putting the monomers into the reactor (20). Accordingly, the wholly aromatic polyamide filament produced exhibits narrow PDI and increased ACS, so as to considerably improve strength and modulus thereof.
摘要翻译：公开了全芳族聚酰胺长丝及其制造方法，其特征在于，在制备全芳族聚酰胺聚合物的方法中，用于聚合单体的多管式进料管和具有相邻内部通道（11a）和将彼此交替排列的外部路径（11b）用于将溶解在聚合溶剂B中的芳族二酰氯A或芳族二胺通过内部和外部路径（11a）和（11a）中的相应的一个进入聚合反应器（20） L1B）。本发明有效地在聚合反应器（20）的所有区域上进行均匀均匀的聚合，从而导致聚合度偏差的降低，因为聚合单体是可混溶的，并且在将单体放入反应器之后立即非常好地反应（20）。因此，所生产的全芳族聚酰胺长丝表现出窄的PDI和增加的ACS，从而显着提高其强度和模量。

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