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1. 发明授权

US08821784B2 Bottles prepared from compositions of polypropylene and inorganic nucleating agents 有权
标题翻译：由聚丙烯和无机成核剂的组合物制备的瓶
公开(公告)号：US08821784B2
公开(公告)日：2014-09-02
申请号：US11793510
申请日：2005-12-21
申请人： Valerie Smits , Emmanuel Humbeeck , Kristien Roegiers
发明人： Valerie Smits , Emmanuel Humbeeck , Kristien Roegiers
IPC分类号： B29C49/06 , B29C49/12 , C08K5/00 , B29C49/00 , B29B11/14 , B29K25/00 , B29K23/00 , B29K67/00 , B29B11/08 , B29K105/00 , B29C49/64 , B29K27/06
CPC分类号： C08K5/0083 , B29B11/08 , B29B11/14 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14106 , B29B2911/14133 , B29B2911/14326 , B29B2911/14333 , B29B2911/1444 , B29B2911/14466 , B29B2911/14686 , B29B2911/14693 , B29B2911/14713 , B29B2911/14726 , B29B2911/14753 , B29B2911/1476 , B29B2911/1488 , B29B2911/14886 , B29C49/0005 , B29C49/06 , B29C49/12 , B29C49/6445 , B29K2023/06 , B29K2023/12 , B29K2025/00 , B29K2027/06 , B29K2067/00 , B29K2105/258 , C08L23/12 , C08L23/10 , C08L23/14
摘要： This invention discloses bottles and pre-forms prepared by injection-stretch-blow-molding (ISBM) from a composition comprising polypropylene and an inorganic non-sorbitol nucleating agent.
摘要翻译：本发明公开了由包含聚丙烯和无机非山梨糖醇成核剂的组合物通过注射拉伸吹塑（ISBM）制备的瓶和预成型体。

2. 发明申请

US20120283388A1 POLYOLEFINS MODIFIED BY SILICONES 审中-公开
标题翻译：硅改性聚硅氧烷
公开(公告)号：US20120283388A1
公开(公告)日：2012-11-08
申请号：US13520855
申请日：2010-12-22
申请人： Michael Backer , Thomas Chausse , Francois De Buyl , Damien Deheunynck , Satoshi Onodera , Valerie Smits
发明人： Michael Backer , Thomas Chausse , Francois De Buyl , Damien Deheunynck , Satoshi Onodera , Valerie Smits
IPC分类号： C08F255/02 , C08F8/00
CPC分类号： C08L23/06 , C08F8/42 , C08F290/04 , C08F290/042 , C08F299/08 , C08L23/12 , C08L51/06 , C08L83/10 , C08F10/00 , C08L2666/24 , C08L2666/06 , C08F230/08 , C08F236/14
摘要： The invention provides a process for grafting silicone onto a polyolefin comprising reacting the polyolefin with a silicon compound containing an unsaturated group in the presence of means capable of generating free radical sites in the polyolefin, characterized in that the silicon compound is a branched silicone resin containing at least one group of the formula —X—CH═CH—R″ (I) or —X—C≡C—R″ (II), in which X represents a divalent organic linkage having an electron withdrawing effect with respect to the —CH═CH— or —C≡C-bond and/or containing an aromatic ring or a further olefinic double bond or acetylenic unsaturation, the aromatic ring or the further olefinic double bond or acetylenic unsaturation being conjugated with the olefinic unsaturation of —X—CH═CH—R″ or with the acetylenic unsaturation of —X—C≡C—R″, X being bonded to the branched silicone resin by a C—Si bond, and R″ represents hydrogen or a group having an electron withdrawing effect or any other activation effect with respect to the —CH═CH— or —C□C-bond. The polyolefin is reinforced by grafting the branched silicone resin onto it.
摘要翻译：本发明提供一种将聚硅氧烷接枝到聚烯烃上的方法，包括使聚烯烃与含有不饱和基团的硅化合物在能够在聚烯烃中产生自由基位点的方式存在下反应，其特征在于硅化合物是含有至少一个式-X-CH = CH-R“（I）或-X-C≡C-R”（II）的基团，其中X表示具有相对于 -CH = CH-或-C≡C-键和/或含有芳环或另外的烯属双键或炔属不饱和键，所述芳环或其它烯属双键或炔属不饱和键与-X 1的烯属不饱和键 -CH = CH-R“或-X-C≡C-R”的炔属不饱和度，X通过C-Si键与支链硅氧烷树脂键合，R“表示氢或具有吸电子基团翼效应或相对于-CH = CH-或-C≡C-键的任何其它活化效应。通过将支化硅树脂接枝到其上来增强聚烯烃。

3. 发明授权

US08476375B2 Polymers modified by silanes 有权
标题翻译：由硅烷改性的聚合物
公开(公告)号：US08476375B2
公开(公告)日：2013-07-02
申请号：US13001677
申请日：2009-07-02
申请人： Michael Backer , Valerie Smits , Damien Deheunynck
发明人： Michael Backer , Valerie Smits , Damien Deheunynck
IPC分类号： C08F230/08 , C08F4/34 , C08J3/28 , C08J9/04 , C08L51/06
CPC分类号： C08F255/02 , C08F255/00 , C08L51/06 , C08L2666/04 , C08L2666/02
摘要： The invention relates to a process for grafting hydrolysable silane groups to a polyolefin, comprising reacting the polyolefin with an unsaturated silane, containing an olefinic —C═C— bond or acetylenic —C≡C— bond and having at least one hydrolysable group bonded to Si, or a hydrolysate thereof, in the presence of means capable of generating free radical sites in the polymer. The silane contains an aromatic ring or a further olefinic double bond or acetylenic unsaturation, the aromatic ring or the further olefinic double bond or acetylenic unsaturation being conjugated with the olefinic —C═C— or acetylenic —C≡C— unsaturation of the silane. The unsaturated silane may also contains electron-withdrawing moiety with respect to the olefinic —C═C— or acetylenic —C≡C— bond. The invention permits to provide a silane-modified polyolefin having a high grafting efficiency while limiting/preventing polymer degradation by chain scission. The silane-modified polyolefin can be further reacted with a polar surface, a filler or a polar polymer or reacted on itself to crosslink the polyolefin and obtain enhanced physical properties of the composites made thereof.
摘要翻译：本发明涉及将可水解硅烷基接枝到聚烯烃上的方法，包括使聚烯烃与不饱和硅烷反应，所述不饱和硅烷含有烯烃-C = C-键或炔属-C = C-键并且具有至少一个可水解基团键合到 Si或其水解产物，在能够在聚合物中产生自由基位点的手段存在下进行。所述硅烷含有芳环或其它烯属双键或炔属不饱和键，所述芳环或所述其它烯属双键或炔属不饱和键与所述硅烷的烯烃-C = C-或炔属-C = C-不饱和键结合。相对于烯烃-C = C-或炔属-C = C-键，不饱和硅烷还可含有吸电子部分。本发明允许提供具有高接枝效率的硅烷改性聚烯烃，同时通过链断裂限制/防止聚合物降解。硅烷改性的聚烯烃可以进一步与极性表面，填料或极性聚合物反应，或者自身反应以使聚烯烃交联并获得由其制成的复合材料的增强的物理性能。

4. 发明授权

US08314164B2 Filled rubber compositions 失效
标题翻译：填充橡胶组合物
公开(公告)号：US08314164B2
公开(公告)日：2012-11-20
申请号：US12745213
申请日：2008-11-28
申请人： Valerie Smits , Michael Backer , Sebastien Grofils , Thierry Materne , Laurence Stelandre , Randall Schmidt , Steven Swier , Thomas Chaussee
发明人： Valerie Smits , Michael Backer , Sebastien Grofils , Thierry Materne , Laurence Stelandre , Randall Schmidt , Steven Swier , Thomas Chaussee
IPC分类号： C08L1/02 , C08K3/34
CPC分类号： B60C1/00 , C08K3/36 , C08K5/5419 , C08K5/5425 , C08K5/548 , C08L9/00 , C08L9/06 , C08L21/00 , C08L83/04 , C08L2666/02 , C08L83/00
摘要： The present invention relates to a curable rubber composition comprising an organic elastomer, a filler and at least one curing agent for the elastomer. Such curable rubber compositions are widely used in the production of cured rubber articles, such as tires, belts and hoses. The composition contains a branched silicone resin having Si-bonded hydroxyl groups or azo groups. This may lead to a reduction in the mixing energy required for processing, particularly in the energy required in the first (non-productive) mixing phase to give good dispersion of the filler in the organic elastomer. Use of the branched silicone resin can also accelerate cure (vulcanization), thus reducing the required cure time or reducing the amount of cure accelerator required.
摘要翻译：本发明涉及包含有机弹性体，填料和至少一种用于弹性体的固化剂的可固化橡胶组合物。这种可固化橡胶组合物广泛用于生产固化橡胶制品，如轮胎，皮带和软管。该组合物含有具有Si键合的羟基或偶氮基团的支链硅树脂。这可能导致加工所需的混合能量的降低，特别是在第一（非生产性）混合阶段所需的能量中，以使填料在有机弹性体中得到良好的分散。使用支化硅树脂也可以加速固化（硫化），从而减少所需的固化时间或减少所需的固化促进剂的量。

5. 发明申请

US20120283346A1 Modified Polyolefins 有权
标题翻译：改性聚烯烃
公开(公告)号：US20120283346A1
公开(公告)日：2012-11-08
申请号：US13520859
申请日：2010-12-22
申请人： Michael Backer , Francois De Buyl , Damien Deheunynck , Jean De La Croix Habimana , Vincent Rerat , Valerie Smits
发明人： Michael Backer , Francois De Buyl , Damien Deheunynck , Jean De La Croix Habimana , Vincent Rerat , Valerie Smits
IPC分类号： C08L23/36 , C08L23/26 , C08J9/00
CPC分类号： C08F255/02 , C08F212/14 , C08F230/08 , C08F236/14
摘要： The invention provides a process for grafting silane or silicone functionality onto a polyolefin, comprising reacting the polyolefin with an unsaturated monomer (A) containing an olefinic —C═C— bond or acetylenic —C≡C— bond and a reactive functional group X in the presence of means capable of generating free radical sites in the polyolefin and with an organosilicon compound (B) having a functional group Y which is reactive with the functional group X of the unsaturated monomer (A), characterized in that the unsaturated monomer (A) contains an aromatic ring or a further olefinic double bond or acetylenic unsaturation, the aromatic ring or the further olefinic double bond or acetylenic unsaturation being conjugated with the olefinic —C═C— or acetylenic —C≡C— unsaturation of the unsaturated monomer (A).
摘要翻译：本发明提供将硅烷或硅氧烷官能度接枝到聚烯烃上的方法，包括使聚烯烃与含有烯烃-C≡C-键或炔属-C≡C-键和反应性官能团X的不饱和单体（A）反应存在能够在聚烯烃中产生自由基位点的装置和具有与不饱和单体（A）的官能团X反应的官能团Y的有机硅化合物（B）的存在，其特征在于不饱和单体（A ）含有芳环或另外的烯属双键或炔属不饱和键，芳环或其它烯属双键或炔属不饱和键与不饱和单体的烯属-C≡C-或炔属-C≡C-不饱和键相结合（一个）。

6. 发明申请

US20070246866A1 Polypropylene Processing with Reduced Cycle Time in Injection-Stretch-Blow Moulding 审中-公开
标题翻译：聚丙烯加工在注塑 - 吹塑成型中减少循环时间
公开(公告)号：US20070246866A1
公开(公告)日：2007-10-25
申请号：US10579266
申请日：2004-11-05
申请人： Valerie Smits
发明人： Valerie Smits
IPC分类号： B29C49/06
CPC分类号： B29C49/0005 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14053 , B29B2911/14066 , B29B2911/1408 , B29B2911/14093 , B29B2911/14106 , B29B2911/14113 , B29B2911/14133 , B29B2911/1414 , B29C49/06 , B29C49/08 , B29K2023/12 , B29K2995/0022 , B29K2995/0089 , B29L2031/712
摘要： This invention discloses the use of metallocene-produced polypropylene to prepare single- or multi-layer articles by injection-stretch blow moulding with a reduced cycle time, said article having excellent optical properties and rigidity.
摘要翻译：本发明公开了使用金属茂制备的聚丙烯通过注射拉伸吹塑成型制备单层或多层制品，循环时间缩短，所述制品具有优异的光学性能和刚性。

7. 发明申请

US20070129518A1 High dimension stability and high processability polyethylene in injection molding 审中-公开
标题翻译：高尺寸稳定性和高加工性聚乙烯注塑成型
公开(公告)号：US20070129518A1
公开(公告)日：2007-06-07
申请号：US10512393
申请日：2003-04-24
申请人： Eric Maziers , Ludovic Leplatois , Valerie Smits
发明人： Eric Maziers , Ludovic Leplatois , Valerie Smits
IPC分类号： C08F110/02
CPC分类号： C08F10/02 , C08F4/65927 , C08F110/02 , Y02P20/52 , C08F2500/12 , C08F2500/09 , C08F2500/07
摘要： This invention discloses single layer articles having improved dimensional stability and improved processability produced by injection moulding and consisting essentially of polyethylene (PE) resins prepared with a bisindenyl metallocene catalyst system.
摘要翻译：本发明公开了具有改进的尺寸稳定性和改进的通过注射成型制备的加工性并且基本上由用双茚基金属茂催化剂体系制备的聚乙烯（PE）树脂组成的单层制品。

8. 发明授权

US09181379B2 Modified polyolefins 有权
标题翻译：改性聚烯烃
公开(公告)号：US09181379B2
公开(公告)日：2015-11-10
申请号：US13520859
申请日：2010-12-22
申请人： Michael Backer , Francois De Buyl , Damien Deheunynck , Jean De La Croix Habimana , Vincent Rerat , Valerie Smits
发明人： Michael Backer , Francois De Buyl , Damien Deheunynck , Jean De La Croix Habimana , Vincent Rerat , Valerie Smits
IPC分类号： C08L23/26 , C08F255/02 , C08F212/14 , C08F230/08
CPC分类号： C08F255/02 , C08F212/14 , C08F230/08 , C08F236/14
摘要： The invention provides a process for grafting silane or silicone functionality onto a polyolefin, comprising reacting the polyolefin with an unsaturated monomer (A) containing an olefinic —C═C— bond or acetylenic —C≡C— bond and a reactive functional group X in the presence of means capable of generating free radical sites in the polyolefin and with an organosilicon compound (B) having a functional group Y which is reactive with the functional group X of the unsaturated monomer (A), characterized in that the unsaturated monomer (A) contains an aromatic ring or a further olefinic double bond or acetylenic unsaturation, the aromatic ring or the further olefinic double bond or acetylenic unsaturation being conjugated with the olefinic —C═C— or acetylenic —C≡C— unsaturation of the unsaturated monomer (A).
摘要翻译：本发明提供将硅烷或硅氧烷官能度接枝到聚烯烃上的方法，包括使聚烯烃与含有烯烃-C≡C-键或炔属-C≡C-键和反应性官能团X的不饱和单体（A）反应存在能够在聚烯烃中产生自由基位点的装置和具有与不饱和单体（A）的官能团X反应的官能团Y的有机硅化合物（B）的存在，其特征在于不饱和单体（A ）含有芳环或另外的烯属双键或炔属不饱和键，芳环或其它烯属双键或炔属不饱和键与不饱和单体的烯属-C≡C-或炔属-C≡C-不饱和键相结合（一个）。

9. 发明授权

US08569417B2 Modified polyolefins 有权
标题翻译：改性聚烯烃
公开(公告)号：US08569417B2
公开(公告)日：2013-10-29
申请号：US13001668
申请日：2009-07-02
申请人： Michael Backer , Francois De Buyl , Valerie Smits , Damien Deheunynck
发明人： Michael Backer , Francois De Buyl , Valerie Smits , Damien Deheunynck
IPC分类号： C08F255/00 , C08F255/02 , C08F8/12 , C08F8/42
CPC分类号： C08F255/00 , C08F255/02 , C08F255/08 , C08L51/06 , C08L2666/02 , C09D151/06 , C09J151/06
摘要： The invention relates to a process for grafting hydrolysable silane groups to a polyolefin in which ethylene units, if present, form less than 50% by weight of the total polyolefin. The polyolefin is reacted with an unsaturated silane, having at least one hydrolysable group bonded to Si, or a hydrolysate thereof, in the presence of means capable of generating free radical sites in the polyolefin. The unsaturated silane has the formula R″—CH═CH—Z (I) or R″—C≡C—Z (II) in which Z represents an electron-withdrawing moiety substituted by a —SiRaR′(3-a) group wherein R represents a hydrolysable group; R′ represents a hydrocarbyl group having 1 to 6 carbon atoms; a has a value in the range 1 to 3 inclusive; and R″ represents hydrogen or a group having an electron withdrawing or any other activation effect with respect to the —CH═CH— or —C≡C— bond. The use of an unsaturated silane of the formula R″—CH═CH—Z (I) or R″—C≡C—Z (II) in carrying out the grafting reaction on the polyolefin may give enhanced grafting yield compared to grafting with an olefinically unsaturated silane such as vinyltrimethoxysilane not containing an electron withdrawing moiety Z. The invention permits to provide a silane-modified polyolefin having a high grafting efficiency while limiting/preventing polymer degradation by chain scission. The silane-modified polyolefin can be further reacted with a polar surface, a filler or a polar polymer or reacted on itself to crosslink the polyolefin and obtain enhanced physical properties of the composites made thereof.
摘要翻译：本发明涉及一种将可水解硅烷基接枝到聚烯烃上的方法，其中乙烯单元（如果存在的话）占总聚烯烃的小于50重量％。在能够在聚烯烃中产生自由基位点的手段的存在下，聚烯烃与不饱和硅烷反应，所述不饱和硅烷具有与Si结合的至少一个可水解基团或其水解产物。不饱和硅烷具有式R“-CH = CH-Z（I）或R”C = CZ（II），其中Z表示被-SiRaR'（3-a）基团取代的吸电子部分其中R表示可水解基团; R'表示碳原子数1〜6的烃基。 a的值在1到3的范围内; R“表示氢或相对于-CH = CH-或-C = C-键具有吸电子或任何其它活化作用的基团。在聚烯烃上进行接枝反应时，使用式R'-CH = CH-Z（I）或R“C = CZ（II）的不饱和硅烷可以提高接枝率，烯属不饱和硅烷如不含吸电子部分Z的乙烯基三甲氧基硅烷。本发明允许提供具有高接枝效率的硅烷改性聚烯烃，同时通过链断裂限制/防止聚合物降解。硅烷改性的聚烯烃可以进一步与极性表面，填料或极性聚合物反应，或者自身反应以使聚烯烃交联并获得由其制成的复合材料的增强的物理性能。

10. 发明申请

US20120289620A1 Process For Forming Crosslinked and Branched Polymers 有权
标题翻译：形成交联和支化聚合物的方法
公开(公告)号：US20120289620A1
公开(公告)日：2012-11-15
申请号：US13520866
申请日：2010-12-22
申请人： Damien Deheunynck , Valerie Smits
发明人： Damien Deheunynck , Valerie Smits
IPC分类号： C08F255/02 , C08J3/24
CPC分类号： C08F255/02 , C08J3/242 , C08J2309/00 , C08J2323/02 , C08F222/1006 , C08F236/14
摘要： The invention provides a polymer composition comprising a polyolefin or a diene elastomer, and an unsaturated compound (A) containing at least two groups each comprising an olefinic —C═C— bond or acetylenic —C≡C— bond, characterized in that each group comprising an olefinic —C═C— bond or acetylenic —C≡C— bond in the unsaturated compound (A) contains an aromatic ring or a further olefinic double bond or acetylenic unsaturation, the aromatic ring or the further olefinic double bond or acetylenic unsaturation being conjugated with the olefinic —C═C— or acetylenic —C≡C— unsaturation. The use of a multifunctional unsaturated compound (A) containing an aromatic ring or a further olefinic bond conjugated with the olefinic —C═C— or acetylenic —C≡C— unsaturation of the multifunctional unsaturated compound gives enhanced crosslinking and/or branching yield and/or less degradation of the polymer compared to crosslinking with a multifunctional unsaturated compound not containing an aromatic ring or a further olefinic bond.
摘要翻译：本发明提供包含聚烯烃或二烯弹性体的聚合物组合物和含有至少两个各自包含烯属-C≡C-键或炔属-C≡C-键的基团的不饱和化合物（A），其特征在于每个基团在不饱和化合物（A）中包含烯属-C≡C-键或炔属-C≡C-键含有芳环或其它烯属双键或炔属不饱和键，芳环或其它烯属双键或炔属不饱和键与烯属-C≡C-或炔属-C≡C-不饱和键共轭。使用多官能不饱和化合物（A）含有芳族环或与多官能不饱和化合物的-C≡C-或炔属-C≡C-不饱和烯烃共轭的另外的烯键，可提高交联和/或支链产率， /或者与不含芳族环或另外的烯键的多官能不饱和化合物的交联相比，聚合物的降解降低。

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