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1. 发明授权

US4055599A N-(Alkylhydrobenzyl)-alkylthio- and mercapto-acetamides 失效
标题翻译： N-（烷基氢苄基） - 烷硫基 - 和巯基 - 乙酰胺
公开(公告)号：US4055599A
公开(公告)日：1977-10-25
申请号：US611043
申请日：1975-09-08
申请人： Helmut Huber-Emden , Karl Eschle , Arthur Maeder
发明人： Helmut Huber-Emden , Karl Eschle , Arthur Maeder
IPC分类号： C07C323/52 , C07C335/32 , C07D307/38 , C08K5/378 , C09K15/28 , C10L1/24 , C11B5/00 , C07C103/38
CPC分类号： C07D307/38 , C07C323/52 , C07C335/32 , C08K5/378 , C09K15/28 , C10L1/2406 , C11B5/0071
摘要： The present invention provides carboxylic acid amides of the formula ##STR1## in which X represents methyl or tertiary butyl, m is the integer 1 or 2, Q represents hydrogen, alkyl, alkylidene, cycloalkylidene, substituted methylene, alkylene, alkenylene or a 3,4,5 or 6-valent saturated aliphatic hydrocarbon radical and p represents an integer which corresponds to the valency of the radical Q. These carboxylic acid amides are suitable for stabilizing organic materials sensitive to oxidations.
摘要翻译：本发明提供了式“IMAGE”的羧酸酰胺，其中X代表甲基或叔丁基，m是整数1或2，Q代表氢，烷基，亚烷基，环亚烷基，取代的亚甲基，亚烷基，亚烯基或3， 4,5或6价饱和脂族烃基，p表示对应于基团Q的化合价的整数。这些羧酸酰胺适用于稳定对氧化敏感的有机材料。

2. 发明授权

US4052485A Perfluoro compounds containing phosphorus 失效
标题翻译：含有磷酸盐的全氟化合物
公开(公告)号：US4052485A
公开(公告)日：1977-10-04
申请号：US227661
申请日：1972-02-18
申请人： Helmut Huber-Emden
发明人： Helmut Huber-Emden
IPC分类号： C07F9/09 , C07F9/14 , C07F9/40 , C07F9/42 , D06M13/282 , D06M15/333
CPC分类号： C07F9/40 , C07F9/09 , C07F9/14 , C07F9/42 , D06M13/282 , D06M15/333 , Y10T442/227
摘要： Perfluoro compounds containing dichloro phosphoryl and/or dichlorophosphoryl radicals are provided which are obtained by reacting perfluoroalkylalkenes with phosphorus trichloride in the presence of oxygen. The compounds are useful to obtain oleophobic finishes on various substrates, especially on fibrous materials.

3. 发明授权

US4990164A Process for the photochemical stabilization of undyed and dyed polyamide fibre material and blends thereof with copper complex of hydroxy-salicyl-oyl-hydroxylamine derivative 失效
标题翻译：未染色和染色的聚酰胺纤维材料的光化学稳定性及其与羟基 - 水杨基 - 羟基 - 羟胺衍生物的铜络合物的共混物的方法
公开(公告)号：US4990164A
公开(公告)日：1991-02-05
申请号：US413370
申请日：1989-09-27
申请人： Helmut Huber-Emden , Gerhard Reinert
发明人： Helmut Huber-Emden , Gerhard Reinert
IPC分类号： D06M13/02 , D06M13/152 , D06M13/322 , D06M13/376 , D06M13/50 , D06M13/503 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/34 , D06P1/642 , D06P3/24
CPC分类号： D06P3/241 , D06M13/503 , D06P1/6423 , Y10S8/924 , Y10S8/926
摘要： A process is described for the photochemical stabilization of undyed and dyed polyamide fibre material, and blends thereof with other fibres, using photochemically stabilizing compositions based on copper compounds of phenols, which process comprises treating the polyamide fibre material with fibre-reactive organic copper complexes of the reaction products of o-hydroxybenzoyl derivatives of the formula ##STR1## wherein R is hydrogen or C.sub.1 -C.sub.4 alkyl and the OH substituent is located in the 3-, 4- or 5-position, with aliphatic diamines or hydroxylamine. The copper complex compounds are distinguished by a high rate of exhaustion on to the polyamide fibre material, a feature which is significant in economic terms because of the low consumption of product.
摘要翻译：描述了使用基于酚化合物的光化学稳定化组合物对未染色和染色的聚酰胺纤维材料的光化学稳定性及其与其它纤维的共混物的方法，该方法包括用纤维反应性有机铜络合物处理聚酰胺纤维材料其中R是氢或C 1 -C 4烷基和OH取代基的式“IMAGE”（1）的邻羟基苯甲酰基衍生物与脂族二胺或羟胺位于3-，4-或5-位。铜络合物的特征在于聚酰胺纤维材料的高耗尽率，这是由于产品消耗低而在经济上显着的特征。

4. 发明授权

US4655785A Process for photochemical stabilization of polyamide and polyurethane fiber materials with metal complex compounds 失效
标题翻译：用金属络合物进行聚酰胺和聚氨酯纤维材料的光化学稳定化工艺
公开(公告)号：US4655785A
公开(公告)日：1987-04-07
申请号：US736927
申请日：1985-05-21
申请人： Gerhard Reinert , Gerhard Back , Helmut Huber-Emden
发明人： Gerhard Reinert , Gerhard Back , Helmut Huber-Emden
IPC分类号： C07F1/08 , C07C243/38 , C07C309/49 , C07F13/00 , C07F15/04 , C09B55/00 , D06M13/02 , D06M13/322 , D06M13/50 , D06M13/503 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36 , D06P1/62 , D06P1/642 , D06P3/24 , D06P3/26 , D06P5/00 , D06P5/06 , D06P5/10 , D06P1/64
CPC分类号： D06P3/26 , C07C243/38 , C09B55/007 , D06M13/503 , D06P1/6423 , D06P3/241 , Y10S8/924 , Y10S8/926
摘要： A process for the photochemical stabilization of undyed and dyed polyamide or polyurethane fibre material that is characterized in that the fibre material is treated with a water soluble, organic copper, manganese or nickel complex that displays an affinity for the fibres. The polyamide or polyurethane fibre material, e.g., textile, that has been so treated retains its stretch characteristics and elasticity even after prolonged periods of illumination. In addition, in the case of dyed material, treatment with the metal complex results in a marked improvement in light-fastness.
摘要翻译：一种用于未染色和染色的聚酰胺或聚氨酯纤维材料的光化学稳定的方法，其特征在于纤维材料用对纤维显示亲和力的水溶性有机铜，锰或镍络合物处理。已经如此处理的聚酰胺或聚氨酯纤维材料，例如纺织品即使在长时间的照明之后也保持其拉伸特性和弹性。此外，在染色材料的情况下，用金属络合物的处理导致耐光性显着提高。

5. 发明授权

US4655783A Process for photochemical stabilization of non-dyed and dyed polyamide fibre material and mixtures thereof 失效
标题翻译：非染色和染色的聚酰胺纤维材料及其混合物的光化学稳定化方法
公开(公告)号：US4655783A
公开(公告)日：1987-04-07
申请号：US797098
申请日：1985-11-12
申请人： Gerhard Reinert , Helmut Huber-Emden , Gerhard Back
发明人： Gerhard Reinert , Helmut Huber-Emden , Gerhard Back
IPC分类号： C07F1/00 , D06M13/51 , D06P1/642 , D06P3/24 , D06P5/02 , D06M9/00 , D06P3/82
CPC分类号： D06M13/51 , C07F1/005 , D06P1/6423 , D06P3/241 , D06P5/02 , Y10S8/924 , Y10S8/926
摘要： A process for photochemical stabilization of non-dyed and dyed polyamide fibre material and mixtures thereof with other fibres which comprises treating the fibre material with a fibre-reactive copper complex of bisazomethines prepared from, for example, salicylaldehydes and aliphatic diamines is described. Some of these copper complexes used are novel compounds. The polyamide fibre material, for example textile material, thus treated largely retains its extensibility and elasticity even after relatively prolonged exposure to light. In addition, a clear improvement in light-fastness is achieved in dyed material by treatment with the metal complex.
摘要翻译：描述了非染色和染色的聚酰胺纤维材料及其与其它纤维的混合物的光化学稳定化方法，该方法包括用由例如水杨醛和脂族二胺制备的双偶氮甲碱的纤维反应性铜络合物处理纤维材料。所使用的这些铜络合物中的一些是新化合物。这样处理的聚酰胺纤维材料，例如纺织材料即使在相对长时间暴露于光线之后也大大地保持其延展性和弹性。此外，通过用金属络合物处理，在染色材料中实现了耐光性的明显改善。

6. 发明授权

US3996281A Fluorinated carboxylic acid amides and polymerization products thereof 失效
标题翻译：氟化羧酸酰胺及其聚合产物
公开(公告)号：US3996281A
公开(公告)日：1976-12-07
申请号：US547530
申请日：1975-02-06
申请人： Helmut Huber-Emden , Paul Schafer
发明人： Helmut Huber-Emden , Paul Schafer
IPC分类号： C08F20/60 , D06M15/285 , C07C103/133
CPC分类号： C08F20/60 , D06M15/285 , C10M2215/08 , C10M2215/082 , C10M2215/28
摘要： New fluorinated carboxylic acid amides of the formula ##STR1## are provided wherein R.sub.f is a perfluoroalkyl radical with 1 to 18 carbon atoms, R is hydrogen or methyl, R.sub.1 is hydrogen or R.sub.f CHOHCHR--, if m is 1, and hydrogen, alkyl with 1 to 18 carbon atoms, cycloalkyl with 5 or 6 carbon atoms, hydroxyalkyl with 2 to 6 carbon atoms, alkoxyalkyl with 1 to 4 carbon atoms in the alkoxy moiety or R.sub.f CHOHCHR--, if m is 0, A is an ethylenically unsaturated hydrocarbon radical with 2 or 3 carbon atoms, m is 0 or 1, y is 1 or 2 and p is an integer from 2 to 6. The fluorinated carboxylic acid amides are useful e.g. as wetting agents, emulsifiers or dispersants and for producing oil-repellent finishes on porous or nonporous substrates or as intermediates for the manufacture of homo- or copolymers, which show also oil-repellent properties.
摘要翻译：提供式（1）的新的氟化羧酸酰胺，其中Rf是具有1至18个碳原子的全氟烷基，R是氢或甲基，R1是氢或RfCHOHCHR-，如果m是1，具有1至18个碳原子的烷基，具有5或6个碳原子的环烷基，具有2至6个碳原子的羟烷基，烷氧基部分中具有1至4个碳原子的烷氧基烷基或RfCHOHCHR-，如果m为0，则A为烯属不饱和烃具有2或3个碳原子的基团，m为0或1，y为1或2，p为2至6的整数。氟化羧酸酰胺可用于例如作为润湿剂，乳化剂或分散剂，并用于在多孔或无孔基材上生产防油整理剂，或作为制备均聚物或共聚物的中间体，其也显示出拒油性能。

7. 发明授权

US3952060A Perfluorinated amino compounds and process for their manufacture 失效
标题翻译：全氟化氨基化合物及其制造方法
公开(公告)号：US3952060A
公开(公告)日：1976-04-20
申请号：US522541
申请日：1974-11-11
申请人： Helmut Huber-Emden , Alberto Deflorin
发明人： Helmut Huber-Emden , Alberto Deflorin
IPC分类号： B01F17/38 , B01F17/16 , C07C67/00 , C07C213/00 , C07C213/04 , C07C215/14 , C08G73/00 , C08G73/02 , C07C91/04
CPC分类号： C08G73/0206
摘要： New perfluorinated amino compounds of the formula ##EQU1## ARE PROVIDED WHEREIN R.sub.f represents a perfluorinated hydrocarbon radical with 1 to 18 carbon atoms and R represents hydrogen or methyl each of R.sub.1, R.sub.2 and R.sub.3 independently represents hydrogen or the radical ##EQU2## in which R.sub.f and R have the meanings already assigned to them, p is an integer from 2 to 6 and m is an integer from 1 to about 500.Due to their surface-active properties the new compounds are useful e.g as foaming, wetting and levelling agents or as emulsifiers. They can be further used as soil-repellent additives for polishes and waxes, as corrosion inhibitors in oils or lubricants and they are also useful as intermediates for the manufacture of oil and water repellents.
摘要翻译：新的全氟化氨基化合物式R f-CH-CH-N-（CH 2）p -N取代基R 1表示具有1至18个碳原子的全氟化烃基，R表示氢或甲基，R 1，R 2和R 3各自独立地表示氢或基团Rf-CH-CH-，|| OHR，其中Rf和R具有已经赋予它们的含义，p是2至6的整数，m是从1到大约500的整数。

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