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1. 发明授权

US3773860A Phosphonocarboxylic acid amides 失效
标题翻译：磷酸酰胺类
公开(公告)号：US3773860A
公开(公告)日：1973-11-20
申请号：US3773860D
申请日：1971-08-05
申请人： CIBA GEIGY AG
发明人： NACHBUR H , MAEDER A
IPC分类号： C07F9/40 , C08K5/5353
CPC分类号： C07F9/4006 , C08K5/5353 , C08L75/04
摘要： PHOSPHONCARBOXYLIC ACID AMINDES OF THE FORMULA

R1-O-P(=X)(-O-R2)-CNH2N-CO-NH-CH(-C(-CL)3)-NH-A

ARE PROVIDED, WHEREIN R1 AND R2 EACH DENOTE AN ALKYL HALOGENOALKYL OR ALKENYL RADICAL WITH AT MOST 4 CARBON ATOMS, A DENOTES AN OPTIONALLY FURTHER SUBSTITUTED ARYL OR ALKYL RADICAL, X DENOTES A SULPHUR OR AN OXYGEN ATOM AND N IS AN INTEGER OF 1 TO 3. THESE COMPOUNDS ARE USEFUL FOR FLAMEPROOFING OF PLASTICS OR CASTING COMPOSITIONS WHICH SERVE FOR THE MANUFACTURE OF SHAPED ARTICLES, SUCH AS FOAMS, FILMS OR FIBERS.

2. 发明授权

US3855309A Process for the manufacture of phosphorus-containing condensation products, the products and their use as flameproofing agents 失效
标题翻译：含磷含量产品，产品及其作为防火剂的制造工艺
公开(公告)号：US3855309A
公开(公告)日：1974-12-17
申请号：US28541872
申请日：1972-08-31
申请人： CIBA GEIGY AG
发明人： NACHBUR H , MAEDER A
IPC分类号： B27K3/15 , C07F9/50 , C07F9/6521 , C08L61/32 , D06M15/431 , D06M15/555 , D06M15/667 , C07F9/28
CPC分类号： D06M15/667 , B27K3/15 , B27K2240/30 , C07F9/50 , C07F9/65212 , C08L61/32 , D06M15/431 , D06M15/555 , Y10S428/921 , Y10T428/2938 , Y10T428/2965 , Y10T428/2967 , Y10T428/31786
摘要： The subject of the invention is a process for the manufacture of water-soluble condensation products of hydroxymethyl-phosphonium compounds and tri-glycidylisocyanurate, characterised in that (a) 1 mol of a tetrakis-(hydroxymethyl)-phosphonium compound is condensed with (b) 0.02 to 0.5 mol, preferably 0.05 to 0.3 mole, of tri-glycidylisocyanurate at 40* to 120*C, optionally in the presence of formaldehyde or a formaldehyde-releasing agent and an inert organic solvent, the condensation is optionally thereafter continued at temperatures of 100* to 150*C and, if appropriate, free hydroxyl groups are etherified at least partially with at least one alkanol with 1 to 4 carbon atoms and, if appropriate, the salts of the condensation products are converted into the corresponding hydroxides. The condensation products are used for flameproofing organic fibre material, especially textiles.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和三缩水甘油基异氰尿酸酯的水溶性缩合产物的方法，其特征在于（a）1摩尔四（羟甲基） - 鏻化合物与（b ）任选在甲醛或甲醛释放剂和惰性有机溶剂的存在下，在40〜120℃下，0.02〜0.5摩尔，优选0.05〜0.3摩尔的三缩水甘油基异氰脲酸酯，任选地，随后在温度至少部分为至少一种具有1至4个碳原子的链烷醇醚化，如果合适的话，缩合产物的盐转化为相应的氢氧化物。

3. 发明授权

US3801678A Phosphonopropionic acid amides 失效
标题翻译：磷酸肌酸
公开(公告)号：US3801678A
公开(公告)日：1974-04-02
申请号：US3801678D
申请日：1972-05-02
申请人： CIBA GEIGY AG
发明人： NACHBUR H , MAEDER A
IPC分类号： C07F9/40 , C08J9/00 , D06M13/288 , C09K3/28
CPC分类号： C08J9/0038 , C07F9/4006 , C08J2375/04 , C08K5/53 , D06M13/288 , C08L75/04
摘要： THE SUBJECT OF THE INVENTION ARE PHOSPHORUS COMPOUNDS OF THE FORMULA

(-N(-CO-CH(-X)-CH2-P(=O)(-O-R1)-O-R2)-CH2-N(-CO-A)-) (-H)

(-Y)

WHEREIN R1 AND R2 EACH DENOTE ALKYL, ALKENYL OR HALOGENOALKYL WITH AT MOST 4 CARBON ATOMS, X DENOTES HYDROGEN OR METHYL, Y DENOTES HYDROGEN OR -CH2-O-Z, Z DENOTES HYDROGEN OR ALKYL WITH 1 TO 4 CARBON ATOMS AND A DENOTES ALKYL OR HALOENOALKYL WITH AT MOST 4 CARBON ATOMS. THESE PHOSPHOROUS COMPOUNDS ARE ABOVE ALL SUITABLE AS FLAMEPROOFING, AGENTS, PARTICULARLY FOR POLYURETHANE AND CELLULOSE CONTAINING TEXTILES.

4. 发明授权

US3843391A Process for finishing textiles 失效
标题翻译：整理纺织品的工艺
公开(公告)号：US3843391A
公开(公告)日：1974-10-22
申请号：US24901472
申请日：1972-05-01
申请人： CIBA GEIGY AG
发明人： TOEPFL R , ABEL H , MAEDER A
IPC分类号： C08G59/58 , D06M15/37 , D06M3/02 , C09D3/58
CPC分类号： C08G59/58 , D06M15/37 , Y10T442/2762
摘要： 1. A PROCESS FOR FINISHING WOOLEN MATERIAL, WHICH COMPRISES TREATING THE WOOLEN MATERIAL AT 30 TO 100* C. WITH AN AQUEOUS PREPARATION OF REACTION PRODUCTS OF EPOXIDES, POLYMERIC FATTY ACIDS AND AMINES, SAID PRODUCTS OF EPOXIDES, TAINED BY REACTING (A) A REACTION PRODUCT OF AT LEAST (A'') ONE EPODIXE WHICH CONTAINS AT LEAST TWO EPOXIDE GROUPS PER MOLECULE AND AT LEAST (A") ONE POLYMERIC UNSATURATED FATTY ACID, DERIVED FROM A FATTY ACID OF 16 TO 22 CARBON ATOMS, WITH THE RATIO OF EQUIVALENTS OF EPOXIDE GROUPS TO ACID GROUPS BEING 0.45:1 TO 0.95:1, WITH (B) AMMONIA OR AN ALIPHATIC OR CYCLOALIPHATIC AMINE WHICH IS A PRIMARY, SECONDARY OR TERTIARY AMINE CONTAINING NO NON-BASIC NITROGEN ATOMS, IN THE PRESENCE OF AN ORGANIC SOLVENT, WITH THE RATIO OF EQUIVALENTS OF ACID GROUPS TO HYDROGEN BONDED AMINE NITROGEN, TO TERITARY AMINO GROUPS OR TO AMMONIA BEING 1:1 TO 1:10, WHEREIN THE REACTION BETWEEN COMPONENTS (a) AND (B) IS CARRIED OUT AT A TEMPERATURE IN THE RANGE OF 20 TO 120* C., AND THEN RINSING AND DRYING THE TREATED WOOLEN MATERIAL.

5. 发明授权

US3709847A Preparations of reaction products of epoxides,fatty amines and basic polyamides,processes for their manufacture and their use 失效
标题翻译：环氧化物，脂肪胺和基础聚氨酯的反应产物的制备，其制造及其使用的方法
公开(公告)号：US3709847A
公开(公告)日：1973-01-09
申请号：US3709847D
申请日：1971-01-29
申请人： CIBA GEIGY AG
发明人： TOEPFL R , ABEL H , MAEDER A
IPC分类号： C08G73/00 , C08G59/50 , C08G65/00 , C08L63/00 , C08L77/00 , D06M13/364 , D06M15/592 , D06P1/52 , D21H17/55 , C08G41/04
CPC分类号： D21H17/55 , C08G59/5013 , C08L63/00 , C08L77/08 , D06M13/364 , D06M15/592 , D06P1/5278 , C08L2666/14
摘要： A PROCESS OF THE MANUFACTURE OF STABLE PREPARATIONS OF WATER-SOLUBLE OR WATER-DISPERSIBLE READTION PRODUCTS OF EPOXIDES, FATTY AMINES AND BASIC POLYAMIDES IS PROVIDED. THE EPOXIDES CONTAINS AT LEAST TWO EPOXIDE GROUPS PER MOLECULE, THE AMINES ARE HIGHER-MOLECULAR WEIGHT FATTY AMINES (H3C-(CH2)X-NH2 WHEREIN X REPRESENTS AN INTEGER HAVING THE VALUE OF 11 TO 23) AND THE POLYAMIDES ARE MADE FROM POLYMERIC UNSATURATED FATTY ACIDS AND POLYALKYLENEPOLYAMINES. THE REACTION IS CARRIED OUT IN THE PRESENCE OF AN ORGANIC SOLVENT AT TEMPERATURES UP TO 95* C. NOT LATER THAN AFTER COMPLETION OF THE REACTION, IT IS ENSURED THAT A SAMPLE OF THE REACTION MIXTURE HAS A PHVALUE OF 2 TO 8 AFTER DILUTION WITH WATER. THE RESULTING REACTION PRODUCTS ARE SOLUBLE IN WATER AND ARE USEFUL IN THE TEXTILES INDUSTRY E.G. FOR RENDERING WOOL NON-FELTING.

6. 发明授权

US3800010A Phosphonopropionic acid amide derivatives 失效
标题翻译：磷酸酰胺衍生物
公开(公告)号：US3800010A
公开(公告)日：1974-03-26
申请号：US11276971
申请日：1971-02-04
申请人： CIBA GEIGY AG
发明人： NACHBUR H , MAEDER A
IPC分类号： C07F9/40 , C08G18/28 , C08G18/38 , C08K5/5353 , D06M13/288 , C08F45/58
CPC分类号： D06M13/288 , C07F9/4006 , C08G18/288 , C08G18/3889 , C08K5/5353
摘要： The subject of the invention are phosphonopropionic acid amide derivatives of the formula

WHEREIN R1 and R2 each denote an alkyl, halogenoalkyl or alkenyl radical with up to 4 carbon atoms each, X denotes a sulphur atom or preferably an oxygen atom, Y denotes a methyl group or preferably a hydrogen atom and A denotes a halogenated alkyl radical. These compounds are made by reacting the corresponding phosphonopropionic acid amide with the corresponding halogenoaldehyde. The compounds are used as flameproofing agents for fibers or in plastics or they serve as intermediates for the manufacture of other valuable compounds.
摘要翻译：本发明的主题是式WHEREIN R 1和R 2的膦酰基丙酸酰胺衍生物各自表示具有至多4个碳原子的烷基，卤代烷基或烯基，X表示硫原子或优选氧原子，Y表示甲基或优选氢原子，A表示卤代烷基。这些化合物通过使相应的膦酰基丙酸酰胺与相应的卤代甲醛反应制得。这些化合物用作纤维或塑料的防火剂，或者它们用作制造其它有价值化合物的中间体。

7. 发明授权

US3769365A Reaction product of epoxy resins,fatty amines,dicarboxylic acids and aminoplasts 失效
标题翻译：环氧树脂，脂肪酸，二羧酸和氨基酸的反应产物
公开(公告)号：US3769365A
公开(公告)日：1973-10-30
申请号：US3769365D
申请日：1971-06-08
申请人： CIBA GEIGY AG
发明人： TOEPFL R , ABEL H , MAEDER A
IPC分类号： C08G59/58 , C08G69/48 , D06M15/37 , D06M15/55 , C08G45/10
CPC分类号： C08G59/58 , C08G69/48 , D06M15/37 , D06M15/55
摘要： STABLE PREPARATIONS ARE PROVIDED CONTAINING REACTION PRODUCTS OBTAINED BY REACTING IN THE PRESENCE OF AN ORGANIC SOLVENT (A) EPOXIDES CONTAINING AT LEAST TWO EPOXIDE GROUPS PER MOLECULE WITH (B) FATTY AINES WITH 12 TO 24 CARBON ATOMS AND (C) ALIPHATIC DICARBOXYLIC ACIDS WITH AT LEAST 7 CARBON ATOMS AND OPTIONALLY (C'') ANHYDRIDES OF AROMATIC DICARBOXYLIC ACIDS OR ALIPHATIC MONOCARBOXYLIC OR DICARBOXYLIC ACIDS, (D) AN AMINOPLAST PRECONDENSATE CONTAINING ALKYLETHER GROUPS, (E) ALIPHATIC DIOLS WITH 2 TO 22 CARBON ATOMS AND (F) POLYFUNCTIONAL COMPOUNDS CONTAINING HALOGEN ATOMS, VINYL, ESTER, ACID, NITRILE HYDROXYL OR EPOXIDE GROUPS. SAID REACTION PRODUCTS CONTAIN FREE CARBOXYL GROUPS AND OPTIONALLY AMMONIA OR AN ORGANIC BASE IS ADDED SO THAT A SAMPLE OF THE REACTION MIXTURE-AFTER ADDING SOME WATER TO ENABLE A PH-READING-HAS A PH-VALUE OF 7.5 TO 12. THE STABLE PREPARATIONS ARE USEFUL TO FINISHING TEXTILE MATERIALS, ESPECIALLY TO RENDERING WOOL NON-FELTING.

8. 发明授权

US3754981A Process for flameproofing cellulose-containing fibre material 失效
标题翻译：包含纤维素的纤维材料的方法
公开(公告)号：US3754981A
公开(公告)日：1973-08-28
申请号：US3754981D
申请日：1971-06-09
申请人： CIBA GEIGY AG
发明人： NACHBUR H , HUBER EMDEN H , KERN J , MAEDER A
IPC分类号： D06M13/44 , C07F9/40 , C09K21/14 , D06M13/288 , C09K3/28 , D06M13/32
CPC分类号： D06M13/288 , C07F9/4006 , Y10T428/8305 , Y10T442/268
摘要： A process for the flame-proofing of cellulose-containing fibrous materials by applying to the substrates aqueous preparations containing a self-condensation product of an N-methylolamide of a dialkyl, dihalogenalkyl or dialkenyl phosphonopropionic acid advantageously together with a curable aminoplast precondensate.
摘要翻译：通过将含有二烷基，二卤代烷基或二烯基膦酰基丙酸的N-羟甲基酰胺的自缩合产物的含水制剂与可固化的氨基塑料预缩合物一起应用于底物含水纤维素材料的阻燃方法。

9. 发明专利

DE2127314C3 未知
公开(公告)号：DE2127314C3
公开(公告)日：1980-11-20
申请号：DE2127314
申请日：1971-06-02
申请人： CIBA GEIGY AG
发明人： ABEL H , MAEDER A , TOEPFL R
IPC分类号： C08G59/58 , C08G69/48 , D06M15/37 , D06M15/55 , C08G59/18
摘要： 1313072 Antifelting treatment for wool; sizing paper CIBA-GEIGY AG 8 June 1971 [9 June 1970 22 Jan 1971] 19450/71 Headings D1P and D2B [Also in Division C3] Wool is rendered non felting and paper may be sized by treatment with a composition comprising a polyepoxide (I) containing at least two epoxy groups per molecule, a C 12-24 fattyamine (II) and an aliphatic saturated dicarboxylic acid (III) containing at least 7 carbon atoms reacted together to form a stable preparation which by adding (if necessary) ammonia or water soluble organic base has a pH value of 7.5-12 on dilution with water. The following optional ingredients may also be present in the reaction mixture: an anhydride of an aromatic dicarboxylic acid (at least C 8 ) or of an aliphatic mono- or di-carboxylic acid (at least C 4 ), an aminoplast precondensate containing alkylether groups, a C 2-22 aliphatic diol, another polyfunctional compound containing labile halogen, vinyl or ester groups together with at most one acid, nitrile OH or epoxy group. The starting materials are reacted together, e.g. at 80-120C in an organic solvent, e.g. ethylene glycol monobutyl ether. I may be a diglycidyl ether of bisphenol A. II may have the formula Me(CH 2 ) x NH 2 in which x = 11-23. III may have the formula HOOC(CH 2 ) v COOH in which y = 5-12. The wool may be pretreated with dichloroisocyanuric acid or a salt thereof. In an example wool yarn is first dyed with a reactive dye in a circulation bath and rinsed. It was then placed in a water containing 41. water and warmed to 40C, then 1 Kg. oxalic acid and 0.2 Kg. of a condensate of 1 mol of a C 16-20 fatty amine and 70 mol ethylene oxide was introduced followed by 10 Kg of a product according to the invention. An emulsion formed which was uniformly absorbed on the wool in 20-30 minutes and thereafter the condensation product of tristearoyl ethylene triamine and ethylene oxide was added as softener. The product may be steamed. The treating bath may optionally contain anonyl phenol ethylene oxide condensate, diammonium phosphate and monoethanolamine sulphite.

10. 发明专利

NO133144C 未知
公开(公告)号：NO133144C
公开(公告)日：1976-03-17
申请号：NO426370
申请日：1970-11-09
申请人： CIBA GEIGY AG
发明人： TOEPFL R , ABEL H , MAEDER A
IPC分类号： D06M15/273 , C08G18/00 , C08G18/58 , C08G59/00 , C08G59/17 , C08G59/58 , C08G63/52 , D04H1/08 , D06M13/02 , D06M13/325 , D06M15/37 , D06M15/55 , D06M15/61 , C08G59/18 , D06M15/12

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