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1. 发明授权

US06242506B1 Flame retardant additive for radiation curable acrylic compositions 失效
标题翻译：用于辐射固化丙烯酸组合物的阻燃添加剂
公开(公告)号：US06242506B1
公开(公告)日：2001-06-05
申请号：US09120508
申请日：1998-07-22
申请人： Mingxin Fan , Gary W. Ceska , James Horgan
发明人： Mingxin Fan , Gary W. Ceska , James Horgan
IPC分类号： C08G1867
CPC分类号： C08G18/672 , C08G18/42 , C08G18/48
摘要： Radiation curable acrylic compositions are improved with regard to flame resistance by incorporating a reactive compound which is the reaction product of tetrabromophthalic anhydride or acid and a (meth)acrylic compound.
摘要翻译：通过加入作为四溴邻苯二甲酸酐或酸与（甲基）丙烯酸类化合物的反应产物的反应性化合物，可辐射固化丙烯酸组合物在阻燃性方面得到改善。

2. 发明授权

US5900472A Copolymerizable benzophenone photoinitiators 失效
标题翻译：可共聚二苯甲酮光引发剂
公开(公告)号：US5900472A
公开(公告)日：1999-05-04
申请号：US772432
申请日：1996-12-23
申请人： Mingxin Fan , Gary W. Ceska , James Horgan
发明人： Mingxin Fan , Gary W. Ceska , James Horgan
IPC分类号： C07C67/08 , C07C69/76 , C07C69/94 , C07C323/62 , C08F2/50 , C08F22/10 , C08F220/30 , C08G6/00 , C08G10/00 , C08G14/00
CPC分类号： C08F22/105 , C07C69/76 , Y10T428/31627 , Y10T428/31649
摘要： Copolymerizable benzophenone photoinitiators of the formula I ##STR1## wherein 1, k=0, 1, 2.R.sub.1 =divalent organic group having 1 to 25 carbon atoms;R.sub.2 =H or methyl; andR.sub.3, R.sub.4 =organic group having 1 to 25 carbon atoms.X, Y=hydrogen, halogen or (C.sub.1 -C.sub.25) groups containing N, S, and/or O;and method of making the photoinitiators.The photoinitiators overcome the leaching problem with prior photoinitiators in radiation curable polymer applications. Radiation curable polymers, cured polymers, and coated articles are also disclosed.
摘要翻译：式I的可共聚二苯甲酮光引发剂，其中1，k = 0,1,2。R1 =具有1至25个碳原子的二价有机基团; R2 = H或甲基; R3，R4 =碳原子数为1〜25的有机基团。 X，Y =氢，卤素或含有N，S和/或O的（C1-C25）基团; 以及制备光引发剂的方法。光引发剂克服了可辐射固化聚合物应用中先前光引发剂的浸出问题。还公开了可辐射固化聚合物，固化聚合物和涂覆制品。

3. 发明授权

US5789512A Method for the epoxidation of unsaturated polymers 失效
标题翻译：不饱和聚合物的环氧化方法
公开(公告)号：US5789512A
公开(公告)日：1998-08-04
申请号：US772313
申请日：1996-12-23
申请人： Mingxin Fan , Gary W. Ceska , James Horgan
发明人： Mingxin Fan , Gary W. Ceska , James Horgan
IPC分类号： C08C19/06 , C08F8/08
CPC分类号： C08C19/06
摘要： A process for epoxidizing unsaturated polymers comprising reacting an unsaturated polymer with hydrogen peroxide in the presence of (a) tungstic acid or its metal salts, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst.
摘要翻译：环氧化不饱和聚合物的方法，包括在（a）钨酸或其金属盐，（b）磷酸或其金属盐存在下使不饱和聚合物与过氧化氢反应，和（c）至少一种相转移催化剂。

4. 发明授权

US4368077A Latex compositions and products made therefrom 失效
标题翻译：乳胶组合物和由其制成的产品
公开(公告)号：US4368077A
公开(公告)日：1983-01-11
申请号：US223805
申请日：1981-01-09
申请人： Gary W. Ceska , Gerald W. Burkhart
发明人： Gary W. Ceska , Gerald W. Burkhart
IPC分类号： C04B28/04 , C08L21/02 , C04B7/356
CPC分类号： C04B28/04 , C08L21/02
摘要： A latex containing a wax additive, useful for example in cement mortar compositions for application in thin layers such as on bridge deck overlays, overpasses, ramps, elevated sections of freeways and other locations where high resistance to penetration by water or corrosive liquids is desired, may be provided by first dissolving the wax in one of the monomers to be emulsion polymerized to form said latex.
摘要翻译：含有蜡添加剂的胶乳，可用于例如用于薄层的水泥砂浆组合物中，例如在桥面叠层，立交桥，斜坡，高速公路的高架部分以及需要水或腐蚀性液体的高抗渗性的其它位置，可以通过首先将蜡溶解在要被乳液聚合的单体之一中以形成所述胶乳来提供。

5. 发明授权

US06399672B1 Oil soluble metal-containing compounds, compositions and methods 失效
标题翻译：含油溶性金属的化合物，组合物和方法
公开(公告)号：US06399672B1
公开(公告)日：2002-06-04
申请号：US09324540
申请日：1999-06-02
申请人： Gary W. Ceska , James P. Horgan , Thomas W. Hazell , William R. Schaeffer
发明人： Gary W. Ceska , James P. Horgan , Thomas W. Hazell , William R. Schaeffer
IPC分类号： C08F246
CPC分类号： C09D4/00 , C07F9/091 , C09D4/06 , Y10T428/31855 , Y10T428/31902 , C08F230/04 , C08F290/06
摘要： Radiation curable compositions for coatings, adhesives, inks, and molded articles are disclosed. The radiation curable compositions comprise (A) at least one polymerizable, ethylenically unsaturated compound of one of the following formulas: wherein M is one or more metal atoms of valence n, wherein n=y·w, wherein M is optionally more than one metal atom, with the proviso that the global equivalent metal valence is n=w·y; n is an integer of about 1-6; R is a residue of a compound having anhydride and/or carboxylic acid groups with initial equivalent carboxy equivalent functionality defined by the equation f=x+y+z, wherein f is an integer of about 2 to 30; R1 is a residue of a hydroxy-containing ethylenically unsaturated compound; R2 is H or a residue of a hydroxy containing ethylenically unsaturated compound different from R1; R3 is a residue of a hydroxy-containing ethylenically unsaturated compound; w is the number of moieties having residue R required for valence n; x is an integer of about 1 to f−1; y is an integer of about 1 to 2 (the number of intramolecular carboxylates bonded to M); z is an integer of about 0 to f−2; Y is H or R3; and (B) at least one copolymerizable ethylenically unsaturated monomer or oligomer.
摘要翻译：公开了用于涂料，粘合剂，油墨和模塑制品的可辐射固化组合物。可辐射固化组合物包含（A）至少一种下列通式之一的可聚合的烯键式不饱和化合物：其中M是价数n的一个或多个金属原子，其中n = yw，其中M任选地多于一个金属原子，全局当量金属价态为n = wy; n为约1-6的整数; R为具有酸酐和/或羧酸基团的化合物的残基，其初始等同的羧基当量官能度由式f = x + y + z，其中f为约2至30的整数; R 1为含羟基的烯键式不饱和化合物的残基; R 2为H或不同于R 1的含羟基的烯属不饱和化合物的残基; R 3为含羟基的烯属不饱和化合物的残基; w是价数n所需的残基R的部分数; x是约1至f-1的整数; y是约1至2的整数（分子内的数目羧酸盐键合到M）; z为约0〜f-2的整数，Y为H或R3; 和（B）至少一种可共聚的烯属不饱和单体或低聚物。

6. 发明授权

US06124483A Process for preparing unsaturated esters containing cyclic epoxy group 失效
标题翻译：制备含环状环氧基的不饱和酯的方法
公开(公告)号：US06124483A
公开(公告)日：2000-09-26
申请号：US773524
申请日：1996-12-23
申请人： Mingxin Fan , Gary W. Ceska , James Horgan
发明人： Mingxin Fan , Gary W. Ceska , James Horgan
IPC分类号： B01J31/24 , B01J31/34 , C07D301/12 , C07D303/16 , C07D303/24 , C07D303/40 , C08F20/32 , C08G59/24
CPC分类号： C07D303/40 , C07D301/12 , C07D303/16 , C07D303/24 , C08G59/24
摘要： Process of making compounds of the formula ##STR1## wherein R.sub.1 =(C.sub.1 -C.sub.6) alkyl;X=O, S, NH;R.sub.2 =divalent saturated organic group;Y=O, S, NH, ester;R.sub.3 =cyclic moiety containing oxirane group;comprising reacting a compound of the formula ##STR2## wherein R.sub.4 is a cyclic moiety containing C.dbd.C group with hydrogen peroxide in the presence of (a) tungstic acid, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst;polymers of compounds of formula I; andcompounds of formula I except for compounds wherein R.sub.4 is a dicyclopentenyl epoxide, Y is O, R.sub.2 is --CH.sub.2 CH.sub.2 --, X is O, and R.sub.1 is H or methyl.
摘要翻译：制备下式化合物的方法其中R1 =（C1-C6）烷基; X = O，S，NH; R2 =二价饱和有机基团; Y = O，S，NH，酯; R3 =含环氧乙烷基团的环状部分; 包括在（a）钨酸，（b）磷酸或其金属盐存在下使下式化合物其中R 4是含有C = C基团的环状部分与过氧化氢反应，和（c）至少一种相转移催化剂; 式I化合物的聚合物; 和式I化合物，除了其中R 4是二环戊烯基环氧化物，Y是O，R 2是-CH 2 CH 2 - ，X是O，R 1是H或甲基的化合物。

7. 发明授权

US4722947A Production of radiation curable partial esters of anhydride-containing copolymers 失效
标题翻译：生产含酸酐共聚物的可辐射固化的偏酯
公开(公告)号：US4722947A
公开(公告)日：1988-02-02
申请号：US762595
申请日：1985-08-05
申请人： Chandrakant B. Thanawalla , Gary W. Ceska
发明人： Chandrakant B. Thanawalla , Gary W. Ceska
IPC分类号： C08F8/14
CPC分类号： C08F8/14 , C08F2810/20 , C08F2810/30
摘要： Radiation-curable low molecular weight partial ester copolymer compositions comprising products of a terminally ethylenically unsaturated compound and a maleic anhydride characterized by having free-anhydride functionality are provided. The partial esters are produced by esterification of certain copolymers under anhydrous conditions with a hydroxyalkyl acrylyl compound, or an admixture thereof with a monohydric alcohol. The compositions of the invention are useful as radiation cross-linkable diluents for radiation-hardenable compositions, particularly in improving adhesion promotion and/or dispersive capabilities of binder resins.
摘要翻译：提供了包含具有非离子酸酐官能团特征的末端烯属不饱和化合物和马来酸酐的产物的可辐射固化的低分子量偏酯共聚物组合物。部分酯通过某些共聚物在无水条件下与羟基烷基丙烯基化合物或其与一元醇的混合物的酯化而产生。本发明的组合物可用作辐射可硬化组合物的辐射可交联稀释剂，特别是用于改进粘合剂树脂的粘合促进和/或分散能力。

8. 发明授权

US06559260B1 Allyl urethane resin compositions 有权
标题翻译：烯丙基聚氨酯树脂组合物
公开(公告)号：US06559260B1
公开(公告)日：2003-05-06
申请号：US09535176
申请日：2000-03-27
申请人： Mingxin Fan , Gary W. Ceska , James Horgan
发明人： Mingxin Fan , Gary W. Ceska , James Horgan
IPC分类号： C08L7516
CPC分类号： C09D175/16 , C08G18/6715
摘要： The present invention is for a new class of allyl urethane resin which can be cured with peroxide at high temperature alone or in combination with some accelerators. These allyl urethane resins can be sued alone or in combination with other free radically polymerizable materials such as allyl monomers and ligomers or (meth)acrylate monomers and oligomers. These new allyl urethane resins contain at least two allyl functional groups.
摘要翻译：本发明是一种新的烯丙基聚氨酯树脂，其可以单独或与一些加速剂组合使用，可以在高温下用过氧化物固化。这些烯丙基聚氨酯树脂可以单独或与其它可自由基聚合的材料如烯丙基单体和连接体或（甲基）丙烯酸酯单体和低聚物组合起来。这些新的烯丙基聚氨酯树脂含有至少两个烯丙基官能团。

9. 发明授权

US6084111A Method for making cycloaliphatic epoxides 失效
标题翻译：制备脂环族环氧化物的方法
公开(公告)号：US6084111A
公开(公告)日：2000-07-04
申请号：US62593
申请日：1998-04-17
申请人： Mingxin Fan , Gary W. Ceska , James Horgan , Henri Strub
发明人： Mingxin Fan , Gary W. Ceska , James Horgan , Henri Strub
IPC分类号： C07D301/12 , C07D303/16 , C07D303/40 , C08G59/24 , C08G59/32 , C07D303/00
CPC分类号： C08G59/24 , C07D301/12 , C07D303/16 , C07D303/40 , C08G59/3218
摘要： Compounds having the formula ##STR1## wherein X is selected from O, (CH.sub.2).sub.m O, S, (CH.sub.2).sub.m S, NH, (CH.sub.2).sub.m NH, COO.sup.-, (CH.sub.2).sub.m COO.sup.-, .sup.- OOC and .sup.- OOC (CH.sub.2).sub.m ;m is 1 to 6;n is 1 to 100;R.sub.1 is selected from H, (C.sub.1 -C.sub.20) alkyl, (C.sub.1 -C.sub.20) alkoxy and (C.sub.1 -C.sub.20) ester; andA is a saturated organic linking group selected from residues of polyol, polythiol, polyamine, and polyacid, are prepared by reacting compounds according to formula II ##STR2## with hydrogen peroxide in the presence of (a) tungstic acid or its metal salts, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst.
摘要翻译：具有下式的化合物其中X选自O，（CH 2）m O，S，（CH 2）m S，NH，（CH 2）m NH，COO-，（CH 2）m COO-， - OOC和-OOC（CH 2）m; m为1〜6; n为1〜100; R1选自H，（C1-C20）烷基，（C1-C20）烷氧基和（C1-C20）酯; （a）钨酸或其金属盐的存在下，通过使根据式II的化合物与过氧化氢反应制备A是选自多元醇，多硫醇，多胺和多元酸的残基的饱和有机连接基团，（b）磷酸或其金属盐，以及（c）至少一种相转移催化剂。

10. 发明授权

US5763629A Alkoxylated glycidyl (meth)acrylates and method of preparation 失效
标题翻译：（甲基）丙烯酸缩水甘油酯及其制备方法
公开(公告)号：US5763629A
公开(公告)日：1998-06-09
申请号：US772979
申请日：1996-12-23
申请人： Mingxin Fan , Gary W. Ceska , James Horgan , Thomas W. Hazell
发明人： Mingxin Fan , Gary W. Ceska , James Horgan , Thomas W. Hazell
IPC分类号： C07D303/16 , C08F20/32 , C08G65/14 , C08L71/02 , C07D301/12
CPC分类号： C08G65/14 , C07D303/16 , C08F20/32 , C08L71/02
摘要： Compounds of the formula ##STR1## wherein R.sub.1 32 H, CH.sub.3 ; R.sub.2 =H, (C.sub.1 -C.sub.6)alkyl; and x=1-20; and process for preparing such compounds by reacting a compound of the formula ##STR2## with hydrogen peroxide in the presence of (a) tungstic acid or its metal salts, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst.
摘要翻译：式（I）的化合物其中R 13 2 H，CH 3; R2 = H，（C1-C6）烷基; 和x = 1-20; 和（a）钨酸或其金属盐，（b）磷酸或其金属盐的存在下，使式（II）化合物与过氧化氢反应制备此类化合物的方法，和（c）至少一种相转移催化剂。

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