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1. 发明授权

US06822068B2 Method for producing highly-branched glycidol-based polyols 失效
标题翻译：高度支化的缩水甘油基多元醇的制备方法
公开(公告)号：US06822068B2
公开(公告)日：2004-11-23
申请号：US10335667
申请日：2003-01-02
申请人： Alexander Sunder , Rolf Mülhaupt
发明人： Alexander Sunder , Rolf Mülhaupt
IPC分类号： C08G6528
CPC分类号： C08G18/48 , C08G65/22 , C08G65/2648
摘要： This invention relates to a process for the preparation of highly-branched polyols by polymerisation of glycidol in the presence of a hydrogen-active starter compound with basic catalysis, wherein glycidol is added in dilute solution and the solvent used for the dilution is continuously distilled off. The polyols thus prepared are colorless, contain as the core unit solely the starter compound used and have polydispersities of less than 1.7. The present invention also relates to polyols that comprise the reaction product of the polyols based on glycidol with one or more expoxide monomers. This invention also relates to a process for the preparation of these polyols.
摘要翻译：本发明涉及通过在具有碱催化作用的氢活化起始化合物存在下缩水甘油聚合来制备高支化多元醇的方法，其中将缩水甘油加入稀溶液中，用于稀释的溶剂被连续地蒸馏掉。如此制备的多元醇是无色的，仅含有起始化合物的核心单元，并且具有小于1.7的多分散性。本发明还涉及包含基于缩水甘油的多元醇与一种或多种过氧化物单体的反应产物的多元醇。本发明还涉及制备这些多元醇的方法。

2. 发明授权

US06765082B2 Method for producing highly-branched glycidol-based polyols 失效
标题翻译：高度支化的缩水甘油基多元醇的制备方法
公开(公告)号：US06765082B2
公开(公告)日：2004-07-20
申请号：US10335681
申请日：2003-01-02
申请人： Alexander Sunder , Rolf Mülhaupt
发明人： Alexander Sunder , Rolf Mülhaupt
IPC分类号： C08G6526
CPC分类号： C08G18/48 , C08G65/22 , C08G65/2648
摘要： This invention relates to as process for the preparation of highly-branched polyols by polymerization of glycidol in the presence of a hydrogen-active starter compound with basic catalysis, wherein glycidol is added in dilute solution and the solvent used for the dilution is continuously distilled off. The polyols thus prepared are colorless, contain as the core unit solely the starter compound used and have polydispersities of less than 1.7.
摘要翻译：本发明涉及通过在具有碱催化作用的氢活化起始化合物存在下，缩水甘油聚合制备高支化多元醇的方法，其中将缩水甘油加入稀溶液中，用于稀释的溶剂被连续蒸馏除去。如此制备的多元醇是无色的，仅含有起始化合物的核心单元，并且具有小于1.7的多分散性。

3. 发明申请

US20100190931A1 CATALYST SYSTEM FOR POLYMERIZATION OF OLEFINIC MONOMERS, PROCESS FOR PREPARING POLYMERS, AND POLYMERS PREPARED BY THE PROCESS 失效
标题翻译：烯烃单体聚合催化剂体系，制备聚合物的方法和工艺制备的聚合物
公开(公告)号：US20100190931A1
公开(公告)日：2010-07-29
申请号：US12452713
申请日：2008-07-22
申请人： Marc Oliver Kristen , Rolf Mülhaupt , Georg Müller
发明人： Marc Oliver Kristen , Rolf Mülhaupt , Georg Müller
IPC分类号： C08F4/64 , C08L23/06 , B32B5/02 , B01J32/00 , B01J31/14 , B01J31/06
CPC分类号： C08F10/00 , C08F4/65925 , Y10S526/943 , Y10T428/249924 , C08F4/027
摘要： The present invention relates to new catalyst supports comprising nanofibers, a catalyst system comprising these supports as well as a process for preparing nanocomposites and the nanocomposites prepared. The invention especially concerns a supported catalyst system for polymerization of olefins, comprising a support made of fibers or a fleece of fibers, wherein the mean fiber diameter is less than 1000 nm, preferably less than 500 nm and the mean fiber length is more than 200,000 nm, preferably more than 500,000 nm and especially preferred more than 1,000,000 nm as well as a process for polymerizing olefinic systems in the presence of these catalyst systems and the resulting nanocomposites.
摘要翻译：本发明涉及包含纳米纤维的新催化剂载体，包含这些载体的催化剂体系以及制备纳米复合材料的方法和制备的纳米复合材料。本发明特别涉及用于烯烃聚合的负载型催化剂体系，其包括由纤维制成的载体或纤维的绒毛，其中平均纤维直径小于1000nm，优选小于500nm，平均纤维长度大于20万 nm，优选大于500,000nm，特别优选大于1,000,000nm，以及在这些催化剂体系存在下聚合烯属体系的方法和所得的纳米复合材料。

4. 发明授权

US06197849B1 Organophilic phyllosilicates 失效
标题翻译：亲缘页硅酸盐
公开(公告)号：US06197849B1
公开(公告)日：2001-03-06
申请号：US09248649
申请日：1999-02-11
申请人： Carsten Zilg , Rolf Mülhaupt , Jürgen Finter
发明人： Carsten Zilg , Rolf Mülhaupt , Jürgen Finter
IPC分类号： C08K900
CPC分类号： C08K9/04 , C08L63/00
摘要： Organophilic phyllosilicates which have been prepared by treating a naturally occurring or synthetic phyllosilicate, or a mixture of such silicates, with a salt of a quaternary or other cyclic amidine compound, or with a mixture of such salts; polymeric systems, in particular thermoplastic polymers and thermosetting polymer systems, preferably epoxy resins, polyurethanes and rubbers, which comprise novel organophilic phyllosilicates, and also shapable moulding materials and finished mouldings in the form of composite materials, in particular in the form of nanocomposites.
摘要翻译：通过将天然存在的或合成的页硅酸盐或这种硅酸盐的混合物与季铵盐或其它环状脒化合物的盐或这些盐的混合物进行处理而制备的亲有性页硅酸盐; 聚合物系统，特别是热塑性聚合物和热固性聚合物体系，优选环氧树脂，聚氨酯和橡胶，其包含新型有机层状硅酸盐，以及成型模塑材料和复合材料形式的成型模制品，特别是纳米复合材料形式。

5. 发明授权

US07495037B2 Dental coating materials 有权
标题翻译：牙科涂料
公开(公告)号：US07495037B2
公开(公告)日：2009-02-24
申请号：US10928540
申请日：2004-08-27
申请人： Norbert Moszner , Simone Klapdohr , Ulrich Salz , Jörg Zimmermann , Volker M. Rheinberger , Rolf Mülhaupt
发明人： Norbert Moszner , Simone Klapdohr , Ulrich Salz , Jörg Zimmermann , Volker M. Rheinberger , Rolf Mülhaupt
IPC分类号： A61K6/083 , A61K6/08 , A61K6/00 , C08F283/12
CPC分类号： C09D183/04 , A61K6/0017 , Y10S522/908 , C08L83/16
摘要： Polymerizable materials which contain (1) 1 to 80 wt.-% of at least one polysiloxane, (2) 0.1 to 5 wt.-% of one or more initiators for radical polymerization, (3) 0 to 60 wt.-% of radically polymerizable monomer and (4) 1 to 50 wt.-% of one or more radically polymerizable monomers which carry at least phosphonic acid group, sulphonic acid group and/or mono- or dihydrogen phosphoric acid ester group, the polysiloxane (1), the monomer (3) or both being substituted by fluorine. The materials are suitable in particular for the coating of natural or artificial teeth.
摘要翻译：含有（1）1至80重量％的至少一种聚硅氧烷的可聚合材料，（2）0.1至5重量％的一种或多种用于自由基聚合的引发剂，（3）0至60重量％可自由基聚合的单体和（4）1至50重量％的至少携带膦酸基，磺酸基和/或单或二氢磷酸酯基的一种或多种可自由基聚合的单体，聚硅氧烷（1），单体（3）或两者均被氟取代。这些材料特别适用于天然或人造牙齿的涂层。

6. 发明授权

US06942830B2 Device and method for the production of three-dimensional objects 有权
标题翻译：用于生产三维物体的装置和方法
公开(公告)号：US06942830B2
公开(公告)日：2005-09-13
申请号：US10257585
申请日：2000-12-01
申请人： Rolf Mülhaupt , Rüdiger Landers , Hendrik John
发明人： Rolf Mülhaupt , Rüdiger Landers , Hendrik John
IPC分类号： C12M1/40 , A61L27/00 , B29C31/04 , B29C41/36 , B29C67/00 , B29C41/02 , B29C41/22
CPC分类号： B29C41/36 , B29C31/045 , B29C64/106 , B29C64/40 , B33Y10/00 , B33Y30/00 , B33Y40/00 , B33Y70/00
摘要： A device and a process for producing three-dimensional objects is disclosed. The device has a container (1) for a medium (2) and a three-dimensionally positionable dispenser (4) for release of a material (3), the addition of which to the medium (2) leads to the formation of solid structures, into the medium (2). Addition of the material (3) by moving the dispenser in XYZ direction on a platform (8) below the filling height of the first material (2) in the container (1) leads to the formation of three-dimensional objects.
摘要翻译：公开了一种用于制造三维物体的装置和方法。该装置具有用于介质（2）的容器（1）和用于释放材料（3）的三维可定位分配器（4），其中添加到介质（2）中导致形成固体结构，进入介质（2）。通过在第一材料（2）的容器（1）的填充高度以下的平台（8）上以XYZ方向移动分配器来添加材料（3），导致三维物体的形成。

7. 发明申请

US20100121009A1 CATALYST SYSTEM FOR OLEFIN POLYMERIZATION PROCESS FOR PRODUCING IT AND A PROCESS FOR THE POLYMERIZATION OF ALPHA-OLEFINS USING THE CATALYST SYSTEM 审中-公开
标题翻译：用于生产烯烃聚合方法的催化剂体系和使用催化剂体系合成α-烯烃的方法
公开(公告)号：US20100121009A1
公开(公告)日：2010-05-13
申请号：US12451207
申请日：2008-05-05
申请人： Marc Oliver Kristen , Rolf Mülhaupt , Gil Scheuermann , Alexander Kurek
发明人： Marc Oliver Kristen , Rolf Mülhaupt , Gil Scheuermann , Alexander Kurek
IPC分类号： C08F4/12 , B01J37/30
CPC分类号： C08F10/00 , C08F110/02 , C08F4/7006 , C08F4/69034 , C08F4/025 , C08F2500/20 , C08F2500/04 , C08F4/69224
摘要： The invention relates to a catalyst system comprising a support in which transition metal cations or uncharged transition metal atoms are distributed. The system further comprises one or more separately added ligands which are capable of forming a coordinate or covalent bond with the transition metals. The catalyst system is produced by replacing metal ions present in a support by transition metal ions. The transition metal ions can optionally be reduced. One or more ligands which are capable of forming a coordinate or covalent bond with the transition metal or metals are subsequently added. The catalyst is used for the polymerization of olefins.
摘要翻译：本发明涉及一种催化剂体系，其包括其中分布有过渡金属阳离子或不带电过渡金属原子的载体。该体系还包含一个或多个单独添加的能够与过渡金属形成配位或共价键的配体。通过用过渡金属离子代替载体中存在的金属离子来制备催化剂体系。可以任选地还原过渡金属离子。随后加入能够与过渡金属或金属形成配位或共价键的一个或多个配位体。该催化剂用于烯烃的聚合。

8. 发明授权

US06469218B1 Process for preparing polyether polyols 失效
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US06469218B1
公开(公告)日：2002-10-22
申请号：US10136208
申请日：2002-05-01
申请人： Ornulf Rexin , Rolf Mülhaupt
发明人： Ornulf Rexin , Rolf Mülhaupt
IPC分类号： C07C4311
CPC分类号： C08G65/105 , C08G65/2675
摘要： The invention is directed to a process for preparing a polyether polyol by the polyaddition of an alkylene oxide on to a starter compound containing active hydrogen atoms under basic catalysis in the presence of phosphonium cations.
摘要翻译：本发明涉及通过在碱性催化下在鏻阳离子存在下将烯化氧加成到含活性氢原子的起始化合物上制备聚醚多元醇的方法。

9. 发明授权

US06313275B1 Azoic compounds functionalized with heterocycles 失效
标题翻译：用杂环官能化的偶氮化合物
公开(公告)号：US06313275B1
公开(公告)日：2001-11-06
申请号：US09582781
申请日：2000-07-03
申请人： Rolf Mülhaupt , Martin Baumert , Michael Geprägs
发明人： Rolf Mülhaupt , Martin Baumert , Michael Geprägs
IPC分类号： C07D26310
CPC分类号： C07D263/10 , C08F271/02 , C08F293/005
摘要： Azo compounds of the formula (I) are functionalized with heterocycles.
摘要翻译：式（I）的偶氮化合物用杂环官能化

10. 发明授权

US09120909B2 Polymer-graphite nanocomposites 有权
标题翻译：聚合物 - 石墨纳米复合材料
公开(公告)号：US09120909B2
公开(公告)日：2015-09-01
申请号：US13496806
申请日：2010-09-13
申请人： Hans-Helmut Görtz , Rolf Minkwitz , Rolf Mülhaupt , Rainer Wissert , Peter Steurer
发明人： Hans-Helmut Görtz , Rolf Minkwitz , Rolf Mülhaupt , Rainer Wissert , Peter Steurer
IPC分类号： H01B1/06 , C08K3/04 , H01B1/24 , C08J3/215
CPC分类号： C08K3/04 , C08J3/215 , C08J2325/12 , C08K3/041 , C08K2201/011 , H01B1/24 , C08L25/12
摘要： Process for producing a polymer-graphite nanocomposite, which comprises the steps a) oxidation of graphite to graphite oxide, b) conversion of the graphite oxide into an aqueous dispersion, c) mixing of the aqueous dispersion comprising graphite oxide or, if appropriate, reduced graphite oxide which is obtained from b) with an aqueous polymer dispersion comprising at least one polymer and d) separating off the polymer-graphite mixture from the aqueous phase, wherein the graphite oxide which has been oxidized in step a) is reduced to graphite between step b) and c) or between step c) and d).
摘要翻译：制备聚合物 - 石墨纳米复合材料的方法，其包括以下步骤：a）将石墨氧化成氧化石墨，b）将石墨氧化物转化为水分散体，c）将包含氧化石墨的水性分散体，或如果合适的话，由b）得到的石墨氧化物与包含至少一种聚合物的聚合物水分散体分散体，和d）从水相中分离出聚合物 - 石墨混合物，其中在步骤a）中被氧化的氧化石墨被还原成石墨在步骤b）和c）或步骤c）和d）之间。

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